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Analytische Chemie: 1

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Bibliographische Detailangaben
Beteilige Person:	Ritgen, Ulf 1969- (VerfasserIn)
Format:	Buch
Sprache:	Deutsch
Veröffentlicht:	Berlin Springer Spektrum [2019]
Schlagwörter:	Analytische Chemie 1652: Hardcover, Softcover / Chemie/Theoretische Chemie A Analytik Analytik Praktikum Band I Chromatographie Einführung Massenspektrometrie NMR NMR-Spektroskopie PNF Paperback / softback SCC11006: Analytical Chemistry SCI013010 SUCO11644: Chemistry and Materials Science
Links:	http://deposit.dnb.de/cgi-bin/dokserv?id=35b1b320edc34ec29b65742b0a6e045d&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031845266&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Umfang:	XI, 306 Seiten Illustrationen, Diagramme
ISBN:	9783662604946

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Datensatz im Suchindex

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adam_text	INHALTSVERZEICHNIS I GRUNDLAGEN 1 GRUNDBEGRIFFE DER ANALYTIK ....................................................................................................... 5 1.1 VERSUCHSPLANUNG ..................................................................................................................................... 6 1.2 UND WIE KOMME ICH ZU EINER BRAUCHBAREN ANTWORT? ............................................................................ 7 2 PROBENNAHME UND PROBENVORBEREITUNG ............................................................................... 11 2.1 TRENNVERFAHREN ....................................................................................................................................... 13 2.2 PROBENTROCKNUNG ................................................................................................................................... 20 3 QUALITAETSSICHERUNG UND KALIBRIERUNG ...................................................................................... 23 3.1 ALLES MUSS SEINE ORDNUNG HABEN: DIE NORM .......................................................................................... 26 3.2 MENGENBEREICHE ..................................................................................................................................... 29 3.3 KALIBRIERUNG ............................................................................................................................................ 31 3.4 STANDARD IST NICHT GLEICH STANDARD ......................................................................................................... 34 3.5 ANALYTISCHE QUALITAETSSICHERUNG (AQS) UND GUTE LABORPRAXIS (GLP) ................................................... 36 3.6 SIGNIFIKANTE ZIFFERN ODER: WANN IST GENAU EINDEUTIG ZU GENAU? .......................................................... 37 3.7 EIN KURZER AUSFLUG IN DIE STATISTIK .......................................................................................................... 44 ANTWORTEN ............................................................................................................................................... 48 LITERATUR .................................................................................................................................................... 54 II MASSANALYSE 4 ALLGEMEINES ZUR MASSANALYSE .................................................................................................... 59 5 MASSANALYSE MIT SAEUREN UND BASEN ......................................................................................... 63 5.1 STARKE SAEURE MIT STARKER BASE (UND UMGEKEHRT) ................................................................................... 69 5.2 SCHWACHE SAEURE MIT STARKER BASE/SCHWACHE BASE MIT STARKER SAEURE .................................................... 72 5.3 MEHRPROTONIGE SAEUREN ........................................................................................................................... 80 5.4 ENDPUNKTBESTIMMUNG ........................................................................................................................... 81 6 MASSANALYSE MIT KOMPLEXEN (KOMPLEXOMETRIE) ................................................................... 85 6.1 KOMBINATION ZWEIER PRINZIPIEN .............................................................................................................. 86 6.2 VIELSEITIG UND VIELGENUTZT: EDTA ............................................................................................................ 88 7 EINE KOMBINATION MIT BEACHTLICHEM POTENTIAL: REDOX-TITRATIONEN .................................. 93 7.1 KURZGESCHLOSSENES ................................................................................... 94 7.2 REFERENZWERTE ........................................................................................................................................ 95 7.3 DER ENDPUNKT (FAST WIE BEI SAEUREN UND BASEN) ..................................................................................... 99 8 SCHWERLOESLICHKEIT KANN VON VORTEIL SEIN: FAELLUNGSTITRATION ................................................ 101 8.1 DIE BEDEUTUNG DES LOESLICHKEITSPRODUKTS ............................................................................................. 102 8.2 GRAPHISCHE DARSTELLUNG ......................................................................................................................... 103 8.3 BESTIMMUNG DES ENDPUNKTS ................................................................................................................... 104 9 GRAVIMETRIE ................................................................................................................................. 105 9.1 FAELLUNGSFORM ............................................................................................................................................ 106 9.2 WIEGEFORM (WAEGEFORM) ................................................................................. - ...................................... 107 9.3 SONDERFALL: ELEKTROGRAVIMETRIE ............................................................................................................... 108 X INHALTSVERZEICHNIS 10 AUSGEWAEHLTE DETEKTIONSMETHODEN .......................................................................................... 109 10.1 DER FARBUMSCHLAG: KOLORIMETRIE ............................................................................................................... 110 10.2 VERAENDERTES ABSORPTIONSVERHALTEN: PHOTOMETRIE .................................................................................... 111 10.3 VERAENDERUNGEN DES ELEKTROCHEMISCHEN POTENTIALS: POTENTIOMETRIE .................................................... 113 10.4 VERAENDERUNGEN DER ELEKTRISCHEN LEITFAEHIGKEIT: KONDUKTOMETRIE ......................................................... 113 ANTWORTEN ................................................................................................................................................. 116 WEITERFUEHRENDE LITERATUR ........................................................................................................................... 122 III CHROMATOGRAPHISCHE METHODEN 11 ALLGEMEINES ZUR CHROMATOGRAPHIE ........................................................................................... 127 12 FLUESSIGCHROMATOGRAPHIE (LC) ..................................................................................................... 131 12.1 DUENNSCHICHTCHROMATOGRAPHIE (TLC) ....................................................................................................... 132 12.2 SAEULENCHROMATOGRAPHIE ........................................................................................................................... 134 12.3 HOCHLEISTUNGS-SAEULENCHROMATOGRAPHIE (HPLC) .................................................................................... 146 12.4 DETEKTIONSMETHODEN .............................................................................................................................. 153 13 GASCHROMATOGRAPHIE (GC) ......................................................................................................... 155 13.1 SAEULEN IN DER GC ...................................................................................................................................... 156 13.2 DETEKTOREN .................................................................................................................................................. 159 14 SPEZIELLERE FORMEN DER CHROMATOGRAPHIE .............................................................................. 161 14.1 IONENAUSTAUSCHER-SAEULEN ....................................................................................................................... 162 14.2 AUSSCHLUSSCHROMATOGRAPHIE .................................................................................................................. 165 14.3 AFFINITAETSCHROMATOGRAPHIE ...................................................................................................................... 166 15 ELEKTROPHORESE ............................................................................................................................ 169 15.1 KAPILLARELEKTROPHORESE (CE) .................................................................................................................... 170 15.2 GELELEKTROPHORESE ................................................................................................................................... 173 16 WAHL DER METHODIK ...................................................................................................................... 177 ANTWORTEN ................................................................................................................................................. 180 WEITERFUEHRENDE LITERATUR ........................................................................................................................... 183 IV MOLEKUELSPEKTROSKOPIE 17 ALLGEMEINES ZUR SPEKTROSKOPIE ................................................................................................. 189 18 ANREGUNG VON ELEKTRONEN ......................................................................................................... 195 18.1 SPEKTROPHOTOMETRIE UND UV/VIS-SPEKTROSKOPIE .................................................................................. 196 18.2 WAS BEWIRKT DIE VOM PHOTON UEBERTRAGENE ENERGIE? .............................................................................. 199 18.3 WER MACHT WAS? .......................................................................................................................................... 212 18.4 RUECKKEHR IN DER GRUNDZUSTAND .................................................................................................................. 217 18.5 TECHNISCHE ASPEKTE VON (SPEKTRAL-)PHOTOMETERN ...................................................................................... 224 18.6 ANWENDUNGEN ............................................................................................................................................ 227 19 SCHWINGUNGSSPEKTROSKOPIE ........................................................................................................ 229 19.1 SCHWINGUNGSMODI ..................................................................................................................................... 230 19.2 INFRAROTSPEKTROSKOPIE (IR) ......................................................................................................................... 233 19.3 AEHNLICH, UND DOCH ANDERS: RAMAN-SPEKTROSKOPIE .................................................................................... 241 ANTWORTEN ................................................................................................................................................... 244 WEITERFUEHRENDE LITERATUR ............................................................................................................................. 248 INHALTSVERZEICHNIS XI V ATOMSPEKTROSKOPIE 20 ALLGEMEINES ZUR ATOMSPEKTROSKOPIE ....................................................................................... 251 20.1 DIE ATOMISIERUNG ..................................................................................................................................... 253 20.1.1 FLAMMEN ..................................................................................................................................................... 253 20.1.2 OFEN ........................................................................................................................................................... 255 20.1.3 PLASMA ........................................................................................................................................................ 256 21 ATOMABSORPTIONSSPEKTROSKOPIE (AAS) .................................................................................... 259 21.1 ANREGUNGSZUSTAENDE DER ATOME ................................................................................................................ 260 21.2 LICHTQUELLEN .............................................................................................................................................. 264 22 ATOMEMISSIONSSPEKTROMETRIE (AES, OES) ................................................................................ 267 22.1 DER HISTORISCHE VORLAEUFER: FLAMMENPHOTOMETRIE ................................................................................... 268 22.2 ICP-OES ...................................................................................................................................................... 268 22.3 IN KOMBINATION MIT DER MASSENSPEKTROMETRIE ....................................................................................... 270 23 ROENTGENFLUORESZENZANALYSE (RFA) ............................................................................................ 273 23.1 DAS GRUNDPRINZIP ..................................................................................................................................... 274 23.2 DETEKTION DER RESULTIERENDEN PHOTONEN ................................................................................................. 277 ANTWORTEN ................................................................................................................................................. 281 LITERATUR ...................................................................................................................................................... 282 SERVICETEIL GLOSSAR ........................................................................................................................................................ 286 STICHWORTVERZEICHNIS ................................................................................................................................ 303
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spellingShingle	Ritgen, Ulf 1969- Analytische Chemie Analytische Chemie (DE-588)4129906-1 gnd
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title	Analytische Chemie
title_auth	Analytische Chemie
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title_full	Analytische Chemie 1 Ulf Ritgen
title_fullStr	Analytische Chemie 1 Ulf Ritgen
title_full_unstemmed	Analytische Chemie 1 Ulf Ritgen
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