Verfügbarkeit: History of number | Technische Universität München

History of number: evidence from Papua New Guinea and Oceania

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Bibliographische Detailangaben
Beteiligte Personen:	Owens, Kay (VerfasserIn), Lean, Glen (VerfasserIn), Paraide, Patricia (VerfasserIn), Muke, Charly (VerfasserIn)
Format:	Elektronisch E-Book
Sprache:	Englisch
Veröffentlicht:	Cham, Switzerland Springer [2018]
Schriftenreihe:	History of mathematics education
Schlagwörter:	Geschichte Education Mathematics History Mathematics / Study and teaching Mathematics Education History of Mathematical Sciences Ethnomathematik Mathematikunterricht Zahl Ozeanien Papua-Neuguinea
Links:	https://doi.org/10.1007/978-3-319-45483-2 https://doi.org/10.1007/978-3-319-45483-2 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030099963&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Umfang:	1 Online-Ressource (xxvii, 461 Seiten) Illustrationen
ISBN:	9783319454832
DOI:	10.1007/978-3-319-45483-2

Internformat

MARC


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Datensatz im Suchindex

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adam_text	IMAGE 1 CONTENTS 1 INTRODUCTION 1 REFERENCES 3 2 BACKGROUND 5 2.1 ASYMMETRIC ORGANOCATALYSIS 5 2.1.1 HISTORICAL DEVELOPMENT 5 2.1.2 CLASSIFICATION 6 2.1.3 AMINOCATALYSIS 7 2.2 CATALYTIC ASYMMETRIC EPOXIDATION O F ELECTRON-DEFICIENT OLEFINS 15 2.2.1 MILESTONES IN CATALYTIC ASYMMETRIC OLEFIN EPOXIDATIONS 15 2.2.2 WEITZ-SCHEFFER EPOXIDATION 17 2.2.3 SYNTHETIC VERSATILITY O F A,(3-EPOXY KETONES 19 2.2.4 STATE O F THE ART: CATALYTIC ASYMMETRIC EPOXIDATION O F A,(3-UNSATURATED KETONES 19 2.2.5 RECENT ADVANCES: THE ORGANOCATALYTIC APPROACH 2 4 2.2.6 ASYMMETRIC EPOXIDATION O F CYCLIC OE,\|3-UNSATURATED KETONES 28 2.3 SYNTHESIS AND RELEVANCE OF 3-HYDROXY-L,2-DIOXOLANES AND 1,2-DIOXOLANES 30 2.3.1 PEROXIDIC NATURAL PRODUCTS 31 2.3.2 GENERAL METHODS FOR THE SYNTHESIS OF 3-HYDROXY-L,2-DIOXOLANES 32 REFERENCES 35 3 OBJECTIVES O F THIS PH.D. WORK 41 REFERENCES 43 4 RESULTS AND DISCUSSION 45 4.1 CATALYTIC ASYMMETRIC EPOXIDATION O F CYCLIC ENONES 45 I X HTTP://D-NB.INFO/1018468935 IMAGE 2 X C O N T E N T S 4.1.1 SCREENING STUDIES 45 4.1.2 REACTION SCOPE AND DISCUSSION 55 4.1.3 SUMMARY AND CONCLUSIONS 73 4.2 CATALYTIC ASYMMETRIC EPOXIDATION AND HYDROPEROXIDATION OF ACYCLIC ENONES 75 4.2.1 SCREENING STUDIES 75 4.2.2 REACTION SCOPE AND DISCUSSION 85 4.2.3 SUMMARY AND CONCLUSIONS 103 4.3 SYNTHETIC TRANSFORMATIONS O F OPTICALLY ACTIVE OC,P-EPOXY KETONES AND 3-HYDROXY-1,2-DIOXOLANES 105 4.3.1 ONE-POT SYNTHESIS O F ALDOL PRODUCTS FROM A,(3-UNSATURATED KETONES 105 4.3.2 SYNTHESIS OF ALDOL PRODUCTS BY REDUCTIVE CLEAVAGE O F A,P-EPOXY KETONES 108 4.3.3 SYNTHESIS OF 1,2-DIOXOLANES FROM PEROXYHEMIKETALS. . . . I L L 4.4 SUMMARY AND CONCLUSIONS 113 4.5 MECHANISTIC CONSIDERATIONS 113 4.5.1 EVALUATION OF MODIFIED CATALYSTS: STRUCTURE-ACTIVITY RELATIONSHIPS 113 4.5.2 ESI-MS STUDIES 116 4.5.3 FURTHER MECHANISTIC INVESTIGATIONS 120 4.5.4 SUMMARY AND CONCLUSIONS 121 4.6 PREPARATION O F STARTING MATERIALS 126 4.6.1 PREPARATION O F CYCLIC [^UNSATURATED KETONES 126 4.6.2 PREPARATION OF ACYCLIC A,P-UNSATURATED KETONES 128 4.7 CATALYST SYNTHESIS 131 4.7.1 SYNTHESIS OF CHIRAL PRIMARY AMINES BASED ON THE QUINUCLIDINE SCAFFOLD 131 4.7.2 SYNTHESIS OF AMINO ACID-DERIVED DIAMINES 134 4.7.3 SYNTHESIS OF BINOL-DERIVED PHOSPHORIC ACIDS 135 REFERENCES 137 5 SUMMARY 141 6 OUTLOOK 147 REFERENCES 151 7 EXPERIMENTAL PART 153 7.1 GENERAL EXPERIMENTAL CONDITIONS 153 7.2 CATALYTIC ASYMMETRIC EPOXIDATION O F CYCLIC ENONES 156 7.2.1 GENERAL PROCEDURE 156 7.2.2 SCOPE O F OPTICALLY ACTIVE CYCLIC A, P-EPOXYKETONES . . . . 157 7.3 CATALYTIC ASYMMETRIC HYDROPEROXIDATION AND EPOXIDATION OF ACYCLIC ENONES 172 IMAGE 3 CONTENTS XI 7.3.1 CATALYTIC ASYMMETRIC HYDROPEROXIDATION OF ACYCLIC ENONES 172 7.3.2 SYNTHESIS O F (/?)-4-(7ERT-BUTYLPEROXY)DECAN-2-ONE 7?)-95A) 182 7.3.3 CATALYTIC ASYMMETRIC EPOXIDATION OF ACYCLIC ENONES. . . 182 7.3.4 HYDROPEROXIDATION OF 4,8-DIMETHYLNONA-3,7- DIEN-2-ONE (100) 194 7.3.5 HYDROPEROXIDATION OF CYCLOHEPTENONE (46S) AND CYCLOOCTENONE (46V) 196 7.4 SYNTHETIC TRANSFORMATIONS O F OPTICALLY ACTIVE PRODUCTS 198 7.4.1 ONE-POT SYNTHESIS OF ALDOL PRODUCTS 198 7.4.2 ORGANOSELENIUM-MEDIATED REDUCTIVE EPOXIDE OPENING 202 7.4.3 SYNTHESIS O F (S^^^-S-HEXYL-S-METHYL-L^- DIOXOLANE (127) 204 7.5 PREPARATION OF STARTING MATERIALS 206 7.5.1 PREPARATION OF CYCLIC OC,P-UNSATURATED KETONES 206 7.5.2 PREPARATION OF ACYCLIC A,P-UNSATURATED KETONES 216 7.6 CATALYST SYNTHESIS 232 7.6.1 SYNTHESIS OF 9-AMINO(9-DEOXY) CINCHONA ALKALOID DERIVATIVES 232 7.6.2 SYNTHESIS O F 9-E/7; QUININE (147) 238 7.6.3 SYNTHESIS O F 6 -ISOPROPOXYCINCHONIDINE (146) 240 7.6.4 SYNTHESIS O F 9-AMINO(9-DEOXY)E;?I-6 HYDROXYCINCHONIDINE (68) 242 7.6.5 SYNTHESIS O F 2-(A-AMINOBENZYL)QUINUCLIDINE (86A) 243 7.6.6 SYNTHESIS O F AMINO ACID-DERIVED DIAMINES 246 7.6.7 SYNTHESIS OF (17?,2/?)-A -JSO-PROPYL-L,2DIPHENYLETHYLENE-L,2-DIAMINE (61) 251 7.6.8 SYNTHESIS O F (5 )-3,3 -BIS(TRIPHENYLSILYL)-1,1 BINAPHTHYL-2,2 -DIOL PHOSPHATE ((S)-7B) 252 REFERENCES 254 APPENDIX 257
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author	Owens, Kay Lean, Glen Paraide, Patricia Muke, Charly
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physical	1 Online-Ressource (xxvii, 461 Seiten) Illustrationen
psigel	ZDB-2-EDA ZDB-2-EDA_2018
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publisher	Springer
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series2	History of mathematics education
spellingShingle	Owens, Kay Lean, Glen Paraide, Patricia Muke, Charly History of number evidence from Papua New Guinea and Oceania Education Mathematics History Mathematics / Study and teaching Mathematics Education History of Mathematical Sciences Ethnomathematik (DE-588)4465939-8 gnd Mathematikunterricht (DE-588)4037949-8 gnd Zahl (DE-588)4067271-2 gnd
subject_GND	(DE-588)4465939-8 (DE-588)4037949-8 (DE-588)4067271-2 (DE-588)4044257-3 (DE-588)4044569-0
title	History of number evidence from Papua New Guinea and Oceania
title_auth	History of number evidence from Papua New Guinea and Oceania
title_exact_search	History of number evidence from Papua New Guinea and Oceania
title_full	History of number evidence from Papua New Guinea and Oceania Kay Owens and Glen Lean with Patricia Paraide and Charly Muke
title_fullStr	History of number evidence from Papua New Guinea and Oceania Kay Owens and Glen Lean with Patricia Paraide and Charly Muke
title_full_unstemmed	History of number evidence from Papua New Guinea and Oceania Kay Owens and Glen Lean with Patricia Paraide and Charly Muke
title_short	History of number
title_sort	history of number evidence from papua new guinea and oceania
title_sub	evidence from Papua New Guinea and Oceania
topic	Education Mathematics History Mathematics / Study and teaching Mathematics Education History of Mathematical Sciences Ethnomathematik (DE-588)4465939-8 gnd Mathematikunterricht (DE-588)4037949-8 gnd Zahl (DE-588)4067271-2 gnd
topic_facet	Education Mathematics History Mathematics / Study and teaching Mathematics Education History of Mathematical Sciences Ethnomathematik Mathematikunterricht Zahl Ozeanien Papua-Neuguinea
url	https://doi.org/10.1007/978-3-319-45483-2 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030099963&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
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