Wort, beer, beer-based beverages: collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission
Gespeichert in:
| Weitere beteiligte Personen: | |
|---|---|
| Format: | Buch |
| Sprache: | Englisch |
| Veröffentlicht: |
Freising
Selbstverl. der MEBAK
2013
|
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025896851&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Umfang: | 603 S. Ill., graph. Darst. |
| ISBN: | 9783980581479 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV040917640 | ||
| 003 | DE-604 | ||
| 005 | 20230508 | ||
| 007 | t| | ||
| 008 | 130328s2013 xx ad|| |||| 00||| eng d | ||
| 020 | |a 9783980581479 |9 978-3-9805814-7-9 | ||
| 035 | |a (OCoLC)835714445 | ||
| 035 | |a (DE-599)BVBBV040917640 | ||
| 040 | |a DE-604 |b ger |e rakwb | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-M49 |a DE-12 |a DE-83 | ||
| 084 | |a VN 8400 |0 (DE-625)147628:253 |2 rvk | ||
| 084 | |a ZE 16000 |0 (DE-625)155779: |2 rvk | ||
| 084 | |a BRA 330f |2 stub | ||
| 084 | |a LEB 070f |2 stub | ||
| 084 | |a BRA 200f |2 stub | ||
| 084 | |a BRA 310f |2 stub | ||
| 084 | |a LEB 720f |2 stub | ||
| 245 | 1 | 0 | |a Wort, beer, beer-based beverages |b collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission |c Mitteleuropäische Brautechnische Analysenkommission ; publ. by Fritz Jacob |
| 264 | 1 | |a Freising |b Selbstverl. der MEBAK |c 2013 | |
| 300 | |a 603 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Bierwürze |0 (DE-588)4145365-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Bier |0 (DE-588)4006537-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Mischgetränk |0 (DE-588)4039532-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Lebensmittelanalyse |0 (DE-588)4167032-2 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Bierwürze |0 (DE-588)4145365-7 |D s |
| 689 | 0 | 1 | |a Bier |0 (DE-588)4006537-6 |D s |
| 689 | 0 | 2 | |a Mischgetränk |0 (DE-588)4039532-7 |D s |
| 689 | 0 | 3 | |a Lebensmittelanalyse |0 (DE-588)4167032-2 |D s |
| 689 | 0 | |C b |5 DE-604 | |
| 700 | 1 | |a Jacob, Fritz |4 edt | |
| 710 | 2 | |a Mitteleuropäische Brautechnische Analysenkommission |0 (DE-588)2098016-4 |4 isb | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025896851&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-025896851 | |
Datensatz im Suchindex
| DE-BY-TUM_call_number | 1002 BRA 200f 2013 A 1834 |
|---|---|
| DE-BY-TUM_katkey | 1921224 |
| DE-BY-TUM_location | 10 |
| DE-BY-TUM_media_number | 040050965496 |
| _version_ | 1821934764626542592 |
| adam_text | IMAGE 1
TABLE OF CONTENTS
PREFACE TO THE NEW EDITION 3
INFORMATION ABOUT THE MEBAK WEBSITE .4
CONTRIBUTORS 5
LIST OF ABBREVIATIONS 7
TABLE OF CONTENTS .9
1 MONITORING BREWHOUSE OPERATIONS 19
1.1 MONITORING BREWERY GRIST 19
1.1.1 GRIST COMPOSITION . 1 9
1.1.2 HUSK VOLUME .22
1.2 MASHING .23
1.2.1 MASHING INTENSITY .23
1.2.2 VISUAL IODINE TEST 24
1.3 TURBIDITY MEASUREMENT DURING LAUTERING 26
1.4 SPENT GRAINS .28
1.4.1 SAMPLE COLLECTION ...28
1.4.2 MOISTURE CONTENT (EBC) .29
1.4.3 SOLUBLE EXTRACT. 30
1.4.3.1 SOLUBLE EXTRACT IN WET SPENT GRAINS OBTAINED BY PRESSING (RAPID
METHOD) 30
1.4.3.2 SOLUBLE EXTRACT IN WET AND DRY SPENT GRAINS OBTAINED BY RINSING
(EBC) .31
1.4.4 AVAILABLE RESIDUAL EXTRACT. . 32
1.4.4.1 AVAILABLE RESIDUAL EXTRACT (EBC) 32
1.4.4.2 AVAILABLE RESIDUAL EXTRACT (DIASTASE) 34
1.4.5 IODINE VALUE OF BREWERY SPENT GRAINS 36
1.4.6 CALCULATION OF EXTRACT IN SPENT GRAINS AS EXTRACT IN MALT... 39
1.5 BREWHOUSE AND EXTRACT YIELD .41
1.5.1 BREWHOUSE YIELD 41
1.5.2 COLD WORT YIELD .42
1.5.3 FERMENTATION CELLAR YIELD 42
9
HTTP://D-NB.INFO/1030585032
IMAGE 2
1.6 SOLIDS 44
1.6.1 SOLIDS IN WORT (LABOR VERITAS METHOD) .44
1.6.2 SOLIDS OR TRUB MATERIAL (FIELD METHOD) 45
1.6.3 COLD TRUB .47
2 WORT AND BEER .51
2.1 SAMPLE COLLECTION . .. 51
2.2 ODOR AND FLAVOR OF WORT 52
2.3 PHOTOMETRIC IODINE TEST 53
2.4 THIOBARBITURIC ACID INDEX (TBI) 56
2.5 HIGH MOLECULAR WEIGHT 0-GLUCAN 59
2.5.1 ENZYMATIC METHOD 59
2.5.2 FLUORIMETRIC METHOD (EBC) .64
2.5.3 MODIFIED FLUORIMETRIC METHOD (HPLC) .68
2.5.4 COLORIMETRIC METHOD (EBC) .70
2.5.5 DETERMINATION OF P-GLUCAN GEI 72
2.6 NITROGENOUS SUBSTANCES 7 3
2.6.1 TOTAL NITROGEN .73
2.6.1.1 KJELDAHL METHOD ( E B C ) 7 3
2 . 6 . 1 . 2 DUMAS COMBUSTION METHOD (EBC) ...76
2 . 6 . 2 COAGULABLE NITROGEN (THERMAL COAGULATION OF PROTEIN) 7 8
2 . 6 . 3 NITROGEN FRACTIONATION .81
2 . 6 . 3 . 1 PRECIPITATION WITH MAGNESIUM SULFATE 8 1
2 . 6 . 3 . 2 PRECIPITATION WITH PHOSPHOMOLYBDIC ACID 8 3
2 . 6 . 4 LOW MOLECULAR WEIGHT NITROGENOUS SUBSTANCES 8 6
2 . 6 . 4 . 1 FREE AMINO NITROGEN (FAN) 8 6
2 . 6 . 4 . 1 . 1 NINHYDRIN METHOD (PHOTOMETRIC METHOD, EBC) 8 6
2 . 6 . 4 . 1 . 2 DETERMINATION OF AMINO ACIDS IN WORT AND BEER 8 9
2 . 6 . 4 . 1 . 3 AMINES IN WORT AND BEER .95
2 . 6 . 4 . 2 NITROSAMINES IN WORT AND BEER. 1 0 1
2 . 6 . 5 PROLAMINS IN BEER (ELISA METHOD) 1 0 6
10
IMAGE 3
2.7 CARBOHYDRATES 110
2.7.1 SUGAR SPECTRUM 110
2.7.2 FERMENTABLE CARBOHYDRATES (EBC) .113
2.7.3 TOTAL CARBOHYDRATES 117
2.7.4 DETERMINATION OF CARBOHYDRATES - ENZYMATIC METHOD 119 2.7.4.1
GLUCOSE AND FRUCTOSE 121
2.7.4.2 SUCROSE 123
2.7.4.3 MALTOSE (AND MALTOTRIOSEJ 124
2.7.4.4 STARCH 125
2.7.5 SUGAR ANALYSIS WITH HPAEC-PAD (HIGH PERFORMANCE ANION EXCHANGE
CHROMATOGRAPHY WITH PULSED AMPEROMETRIC DETECTION) 127
2.8 DEGREE OF ATTENUATION 131
2.8.1 LIMIT OF ATTENUATION IN WORT (FERMENTATION TUBE METHOD), 131 2.8.2
LIMIT OF ATTENUATION IN WORT AND BEER (REFERENCE METHOD - EBC) 134
2.8.3 LIMIT OF ATTENUATION IN WORT AND BEER
(RAPID METHOD - EBC) 136
2.8.4 ATTENUATION OF MATURING BEER AND FINISHED BEER 137
2.9 ORIGINAL GRAVITY AND ALCOHOL 139
2.9.1 DEGASSING A SAMPLE (EBC) 140
2.9.2 DENSITY MEASUREMENT 141
2.9.2.1 PYCNOMETER 141
2.9.2.2 HYDROMETER., 143
2.9.2.3 OSCILLATING U-TUBE DENSITY MEASUREMENT (EBC) .....144
2.9.3 APPARENT EXTRACT (EBC) 145
2.9.4 DISTILLATION ANALYSIS (REFERENCE METHOD - EBC) 146
2.9.5 REFRACTOMETRIC ANALYSIS. 150
2.9.6 MULTIFUNCTIONAL DEVICES 153
2.9.6.1 OSCILLATING U-TUBE AND SOUND VELOCITY MEASUREMENTS 154 2.9.6.2
OSCILLATING U-TUBE DENSITY AND ALCOHOL CONTENT MEASUREMENTS 154
2.9.6.3 OSCILLATING U-TUBE DENSITY AND NIR MEASUREMENTS 155 2.9.6.4
THERMAL ANALYSIS METHOD - FERMENTO-STAR 157
2.9.7 ALCOHOL (ETHANOL). 158
2.9.7.1 ENZYMATIC ANALYSIS (EBC) 158
2.9.7.2 ETHANOL (CHROMATOGRAPHIC) _ _ _ _ _ 160
11
IMAGE 4
161
161 162
1 6 4
. 1 6 6
1 6 7
1 6 7
168
168 1 6 9
1 7 0
1 7 0
1 7 0
. 1 7 0
. 1 7 1
184
189 1 8 9
1 9 1
194
198 1 9 8
1 9 8
. 1 9 9
201
201 2 0 3
2 0 5
2 0 7
2 0 9
NUTRITIONAL ANALYSES
ENERGY VALUE OR CALORIC VALUE MEASURING OSMOLALITY WITH AN OSMOMETER
RECOMMENDED ANALYSIS FOR HIGHLY ATTENUATED BEER (FORMERLY, ANALYSIS OF
DIETETIC BEER)
GENERAL ANALYSES DETERMINATION OF CARBOHYDRATE CONTENT BASED ON
NUTRITIONAL VALUE (TOTAL GLUCOSE) HYDROLYSIS ENZYMATIC DETERMINATION OF
GLUCOSE
FERMENTABLE EXTRACT. CALCULATION OF DEXTRIN CONTENT CALCULATION OF
CARBOHYDRATE CONTENT CALCULATION OF UTILIZABLE CARBOHYDRATES ENERGY
VALUE OR CALORIC VALUE BREAD UNITS
BIG FOUR OR BIG EIGHT DECLARATION OF NUTRITION INFORMATION FOR
BEVERAGES
DETERMINATION OF VITAMIN BI AND B 2 IN WORT AND BEER
COLOR VISUAL DETERMINATION OF COLOR BY COMPARISON SPECTROPHOTOMETRIC
COLOR (EBC)._._
PH (EBC)
HAZE FORMATION (PROTEIN STABILITY) HAZE VISUAL METHOD OPTICAL METHOD
PREDICTING CHEMICAL-PHYSICAL STABILITY (PROTEIN STABILITY) FORCED AGING
ALCOHOL CHILL HAZE TEST, CHAPON (COLD SENSITIVITY)..
FORMALDEHYDE TEST PRECIPITATION WITH AMMONIUM SULFATE ESBACH REACTION
TEST
IMAGE 5
2.15 REDUCTION POTENTIAL 211
2.15.1 SPECTROPHOTOMETRIC METHOD ... 211
2.15.2 INDICATOR TIME TEST (ITT) 213
2.15.3 ENDOGENOUS ANTIOXIDATIVE POTENTIAL (EAP VALUE) AND RADICAL
GENERATION (T VALUE) IN BEVERAGES (ESR SPECTROSCOPY) .214
2.15.4 CHARACTERISTICS OF MALT AND MALT MIXTURES DURING THE PROCESS OF
MASHING-IN (TENDENCY FOR OXIDATION): MEASUREMENT OF OXIDATION REACTIONS
WHILE MASHING-IN
THROUGH CHEMILUMINESCENCE 225
2.16 PHENOLIC COMPOUNDS . .229
2.16.1 TOTAL POLYPHENOLS (EBC) .229
2 . 1 6 . 2 ANTHOCYANOGENS, HARRIS AND RICKETTS METHOD 2 3 2
2 . 1 6 . 3 TANNOIDS . . . 2 3 4
2 . 1 6 . 4 STEAM-VOLATIIE PHENOLS . 2 3 7
2.17 BITTER SUBSTANCES .....240
2.17.1 BITTERING UNITS (EBC) . 240
2.17.2 ISO-A-ACIDS AND P-ACIDS (SPECTROPHOTOMETRY) .243
2.17.3 DETERMINATION OF HOP BITTER SUBSTANCES IN WORT AND BEER (EBC).
.245
2.17.4 DETERMINATION OF XANTHOHUMOI USING HPLC .249
2.18 FOAM 254
2.18.1 FOAM STABILITY, ROSS AND CLARK .254
2.18.2 FOAM STABILITY, NIBEM 257
2.18.3 FOAM STABILITY, LG-FOAM FESTER .262
2.18.4 FOAM STABILITY, STEINFURTH FOAM STABILITY FESTER 264
2.18.5 NIBEM CLING METER (HAFFMANS) 265
2.19 PROOF OF PASTEURIZATION 270
2.20 FILTERABILITY OF BEER 273
2.20.1 MEMBRANE FILTER TEST (ESSER) 273
2.20.2 FILTERABILITY TEST (RAIBLE) .277
2.21 FERMENTATION BY-PRODUCTS (GENERAL) .280
2.21.1 HIGHLY VOLATILE FERMENTATION BY-PRODUCTS (HEADSPACE METHOD) .280
13
IMAGE 6
2.21.2 FERMENTATION BY-PRODUCTS____ .....286
2.21.2.1 FERMENTATION BY-PRODUCTS (DISTILLATION METHOD).. ...286
2.21.2.2 FERMENTATION BY-PRODUCTS (DICHLOROMETHANE EXTRACTION) 290
2.21.3 AROMATIC ALCOHOLS AND PHENOLCARBOXYLIC ACIDS. .. ...296
2.21.3.1 AROMATIC ALCOHOLS. 296
2.21.3.2 COUMARIC ACID AND FERULIC ACID 300
2.21.3.3 4-VINYL GUAIACOL AND 4-VINYL PHENOL (HPLCJ 303
2.21.4 SHORT CHAIN FATTY ACIDS (DISTILLATION METHOD) 307
2.21.5 VICINAL DIKETONES 311
2.21.5.1 VICINAL DIKETONES (HEADSPACE METHOD) 311
2.21.5.2 VICINAL DIKETONES (EBC) 314
2.21.5.3 VICINAL DIKETONES (DISTILLATION METHOD) 319
2.21.5.4 3-HYDROXY-2-BUTANONE (ACETOIN) (HEADSPACE METHOD) 324
2.21.6 HIGHER ALCOHOLS AND ESTERS IN BEER 326
2.21.7 ORGANIC ACIDS _ ...335
2.21.7.1 ENZYMATIC DETERMINATION OF ORGANIC ACIDS 335
2.21.7.1.1 FORMIC ACID (FORMATE) 336
2.21.7.1.2 L-MALIC ACID (MALATE) 337
2.21.7.1.3 ASCORBIC ACID (ASCORBATE) ...338
2.21.7.1.4 PYRUVIC ACID (PYRUVATE) .340
2.21.7.1.5 CITRIC ACID (CITRATE).. 341
2.21.7.1.6 ACETIC ACID (ACETATE) (EBC)____ 342
2.21.7.1.7 L-LACTIC ACID (EBC)/D-LACTIC ACID (LACTATE) 344
2.21.7.1.8 OXALIC ACID (OXALATE) AND FORMIC ACID (FORMATE) ...346
2.21.7.2 ORGANIC ACIDS IN BEER AND UPSTREAM INTERMEDIARY BREWERY
PRODUCTS, NON-ALCOHOLIC BEVERAGES, WATER
UND WASTEWATER USING ION CHROMATOGRAPHY 347
2.21.8 SULFUR DIOXIDE 350
2.21.8.1 ENZYMATIC METHOD 351
2.21.8.2 DISTILLATION METHOD (EBC) ...353
2.21.8.3 DETECTION WITH CONTINUOUS FLOW RATE ANALYSIS (CFA) 356 2.21.8.4
ION CHROMATOGRAPHIC DETECTION _____360
2.22 ANIONS 364
2.22.1 CHLORIDE, SULFATE, NITRATE AND PHOSPHATE IN BEER (EBC) 364 2.22.2
BROMIDE, CHLORIDE, FLUORIDE, NITRATE, NITRITE, OXALATE, PHOSPHATE AND
SULFATE IN WATER, MALT, HOPS, WORT AND BEER .367
2.22.3 NITRATE, ENZYMATIC DETERMINATION 371
14
IMAGE 7
2.22.4 CHLORIDE 373
2.22.5 SULFATE .375
2.23 SPECIAL CHROMATOGRAPHIC METHODS 377
2.23.1 DIMETHYL SULFIDE AND ITS PRECURSOR 377
2.23.1.1 FREE DMS IN WORT AND BEER 377
2.23.1.2 DMS PRECURSORS IN WORT 380
2.23.2 DETERMINATION OF LONG-CHAIN FATTY ACIDS IN WORT AND BEER BY GAS
CHROMATOGRAPHY 381
2.23.3 HYDROXYMETHYLFURFURAL IN WORT AND BEER BY HPLC 384
2.23.4 DETERMINATION OF AGING INDICATORS IN BEER 386
2.23.5 DETERMINATION OF STEAM-VOLATILE AROMA COMPOUNDS IN WORT 395
2.23.6 DETERMINATION OF STEAM-VOIATILE AROMA COMPOUNDS IN BEER 405
2.24 MINERALS 415
2.24.1 SODIUM (EBC) 416
2.24.2 POTASSIUM (EBC) 419
2.24.3 MAGNESIUM (EBC) 422
2.24.4 CALCIUM (EBC) .424
2.24.5 MANGANESE 427
2.24.6 IRON .429
2.24.6.1 IRON (EBC) .430
2.24.6.2 IRON (SPECTROPHOTOMETRIC METHOD - EBC) 432
2.24.7 NICKEL 435
2.24.7.1 NICKEL (GRAPHITE FURNACE AAS). .435
2.24.7.2 NICKEL (EBC) .438
2.24.8 COPPER 440
2.24.8.1 COPPER (EBC) 440
2.24.8.2 COPPER (ZDBT - EBC) .443
2.24.8.3 COPPER (CUPRETHOL RAPID METHOD - EBC) 446
2.24.9 ZINC (EBC) .447
2.24.10 ALUMINUM .450
2.24.11 TIN * 452
2.24.12 MULTI-ELEMENT DETERMINATION USING INDUCTIVELY COUPLED PLASMA
EMISSION SPECTROMETRY (ICP-OES) IN BEER AND WORT .454
15
IMAGE 8
2.25 VISCOSITY (EBC) IN CAST-OUT WORT AND BEER 459
2.25.1 HOPPLER FALLING BALL VISCOMETER 4 6 1
2.25.2 ROTATIONAL VISCOMETER 464
2.25.3 CAPILLARY VISCOMETER 464
2.26 CARBON DIOXIDE .469
2.26.1 MANOMETRIC METHOD 4 6 9
2 . 2 6 . 1 . 1 MEASURING DEVICE FOR CARBON DIOXIDE
IN TANKS OR LINES, HAFFMANS 4 7 0
2 . 2 6 . 1 . 2 RAPID DETERMINATION OF CARBON DIOXIDE IN BOTTLED BEER,
STADLER AND ZELLER 4 7 1
2 . 2 6 . 1 . 3 C 0 2 MEASURING DEVICE, STEINFURTH SYSTEM 4 7 2
2 . 2 6 . 1 . 4 CARBON DIOXIDE IN BOTTLED BEER, ZAHM AND NAGEL 4 7 4
2 . 2 6 . 1 . 5 CARBON DIOXIDE IN PACKAGED BEVERAGES
OR AT-LINE WITH CARBOQC, ANTON PAAR 4 7 5
2 . 2 6 . 2 CARBON DIOXIDE IN BEER IN A BOTTLE OR TANK,
BLOM AND LUND (TITRIMETRIC METHOD).... 4 7 7
2 . 2 6 . 3 ORBISPHERE C 0 2 ANALYZER (THERMAL CONDUCTIVITY) 4 8 1
2 . 2 6 . 4 C 0 2 DETERMINATION USING A TOC ANALYZER .482
2.27 NITROGEN 485
2.28 OXYGEN AND AIR 486
2.28.1 DISSOLVED OXYGEN .487
2.28.1.1 ELECTROMETRIC METHODS .487
2.28.1.1.1 OXYGEN DETERMINATION WITH CLARK ELECTRODES (MEASUREMENT OF
ELECTRICAL CURRENT) .487
2.28.1.1.2 OXYGEN DETERMINATION, TODT AND TESKE (DIGOX ANALYZER) 490
2.28.1.1.3 0 2 MEASUREMENT DEVICE ORBISPHERE 3650 (HACH LANGE) .494
2.28.1.2 OXYGEN MEASUREMENT WITH OPTOCHEMICAL SENSORS 495 2.28.1.2.1 C0
2 /0 2 METER, MODEL C-DGM AND 0 2 METER, MODEL O-DGM (HAFFMANS) 497
2.28.1.2.2 0 2 MEASURING DEVICE OXYQC (ANTON PAAR) 498
2.28.1.2.3 0 2 MEASUREMENT DEVICE 3110 (HACH LANGE) 500
2.28.2 AIR IN HEADSPACE AND TOTAL AIR IN BOTTLES AND CANS OXYGEN IN
HEADSPACE 501
2.28.2.1 UNDERWATER FUNNEL METHOD .501
2.28.2.2 UNDERWATER FUNNEL METHOD WITH AUXILIARY BURETTE 504
16
IMAGE 9
2 . 2 8 . 2 . 3 TOTAL AIR IN BOTTLES AND CANS, ZAHM AND NAGEL ____ 5 0 6
2.28.2.4 GASES IN PACKAGING _ _ _ _ _ . 508
2.28.2.4.1 INPACK TP0/C0 2 METER, TYPE C-TPO (HAFFMANS) 508 2.28.2.4.2
ORBISPERE 6110 PACKAGE ANALYZER (HACH LANGE)____ ___.511 2.28.2.4.3
PACKAGE ANALYZER MODEL 76060 (MECSENS)__ 513
2.28.3 TOTAL OXYGEN IN BOTTLED AND CANNED BEER . 515
3 NON-ALCOHOLIC BEVERAGES AND BEER-BASED BEVERAGES 518
3.1 BEER-BASED BEVERAGES _ _ _ _ 518
3.1.1 ORIGINAL GRAVITY AND ALCOHOL _____ _____ 5 1 8
3 . 1 . 2 COLOR ____ ______ _____ ______ ____ 5 1 8
3 . 1 . 3 PH _____ ______ ____ 5 1 8
3 . 1 . 4 TURBIDITY ____ ____ . . . 5 1 9
3 . 1 . 5 C 0 2 CONTENT ____ _____ ____ 5 1 9
3.2 NON-ALCOHOLIC SOFT DRINKS AND MALT BEVERAGES 520
3.2.1 DRY MATTER (EXTRACT) - REFRACTOMETRIC DETERMINATION .520
3 . 2 . 2 CARBOHYDRATES ____ _____ ____ _____ _ _ _ 5 2 3
3.2.2.1 SUGARS ____ _ _ _ ____ .....523
3 . 2 . 2 . 1 . 1 GLUCOSE, FRUCTOSE AND SUCROSE (ENZYMATIC METHOD) .523
3 . 2 . 2 . 1 . 2 GLUCOSE, FRUCTOSE AND SUCROSE (HPLC) 5 2 3
3 . 2 . 2 . 1 . 3 MALTOSE (ENZYMATIC METHOD) _____ _____ ____ . 5 2 3
3 . 2 . 2 . 2 SUGAR ALCOHOLS _ _ _ _ _ _____ .....524
3 . 2 . 2 . 2 . 1 D-SORBITOL (ENZYMATIC METHODJ___ ____ ____ 5 2 4
3 . 2 . 2 . 2 . 2 SORBITOL (ION CHROMATOGRAPHY METHOD) ____ ____ 5 2 6
3 . 2 . 3 TITRATABLE ACID ____ 5 2 8
3 . 2 . 4 VOLATILE ACIDS _____ ____ ____ . 5 3 0
3 . 2 . 5 ORGANIC ACIDS ____ ____ ____ ____ 5 3 4
3.2.5.1 ION CHROMATOGRAPHY ANALYSIS_____ _____ ____ 5 3 4
3 . 2 . 5 . 2 ENZYMATIC ANALYSIS ____ _____ .....535
3.2.5.2.1 L-MALIC ACID _____ ____ 5 3 5
3 . 2 . 5 . 2 . 2 CITRIC ACID ____ ____ _____ _____ ... 5 3 5
3 . 2 . 5 . 2 . 3 DL-LACTIC ACID.... ______ 5 3 5
3 . 2 . 5 . 2 . 4 TOTAL D-LSOCITRATE ACCORDING TO WALLRAUCH 5 3 6
3 . 2 . 5 . 2 . 5 D-GLUCONATE ____ _____ _____ _____ _____ .....538
3 . 2 . 6 DETERMINATION OF FRUIT JUICE CONTENT _____540
3 . 2 . 7 VITAMINS ______ ______ _____ ____ . . . 5 4 2
3.2.7.1 ASCORBIC ACID ____ _____ ____ _____ . . . 5 4 3
3 . 2 . 7 . 1 . 1 ASCORBIC ACID (HPLC) ____ _____ _____ ____ . 5 4 3
17
IMAGE 10
3.2.7.1.2 ASCORBIC ACID (ENZYMATIC METHOD) _ _ _ _ _ 545
3.2.7.1.3 ASCORBIC ACID (TITRIMETRIC METHOD), TANNER AND BRUNNER 545
3.2.7.2 CAROTENOIDS____ .547
3.2.7.2.1 TOTAL CAROTENOIDS (PHOTOMETRIC METHOD)_____ 547
3.2.7.2.2 DETERMINATION OF TOTAL CAROTENE AND HPLC ANALYSIS (WESERGOLD
RAPID METHOD WITH CARREZ EXTRACTION) 550 3.2.7.3 NIACIN (HPLC) _ _ _ _ _
______ _ .555
3.2.7.4 VITAMIN BI (MICROBIOLOGICAL ASSAY ON MICROTITER PLATES) 557
3.2.7.5 VITAMIN B2 (RIBOFLAVIN) (HPLC)___._ 558
3.2.7.6 VITAMIN B 6 (PYRIDOXINE) (HPLC) 560
3.2.7.7 VITAMIN E (HPLC).___ .562
3.2.7.8 PANTOTHENIC ACID
(MICROBIOLOGICAL ASSAY ON MICROTITER PLATES). 564
3.2.7.9 FOLIC ACID
(MICROBIOLOGICAL ASSAY ON MICROTITER PLATES). 565
3.2.8 TAURINE (IC METHOD) 566
3.2.9 GLUCURONOLACTONE (IC METHOD) . 568
3.2.10 CAFFEINE AND THEOBROMINE (HPLC) .571
3.2.11 QUININE (HPLC)... 574
3.2.12 SWEETENERS 576
3.2.12.1 ASPARTAME, ACESULFAME AND SACCHARIN (HPLC) .. .576 3.2.12.2
NEOHESPERIDIN DIHYDROCHALCONE (HPLC) .....579
3.2.12.3 CYCLAMATE (PHOTOMETRIC METHOD) ... 581
3.2.13 HYDROXYMETHYLFURFURAL (HMF) 583
3.2.13.1 HYDROXYMETHYLFURFURAL (HPLC) . .584
3.2.13.2 HYDROXYMETHYLFURFURAL (PHOTOMETRIC METHOD) 586
3.2.14 PRESERVATIVES _ _ 588
3.2.14.1 BENZOIC ACID AND SORBIC ACID (HPLC) 588
3.2.14.2 TOTAL SULFUROUS ACID (DISTILLATION METHOD) .592
3.2.15 DIMETHYL DICARBONATE (DMDC) - DOSAGE DETERMINATION 593
THE FUNDAMENTALS OF STATISTICS MEBAK.ORG
INDEX _ _ _ _ _ 594
LIST OF ADVERTISERS 602
18
|
| any_adam_object | 1 |
| author2 | Jacob, Fritz |
| author2_role | edt |
| author2_variant | f j fj |
| author_facet | Jacob, Fritz |
| building | Verbundindex |
| bvnumber | BV040917640 |
| classification_rvk | VN 8400 ZE 16000 |
| classification_tum | BRA 330f LEB 070f BRA 200f BRA 310f LEB 720f |
| ctrlnum | (OCoLC)835714445 (DE-599)BVBBV040917640 |
| discipline | Chemie / Pharmazie Biologie Agrar-/Forst-/Ernährungs-/Haushaltswissenschaft / Gartenbau |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01948nam a2200469 c 4500</leader><controlfield tag="001">BV040917640</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20230508 </controlfield><controlfield tag="007">t|</controlfield><controlfield tag="008">130328s2013 xx ad|| |||| 00||| eng d</controlfield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783980581479</subfield><subfield code="9">978-3-9805814-7-9</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)835714445</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV040917640</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-M49</subfield><subfield code="a">DE-12</subfield><subfield code="a">DE-83</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VN 8400</subfield><subfield code="0">(DE-625)147628:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">ZE 16000</subfield><subfield code="0">(DE-625)155779:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">BRA 330f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">LEB 070f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">BRA 200f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">BRA 310f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">LEB 720f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Wort, beer, beer-based beverages</subfield><subfield code="b">collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission</subfield><subfield code="c">Mitteleuropäische Brautechnische Analysenkommission ; publ. by Fritz Jacob</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Freising</subfield><subfield code="b">Selbstverl. der MEBAK</subfield><subfield code="c">2013</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">603 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Bierwürze</subfield><subfield code="0">(DE-588)4145365-7</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Bier</subfield><subfield code="0">(DE-588)4006537-6</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Mischgetränk</subfield><subfield code="0">(DE-588)4039532-7</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Lebensmittelanalyse</subfield><subfield code="0">(DE-588)4167032-2</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Bierwürze</subfield><subfield code="0">(DE-588)4145365-7</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Bier</subfield><subfield code="0">(DE-588)4006537-6</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="2"><subfield code="a">Mischgetränk</subfield><subfield code="0">(DE-588)4039532-7</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="3"><subfield code="a">Lebensmittelanalyse</subfield><subfield code="0">(DE-588)4167032-2</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="C">b</subfield><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Jacob, Fritz</subfield><subfield code="4">edt</subfield></datafield><datafield tag="710" ind1="2" ind2=" "><subfield code="a">Mitteleuropäische Brautechnische Analysenkommission</subfield><subfield code="0">(DE-588)2098016-4</subfield><subfield code="4">isb</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025896851&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-025896851</subfield></datafield></record></collection> |
| id | DE-604.BV040917640 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T16:27:08Z |
| institution | BVB |
| institution_GND | (DE-588)2098016-4 |
| isbn | 9783980581479 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025896851 |
| oclc_num | 835714445 |
| open_access_boolean | |
| owner | DE-M49 DE-BY-TUM DE-12 DE-83 |
| owner_facet | DE-M49 DE-BY-TUM DE-12 DE-83 |
| physical | 603 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Selbstverl. der MEBAK |
| record_format | marc |
| spellingShingle | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission Bierwürze (DE-588)4145365-7 gnd Bier (DE-588)4006537-6 gnd Mischgetränk (DE-588)4039532-7 gnd Lebensmittelanalyse (DE-588)4167032-2 gnd |
| subject_GND | (DE-588)4145365-7 (DE-588)4006537-6 (DE-588)4039532-7 (DE-588)4167032-2 |
| title | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission |
| title_auth | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission |
| title_exact_search | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission |
| title_full | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission Mitteleuropäische Brautechnische Analysenkommission ; publ. by Fritz Jacob |
| title_fullStr | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission Mitteleuropäische Brautechnische Analysenkommission ; publ. by Fritz Jacob |
| title_full_unstemmed | Wort, beer, beer-based beverages collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission Mitteleuropäische Brautechnische Analysenkommission ; publ. by Fritz Jacob |
| title_short | Wort, beer, beer-based beverages |
| title_sort | wort beer beer based beverages collection of brewing analysis methods of the mitteleuropaische brautechnische analysenkommission |
| title_sub | collection of brewing analysis methods of the Mitteleuropäische Brautechnische Analysenkommission |
| topic | Bierwürze (DE-588)4145365-7 gnd Bier (DE-588)4006537-6 gnd Mischgetränk (DE-588)4039532-7 gnd Lebensmittelanalyse (DE-588)4167032-2 gnd |
| topic_facet | Bierwürze Bier Mischgetränk Lebensmittelanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025896851&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT jacobfritz wortbeerbeerbasedbeveragescollectionofbrewinganalysismethodsofthemitteleuropaischebrautechnischeanalysenkommission AT mitteleuropaischebrautechnischeanalysenkommission wortbeerbeerbasedbeveragescollectionofbrewinganalysismethodsofthemitteleuropaischebrautechnischeanalysenkommission |
Inhaltsverzeichnis
Paper/Kapitel scannen lassen
Paper/Kapitel scannen lassen
Teilbibliothek Weihenstephan
| Signatur: |
1002 BRA 200f 2013 A 1834
Lageplan |
|---|---|
| Exemplar 1 | Ausleihbar Am Standort |