Microreactors: new technology for modern chemistry
Gespeichert in:
| Beteiligte Personen: | , , |
|---|---|
| Format: | Buch |
| Sprache: | Englisch |
| Veröffentlicht: |
Weinheim [u.a.]
Wiley-VCH
2000
|
| Ausgabe: | 1. ed. |
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008974887&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Umfang: | XI, 288 S. Ill., graph. Darst. |
| ISBN: | 3527295909 |
Internformat
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Datensatz im Suchindex
| DE-BY-TUM_call_number | 0702 CIT 350f 2000 A 70282 |
|---|---|
| DE-BY-TUM_katkey | 1135787 |
| DE-BY-TUM_location | 07 |
| DE-BY-TUM_media_number | 040070240276 |
| _version_ | 1821932113651302401 |
| adam_text | Titel: Microreactors
Autor: Ehrfeld, Wolfgang
Jahr: 2000
Contents
1 State of the Art of Microreaction Technology .............................................1
1.1 Definition..........................................................................................................I
1.1.1 Microsystems Termed Microreactor.................................................................1
1.1.2 Structural Hierarchy of Microreactors..............................................................1
1.1.3 Functional Classification of Microreactors......................................................4
1.1.4 Dividing Line Between Analysis and Reaction Systems..................................4
1.2 Fundamental Advantages of Microreactors......................................................5
1.2.1 Fundamental Advantages of Miniaturized Analysis Systems...........................5
1.2.2 Fundamental Advantages of Nano-Scale Reactors...........................................5
1.2.3 Advantages of Microreactors Due to Decrease of Physical Size......................6
1.2.4 Advantages of Microreactors Due to Increase of Number of Units.................8
1.3 Potential Benefits of Microreactors Regarding Applications.........................10
1.4 References......................................................................................................12
2 Modern Microfabrication Techniques for Microreactors ........................15
2.1 Microfabrication Techniques Suitable for Microreactor Realization.............15
2.2 Evaluation of Suitability of a Technique........................................................16
2.3 Anisotropic Wet Etching of Silicon................................................................17
2.4 Dry Etching of Silicon....................................................................................19
2.5 LIGA Process.................................................................................................20
2.6 Injection Molding...........................................................................................21
2.7 Wet Chemical Etching of Glass......................................................................22
2.8 Advanced Mechanical Techniques.................................................................23
2.8.1 Surface Cutting with Diamond Tools.............................................................23
2.8.2 Milling, Turning and Drilling.........................................................................23
2.8.3 Punching.........................................................................................................24
2.8.4 Embossing......................................................................................................24
2.9 Isotropic Wet Chemical Etching of Metal Foils.............................................25
2.10 Electro Discharge Machining (EDM) of Conductive Materials.....................26
2.10.1 Wire-Cut Erosion and Die Sinking.................................................................27
2.10.2 p-EDM Drilling..............................................................................................29
2.11 Laser Micromachining....................................................................................29
2.12 Interconnection Techniques............................................................................30
2.12.1 Microlamination of Thin Metal Sheets...........................................................30
2.13 Functional Coatings........................................................................................33
2.13.1 Functional Coatings for Corrosion Prevention...............................................33
2.13.2 Functional Coatings for Fouling Prevention...................................................34
2.14 References......................................................................................................35
Contents
3 Micromixcrs ..................................................................................
3.1 Mixing Principles and Classes of Macroscopic Mixing Equipment
3.2 Mixing Principles and Classes ot Miniaturized Mixers..................
3 A Contacting of Two Substreams, e.g. in a Mixing Tee Configuration..............49
3.4.1 Mixing Tee-Type Configuration..................................................................... *9
3.4.2 Double Mixing Tee-Type Configuration ........................................................5(J
3.5 Collision of High-Energy Substreams for Spraying/Atomizing.....................52
3.5.1 Collision of Three Substreams in a Microjet Reactor....................................52
3.6 Injection of Many Small Substreams of One Component into a
Main Stream of Another Component..............................................................53
3.6.1 Injection of Multiple Microjets ......................................................................53
3.7 Manifold Splitting and Recombination of a Stream Consisting of
Two Fluid Lamellae of Both Components......................................................55
3.7.1 Multiple Flow Splitting and Recombination Combined with Channel
Reshaping.......................................................................................................55
3.7.2 Multiple Flow Splitting and Recombination Using Fork-Like Elements.......58
3.7.3 Multiple Flow Splitting and Recombination Using a Separation Plate..........60
3.7.4 Multiple Flow Splitting and Recombination Using a Ramp-Like
Channel Architecture......................................................................................62
3.8 Injection of Many Substreams of Both Components......................................64
3.8.1 Multilamination of Fluid Layers in an Interdigital Channel
Configuration..................................................................................................64
3.8.2 Vertical Multilamination of Fluid Layers Using a V-typc Nozzle Array........73
3.8.3 Multilamination Using a Stack of Platelets with Microchannels...................75
3.8.4 Multilamination Using a Stack of Platelets with Star-Shaped Openings.......79
3.9 Decrease of Diffusion Path Perpendicular to the Flow Direction by
Increase of Flow Velocity...............................................................................80
3.9.1 Decrease of Layer Thickness by Hydrodynamic Focusing............................80
3.10 Externally Forced Mass Transport, e.g. by Stirring, Ultrasonic Wave,
Electrical and Thermal Energy.......................................................................83
3.10.1 Dynamic Micromixer Using Magnetic Beads................................................83
3.11 References......................................................................................................83
4 Micro Heat Exchangers ...............................................................................87
4.1 Micro Heat Exchangers with Wide and Flat Channels...................................89
4.1.1 Cross-Flow Heat Exchange in Stacked Plate Devices....................................89
4.1.2 Cross-Flow Heat Exchange Based on Cross-Mixing .....................................92
4.1.3 Counter-Flow Heat Exchange in Stacked Plate Devices................................94
4.1.4 Electrically Heated Slacked Plate Devices.....................................................97
4.2 Micro Heat Exchangers with Narrow and Deep Channels.............................99
4.2.1 Heat Exchanger with One-Sided Structured Channels...................................99
4.2.2 Heat Exchanger with Double-Sided Structured Channels............................ 100
VIII
Contents
4.3 Micro Heat Exchangers with Breakthrough Channels.................................102
4.4 Axial Heat Conduction.................................................................................104
4.4.1 Numerical Calculations of the Influence of Material Choice on
Heat Transfer Efficiency...............................................................................104
4.4.2 The Use of Thermal Blocking Structures.....................................................105
4.5 Permanent Generation of Entrance Flow by Fins.........................................106
4.6 Generation of a Periodic Flow Profile by Sine-Wave Microchannels..........107
4.7 Microtechnology-Based Chemical Heat Pumps...........................................108
4.8 Performance Characterization of Micro Heat Exchangers...........................109
4.8.1 Temperature Profiles of Micro Heat Exchangers Yielded by
Thermograms of Infrared Cameras...............................................................110
4.9 References....................................................................................................112
5 Microseparation Systems and Specific Analytical Modules for
Microreactors .............................................................................................115
5.1 Microextractors............................................................................................115
5.1.1 Partially Overlapping Channels....................................................................115
5.1.2 Wedge-Shaped Flow Contactor....................................................................119
5.1.3 Contactor Microchannels Separated by a Micromachined Membrane.........122
5.1.4 Contactor Microchannels Separated by Sieve-Like Walls............................126
5.1.5 Micromixer-Settler Systems.......................................................................126
5.2 Microfilters...................................................................................................130
5.2.1 Isoporous-Sieve Microfilters........................................................................131
5.2.2 Cross-Flow Microfilters................................................................................131
5.3 Gas Purification Microsystems.....................................................................133
5.4 Gas Separation Microdevices.......................................................................134
5.5 Specific Analytical Modules for Microreactors............................................136
5.5.1 Analytical Modules for In-Line IR Spectroscopy........................................136
5.5.2 Analytical Module for Fast Gas Chromatography........................................136
5.6 References....................................................................................................140
6 Microsystems for Liquid Phase Reactions...............................................143
6.1 Types of Liquid Phase Microreactors...........................................................144
6.2 Liquid/Liquid Synthesis of a Vitamin Precursor in a Combined Mixer
and Heat Exchanger Device..........................................................................144
6.3 Aery late Polymerization in Micromixers.....................................................151
6.4 Ketone Reduction Using a Grignard Reagent in Micromixers.....................154
6.5 Laboratory-Scale Organic Chemistry in Micromixer/Tube Reactors...........158
6.6 Dushman Reaction Using Hydrodynamic Focusing Micromixers and
High-Aspect Ratio Heat Exchangers............................................................162
6.7 Synthesis of Microcrystallites in a Microtechnology-Based Continuous
Segmented-Flow Tubular Reactor................................................................164
6.8 Electrochemical Microreactors.....................................................................166
IX
Contents
6.8.1 Synthesis of 4-Methoxybenzaldehyde in a Plate-to-Plate Electrode ^ ^
Configuration.........................................................;......................................
6.8.2 Scouting Potentiodynamic Operation of Closed Microcells........................
6.9 References....................................................................................................
171
7 Microsystems for Gas Phase Reactions ...................................................
7.1 Catalyst Supply for Microreactors................................................................ J*
7.2 Types of Gas Phase Microreactors ...............................................................175
7.3 MicroChannel Catalyst Structures.................................................................177
7.3.1 Flow Distribution in MicroChannel Catalyst Reactors.................................I77
7.3.2 Partial Oxidation of Propene to Acrolein .....................................................178
7.3.3 Selective Partial Hydrogenation of a Cyclic Triene......................................180
7.3.4 H2/02 Reaction.............................................................................................
7.3.5 Selective Partial Hydrogenation of Benzene................................................186
7.3.6 Selective Oxidation of 1-Butene to Maleic Anhydride.................................187
7.3.7 Selective Oxidation of Ethylene to Ethylene Oxide.....................................I87
7.3.8 Reactions Utilizing Periodic Operation........................................................I88
7.4 Microsystems with Integrated Catalyst Structures and Heat
Exchanger.....................................................................................................193
7.4.1 Oxidative Dehydrogenation of Alcohols......................................................193
7.4.2 Synthesis of Methyl Isocyanate and Various Other Hazardous Gases..........197
7.4.3 H2/02 Reaction in the Explosion Regime.....................................................200
7.5 Microsystems with Integrated Catalyst Structures and Mixer......................203
7.5.1 Synthesis of Ethylene Oxide ........................................................................203
7.6 Microsystems with Integrated Catalyst Structures, Heat Exchanger and
Sensors........................................................................................ ................209
7.6.1 Oxidation of Ammonia.................................................................................209
7.6.2 H2/02 Reaction.............................................................................................214
7.7 Microsystems with Integrated Mixer, Heat Exchanger, Catalyst
Structures and Sensors..................................................................................217
7.7.1 HCN Synthesis via the Andrussov Process..................................................217
7.8 References ....................................................................................................224
8 Gas/Liquid Microreactors .........................................................................229
8.1 Gas/Liquid Contacting Principles and Classes of Miniaturized
Contacting Equipment..................................................................................229
8.2 Contacting of Two Gas and Liquid Substreams in a Mixing Tee
Configuration...............................................................................................232
8.2.1 Injection of One Gas and Liquid Substream ................................................232
8.2.2 Injection of Many Gas and Liquid Substreams into One Common
Channel................................................................................................................933
8.2.3 Injection of Many Gas and Liquid Substreams into One Packed
Channel..................................................................................................................235
X
Contents
8.2.4 Injection of Many Gas Substreams into One Liquid Channel with
Catalytic Walls..............................................................................................237
8.2.5 Injection of Many Gas and Liquid Substreams into Multiple Channels......239
8.3 Generation of Thin Films in a Falling Film Microreactor............................244
8.4 References....................................................................................................255
9 Microsystems for Energy Generation ......................................................257
9.1 Microdevices for Vaporization of Liquid Fuels............................................257
9.2 Microdevices for Conversion of Gaseous Fuels to Syngas by Means
of Partial Oxidations.....................................................................................260
9.2.1 Hydrogen Generation by Partial Oxidations................................................260
9.2.2 Partial Oxidation of Methane in a Stacked Stainless Steel Sheet System .... 261
9.2.3 Partial Oxidation of Methane in a MicroChannel Reactor............................263
9.3 Microdevices for Conversion of Gaseous Fuels to Syngas by Means
of Steam Reforming.....................................................................................265
9.3.1 Steam Reforming of Methanol in Microstructured Platelets........................265
9.4 References....................................................................................................268
10 Microsystems for Catalyst and Material Screening ...............................271
10.1 Parallel Screening of Heterogeneous Catalysts in a MicroChannel
Reactor..........................................................................................................271
10.2 Parallel Screening of Heterogeneous Catalysts in Conventional
Mini-Scale Reactors.....................................................................................274
10.3 References....................................................................................................276
11 Methodology for Distributed Production ................................................277
11.1 The Miniplant Concept.................................................................................277
11.1.1 Miniplant Concept for HCN Manufacture....................................................278
11.1.2 The Disposable Batch Miniplant..................................................................279
11.2 Paradigm Change in Large-Scale Reactor Design Towards Operability
and Environmental Aspects Using Miniplants.............................................280
11.3 References....................................................................................................283
Index ......................................................................................................................285
XI
|
| any_adam_object | 1 |
| author | Ehrfeld, Wolfgang 1938- Hessel, Volker 1964- Löwe, Holger |
| author_GND | (DE-588)172060230 (DE-588)128736267 |
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| discipline | Chemie / Pharmazie |
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| id | DE-604.BV013173148 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T10:42:26Z |
| institution | BVB |
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| language | English |
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| physical | XI, 288 S. Ill., graph. Darst. |
| publishDate | 2000 |
| publishDateSearch | 2000 |
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| publisher | Wiley-VCH |
| record_format | marc |
| spellingShingle | Ehrfeld, Wolfgang 1938- Hessel, Volker 1964- Löwe, Holger Microreactors new technology for modern chemistry Microréacteurs chimiques Química industrial larpcal Reatores químicos larpcal Microreactors Chemischer Reaktor (DE-588)4121085-2 gnd Mikrosystemtechnik (DE-588)4221617-5 gnd Miniaturisierung (DE-588)4406753-7 gnd |
| subject_GND | (DE-588)4121085-2 (DE-588)4221617-5 (DE-588)4406753-7 |
| title | Microreactors new technology for modern chemistry |
| title_auth | Microreactors new technology for modern chemistry |
| title_exact_search | Microreactors new technology for modern chemistry |
| title_full | Microreactors new technology for modern chemistry Wolfgang Ehrfeld ; Volker Hessel ; Holger Löwe |
| title_fullStr | Microreactors new technology for modern chemistry Wolfgang Ehrfeld ; Volker Hessel ; Holger Löwe |
| title_full_unstemmed | Microreactors new technology for modern chemistry Wolfgang Ehrfeld ; Volker Hessel ; Holger Löwe |
| title_short | Microreactors |
| title_sort | microreactors new technology for modern chemistry |
| title_sub | new technology for modern chemistry |
| topic | Microréacteurs chimiques Química industrial larpcal Reatores químicos larpcal Microreactors Chemischer Reaktor (DE-588)4121085-2 gnd Mikrosystemtechnik (DE-588)4221617-5 gnd Miniaturisierung (DE-588)4406753-7 gnd |
| topic_facet | Microréacteurs chimiques Química industrial Reatores químicos Microreactors Chemischer Reaktor Mikrosystemtechnik Miniaturisierung Mikroreaktor |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008974887&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ehrfeldwolfgang microreactorsnewtechnologyformodernchemistry AT hesselvolker microreactorsnewtechnologyformodernchemistry AT loweholger microreactorsnewtechnologyformodernchemistry |
Inhaltsverzeichnis
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Paper/Kapitel scannen lassen
Teilbibliothek Maschinenwesen
| Signatur: |
0702 CIT 350f 2000 A 70282
Lageplan |
|---|---|
| Exemplar 1 | Ausleihbar Am Standort |