Chromatographic retention indices: an aid to identification of organic compounds
Gespeichert in:
| Beteiligte Personen: | , |
|---|---|
| Format: | Buch |
| Sprache: | Englisch Tschechisch |
| Veröffentlicht: |
New York u.a.
Horwood
1992
|
| Ausgabe: | 1. publ. |
| Schriftenreihe: | Ellis Horwood series in analytical chemistry
|
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005234953&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Umfang: | 285 S. graph. Darst. |
| ISBN: | 0137723288 |
Internformat
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Datensatz im Suchindex
| _version_ | 1819246762349559808 |
|---|---|
| adam_text | CHROMATOGRAPHIC
RETENTION INDICES
AN AID TO IDENTIFICATION
OF ORGANIC COMPOUNDS
VfiRA R CAKOVA and LADISLAV FELTL,
Department of Analytical Chemistry, Charles University, Prague
Translator:
KAREL STULfK
Translation Editor:
Dr MARY MASSON,
Department of Chemistry, University of Aberdeen
ELLIS HORWOOD
NEW YORK LONDON TORONTO SYDNEY TOKYO SINGAPORE
Table of contents
Preface 5
Introduction 11
1 Ways of expressing retention data IS
1 1 Absolute retention data 15
1 2 Relative retention data 18
121 Relative retention 18
122 The retention index 19
123 Other retention systems in gas chromatography 21
124 Retention indices in liquid chromatography 24
125 Retention indices in supercritical fluid chromatography 29
126 Retention indices for mixed stationary phases in gas chromato-
graphy 30
1 3 Precision and accuracy of the retention indices 33
131 Methods of measurement and calculation of the dead time and
the adjusted retention times 34
132 Adsorption phenomena 44
133 Other sources of errors 52
1 4 Sadtler standard retention index system 57
References 58
2 Temperature dependence of retention indices 64
2 1 Thermodynamic background 64
2 2 Relationship between d / /d T and the structure of the analytes 68
2 3 Retention indices in Programmed-Temperature Gas Chromatography
(PTGC) 71
References 77
8 Table of contents
3 Relationship between retention indices and the structures of analytes 80
3 1 Relationship between the retention index and the boiling temperature
of the substance 81
3 2 The dependence of the retention index on the number of carbon atoms
in the molecule (the 5/CH2 increments) 83
3 3 The effect of characteristic groups on retention indices 87
331 The H increment 87
332 The A/ increments 88
3 4 Correlation of retention indices with other properties of analytes 90
341 Correlation between the retention index and the physico-chemi-
cal properties of the solute 90
342 Correlation between the retention index and the topological
properties of the solute 93
3 5 Multiparametric correlations of retention indices 96
3 6 The use of relationships between retention indices and structure for
indentification of substances 98
References 98
4 Methods for calculation of retention indices 102
References 110
5 The use of retention indices for characterization of stationary phases 113
References 124
6 Retention indices on selected stationary phases 126
6 1 The relationship between retention indices and resolution 126
6 2 Tables of retention indices 127
Tables 6 1 Retention indices of alkanes on squalane 129
Tables 6 2 Retention indices of alkenes and alkynes on squalane 134
Tables 6 3 Retention indices of aromatic hydrocarbons on squalane 146
Tables 6 4 Retention indices of alicyclic hydrocarbons on squalane 150
Tables 6 5 Retention indices of oxygen-containing compounds on
squalane 166
Tables 6 6 Retention indices of halogenated compounds on squalane 172
Tables 6 7 Retention indices of sulphur-containing compounds on
squalane 175
Tables 6 8 Retention indices of alkanes on Apiezon L 176
Tables 6 9 Retention indices of alkenes and alkynes on Apiezon L 182
Tables 6 10 Retention indices of alicyclic hydrocarbons and adamantanes
on Apiezon L 190
Tables 6 11 Retention indices of aromatic hydrocarbons on Apiezon L 197
Tables 6 12 Retention indices of halogenated compounds on Apiezon L 200
Table of contents 9
Tables 6 13 Retention indices of oxygen-containing compounds on
Apiezon L 205
Tables 6 14 Retention indices of nitrogen-containing compounds on
Apiezon L 210
Tables 6 15 Retention indices of sulphur-containing compounds on
Apiezon L 217
Tables 6 16 Retention indices of terpenes and silanes on Apiezon L 221
Tables 6 17 Retention indices of aliphatic hydrocarbons on SE-30 224
Tables 6 18 Retention indices of aromatic hydrocarbons, including deriva-
tives (X, O, N) on SE-30 227
Tables 6 19 Retention indices of oxygen- and sulphur-containing com-
pounds on SE-30 230
Tables 6 20 Retention indices of aliphatic hydrocarbons on
Carbowax 20 M 238
Tables 6 21 Retention indices of aromatic hydrocarbons on
Carbowax 20 M 241
Tables 6 22 Retention indices of oxygen-, nitrogen- and sulphur-contain-
ing compounds on Carbowax 20 M 245
Tables 6 23 Retention indices of various organic compounds on OV-1 251
Tables 6 24 Retention indices of various organic compounds on OV-17 254
Tables 6 25 Retention indices of aliphatic and cyclic compounds on
OV-101 263
Tables 6 26 Retention indices of aromatic and sulphur-containing com-
pounds on OV-101 268
Tables 6 27 Retention indices of oxygen- and nitrogen-containing com-
pounds on OV-101 272
Tables 6 28 Retention indices of various organic compounds on
Apolan C-87 278
Index 282
|
| any_adam_object | 1 |
| author | Pacáková, Věra Feltl, Ladislav |
| author_facet | Pacáková, Věra Feltl, Ladislav |
| author_role | aut aut |
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| building | Verbundindex |
| bvnumber | BV007922015 |
| callnumber-first | Q - Science |
| callnumber-label | QD272 |
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| dewey-full | 547.3/089 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.3/089 |
| dewey-search | 547.3/089 |
| dewey-sort | 3547.3 289 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 1. publ. |
| format | Book |
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| id | DE-604.BV007922015 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T09:14:13Z |
| institution | BVB |
| isbn | 0137723288 |
| language | English Czech |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-005234953 |
| oclc_num | 26095189 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-188 |
| physical | 285 S. graph. Darst. |
| publishDate | 1992 |
| publishDateSearch | 1992 |
| publishDateSort | 1992 |
| publisher | Horwood |
| record_format | marc |
| series2 | Ellis Horwood series in analytical chemistry |
| spellingShingle | Pacáková, Věra Feltl, Ladislav Chromatographic retention indices an aid to identification of organic compounds Chromatographie - Tables ram Compostos orgânicos larpcal Composés organiques - Analyse ram Cromatografia larpcal Chromatographic analysis Tables Organic compounds Analysis Gaschromatographie (DE-588)4019330-5 gnd Retentionsindex (DE-588)4308465-5 gnd Chromatographie (DE-588)4010153-8 gnd |
| subject_GND | (DE-588)4019330-5 (DE-588)4308465-5 (DE-588)4010153-8 |
| title | Chromatographic retention indices an aid to identification of organic compounds |
| title_auth | Chromatographic retention indices an aid to identification of organic compounds |
| title_exact_search | Chromatographic retention indices an aid to identification of organic compounds |
| title_full | Chromatographic retention indices an aid to identification of organic compounds Věra Pacáková and Ladislav Feltl |
| title_fullStr | Chromatographic retention indices an aid to identification of organic compounds Věra Pacáková and Ladislav Feltl |
| title_full_unstemmed | Chromatographic retention indices an aid to identification of organic compounds Věra Pacáková and Ladislav Feltl |
| title_short | Chromatographic retention indices |
| title_sort | chromatographic retention indices an aid to identification of organic compounds |
| title_sub | an aid to identification of organic compounds |
| topic | Chromatographie - Tables ram Compostos orgânicos larpcal Composés organiques - Analyse ram Cromatografia larpcal Chromatographic analysis Tables Organic compounds Analysis Gaschromatographie (DE-588)4019330-5 gnd Retentionsindex (DE-588)4308465-5 gnd Chromatographie (DE-588)4010153-8 gnd |
| topic_facet | Chromatographie - Tables Compostos orgânicos Composés organiques - Analyse Cromatografia Chromatographic analysis Tables Organic compounds Analysis Gaschromatographie Retentionsindex Chromatographie |
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