Applications of nuclear magnetic resonance spectroscopy in organic chemistry:
Gespeichert in:
| Beteiligte Personen: | , |
|---|---|
| Format: | Buch |
| Sprache: | Englisch |
| Veröffentlicht: |
Oxford [u.a.]
Pergamon Pr.
1969
|
| Ausgabe: | 2. ed. |
| Schriftenreihe: | International series of monographs on organic chemistry
5 |
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001258590&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Umfang: | XVI, 456 S. Ill., graph. Darst. |
Internformat
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| 245 | 1 | 0 | |a Applications of nuclear magnetic resonance spectroscopy in organic chemistry |c by L. M. Jackman ; S. Sternhell |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a Oxford [u.a.] |b Pergamon Pr. |c 1969 | |
| 300 | |a XVI, 456 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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| 490 | 1 | |a International series of monographs on organic chemistry |v 5 | |
| 650 | 4 | |a Chimie organique | |
| 650 | 4 | |a Spectroscopie de la résonance magnétique nucléaire | |
| 650 | 4 | |a Chemistry, Organic | |
| 650 | 4 | |a Magnetic Resonance Spectroscopy | |
| 650 | 4 | |a Nuclear magnetic resonance spectroscopy | |
| 650 | 4 | |a Spectrum Analysis | |
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Datensatz im Suchindex
| _version_ | 1819374686782357504 |
|---|---|
| adam_text | Titel: Applications of nuclear magnetic resonance spectroscopy in organic chemistry
Autor: Jackman, Lloyd M
Jahr: 1969
CONTENTS
Preface
xii
Preface
io
the
1st
Edition
xiv
Editorial
Preface
to
the
2nd
Edition
xvi
PART
1
An
introduction
to
the
theory
and
practice
of
nuclear
magnetic
resonance
spectroscopy
1
Chapter
1-1.
Theory
of
nuclear
magnetic
resonance
1
A.
Dynamic
and
magnetic
properties
of
atomic
nuclei
1
B.
Nuclear
resonance
2
C.
Relaxation
processes
5
D.
Chemical
effects
in
n.m.r.
11
(i)
Chemical
shift
11
(ii)
Absorption
intensities
13
(iii)
Spin-spin
coupling
13
(iv)
Time-dependent
phenomena
17
Chapter
1-2.
The
experimental
method
21
A.
The
nuclear
magnetic
resonance
spectrometer
21
(i)
The
magnet
22
(ii)
The
radiofrequency
oscillator
25
(iii)
Scanning
devices
26
(iv)
The
detector
26
(v)
Field-frequency
locks
29
B.
Experimental
factors
which
influence
resolution
and
the
shapes
of
absorption
lines
30
(i)
Homogeneity
of
the
magnetic
field
30
(ii)
Spinning
side
bands
33
(iii)
Radiofrequency
phase
33
(iv)
Sweep
rate
33
(v)
R.f.
power
level
36
(vi)
Sample
preparation
36
C.
Experimental
factors
which
influence
sensitivity
(signal-to-noise
ratio)
37
(i)
Frequency
response
38
(ii)
R.f.
power
level
38
(iii)
Concentration
38
(iv)
Availability
of
compounds—small
capacity
cells
40
(v)
Enhancement
of
sensitivity
by
time-averaging
devices
41
D.
Measurement
of
line
positions
and
determination
of
the
chemical
shift
42
E.
Measurement
of
intensities
49
F.
Solvents
52
G.
Deuterium
exchange
53
vii
Contents
viii
PART
2
Theory
of
chemical
effects
in
nuclear
magnetic
resonance
spectroscopy
55
Chapter
2-1.
Time-dependent
effects
in
nuclear
magnetic
resonance
SPECTROSCOPY
55
Chapter
2-2.
Theory
of
the
chemical
shift
61
A.
Classification
of
shielding
effects
61
B.
Local
diamagnetic
proton
shielding
63
(i)
Direct
electrostatic
effects
67
(ii)
Inductive
effects
69
(iii)
Mesomeric
effects
70
(iv)
Hybridization
70
(v)
Van
der
Waal
effects
71
C.
Long
range
shielding
72
(i)
General
principles
72
(ii)
Shielding
by
carbon-carbon
single
bonds
and
carbon-hydrogen
bonds
78
(iii)
Shielding
by
halogens
80
(iv)
Shielding
by
oxygen
atoms
in
ethers
and
alcohols
80
(v)
Shielding
by
nitrogen
atoms
81
(vi)
Shielding
by
carbon-carbon
double
bonds
83
(vii)
Shielding
by
the
carbonyl
group
88
(viii)
Shielding
by
the
carbon-carbon
triple
bond
92
(ix)
Shielding
by
the
nitrile
group
93
(x)
Shielding
by
the
nitro
group
94
(xi)
Shielding
by
aromatic
rings
94
(xii)
Shielding
by
three-membered
rings
98
D.
Contact
shifts
102
E.
The
hydrogen
bond
103
F.
Solvent
effects
104
Chapter
2-3.
Theory
of
spin-spin
multiplicity
114
A.
Recognition
of
spin-spin
multiplets
115
B.
The
mechanism
of
spin-spin
coupling
115
C.
Analysis
of
n.m.r.
spectra
118
(i)
Some
definitions
119
(ii)
The
exact
analysis
of
n.m.r.
spectra
122
(iii)
The
first-order
theory
124
(iv)
Recognition
of
second-order
spectra
128
(v)
Discussion
of
individual
spin
systems
128
a.
The
two-spin
system
(AB)
129
b.
The
three-spin
systems:
The
AB
2
to
AX
2
cases
130
c.
The
three-spin
systems:
The
AMX,
ABX
and
ABC
cases
132
d.
The
multispin
systems
related
to
ABX:
The
ABX„
system
134
e.
The
symmetrical
four-spin
systems:
A
2
X
2
,
A
2
B
2
,
AA BB ,
AA XX
134
f.
More
complex
systems
137
(vi)
Field
variation
as
an
aid
in
the
analysis
of
spectra
139
(vii)
Analysis
of
proton
spectra
with
the
aid
of
l3
C
satellite
bands
140
(viii)
Deuterium
substitution
as
an
aid
in
the
analysis
of
proton
spectra
142
(ix)
Solvent
effects
as
an
aid
in
the
analysis
of
spectra
144
(x)
Contact
shifts
as
an
aid
in
the
analysis
of
spectra
144
(xi)
Analysis
of
spectra
by
spin
decoupling
145
(xii)
Virtual
coupling
and
deceptively
simple
spectra
147
Contents
ix
Chapter
2-4.
Theory
and
applications
of
multiple
irradiation
151
A.
Theory
151
B.
Applications
153
(i)
Simplification
of
complex
spin-spin
multiplets
153
(ii)
Determination
of
relative
signs
of
spin-spin
coupling
constants
154
(iii)
Highly
accurate
determination
of
chemical
shifts
155
(iv)
Location
of
“hidden”
absorptions
155
(v)
Interrelation
of
two
or
more
coupled
groups
of
nuclei
157
(vi)
Investigation
of
moderately
rapid
chemical
exchange
reactions
157
PART
3
Applications
of
the
chemical
shift
159
Chapter
3-1.
General
considerations
159
Chapter
3-2.
Protons
bonded
to
non-cyclic
sp
3
carbon
atoms
163
A.
H—C—C
167
B.
H—C—X
174
C.
Effect
of
multiple
substitution
at
the
a-carbon
atom
181
Chapter
3-3.
Protons
bonded
to
non-aromatic
sp
2
carbon
atoms
184
A.
Olefinic
protons
H—C=C
184
B.
Formyl
protons
H—C=X
192
Chapter
3-4.
Protons
bonded
to
sp
carbon
atoms
193
Chapter
3-5.
Protons
bonded
to
sp
3
carbon
atoms
in
non-aromatic
cyclic
structures
195
Chapter
3-6.
Protons
bonded
to
aromatic
and
heterocyclic
CARBON
ATOMS
201
A.
Benzene
derivatives
201
B.
Polynuclear
and
non-benzenoid
carbocyclic
aromatic
compounds
204
C.
Heterocyclic
compounds
207
Chapter
3-7.
Protons
bonded
to
elements
other
than
carbon
215
A.
—OH,
—NH
and
—
SH
groups
215
Chapter
3-8.
Stereochemistry
and
the
chemical
shift
219
A.
Symmetry
arguments
220
(i)
Structural
applications
220
(ii)
Stereochemical
applications
222
B.
Geometrical
isomerism
in
ethylene
derivatives
222
C.
Geometrical
isomerism
in
systems
containing
C=N
and
N=N
bonds
226
D.
Cyclopropanes
and
heterocyclopropanes
227
E.
Multi-ring
structures
229
F.
Cis-trans
stereochemistry
in
four-,
five-,
and
six-membered
rings
234
G.
The
chemical
shifts
of
axial
and
equatorial
protons
and
groups
attached
to
six-membered
rings
in
chair
conformation
238
H.
Chemical
shift—stereochemistry
correlations
in
some
complex
natural
products
241
I.
Conformation
245
J.
Stereochemistry
and
the
solvent
shift
246
X
Contents
Chapter
3-9.
Carbonium
ions,
carbanions
and
related
systems
249
A.
Carbonium
ions
249
(i)
Alkyl
and
alicyclic
carbonium
ions
250
(ii)
Aryl
and
arylalkyl
carbonium
ions
251
(iii)
Alkenyl
and
cycloalkenyl
carbonium
ions
252
(iv)
Alkynyl
carbonium
ions
252
(v)
Cyclopropyl
carbonium
ions
253
(vi)
Arenonium
ions
254
(vii)
Non-classical
carbonium
ions
256
(viii)
Aromatic
cations
261
(ix)
Acyl
and
related
cations
262
B.
Carbanions
262
(i)
Grignard
reagents
and
alkylmagnesium
compounds
263
(ii)
Lithium
alkyls
and
related
compounds
264
(iii)
Aromatic
anions
265
(iv)
Miscellaneous
carbanions
266
PART
4
Spin-spin
coupling
269
Chapter
4-1.
Geminal
interproton
coupling
270
A.
Geminal
coupling
across
an
sp
3
carbon
atom
270
(i)
Influence
of
the
H—C—H
angle
273
(ii)
Influence
of
neighbouring
Tt-bonds
273
(iii)
Influence
of
ring
size
275
(iv)
Influence
of
substituent
electronegativity
276
(v)
Effect
of
orientation
of
a-substituents
277
(vi)
Miscellaneous
effects
277
B.
Geminal
coupling
across
an
sp
2
carbon
atom
277
C.
Geminal
coupling
across
a
heteroatom
279
Chapter
4-2.
Vicinal
interproton
coupling
280
A.
Vicinal
coupling
across
three
single
bonds
280
(i)
The
relation
between
vicinal
coupling
and
dihedral
angle—the
Karplus
rule
281
(ii)
Influence
of
substituent
electronegativity
283
(iii)
Influence
of
hybridization
284
(iv)
Negative
vicinal
coupling
constants
285
(v)
Influence
of
other
factors
286
(vi)
Vicinal
coupling
in
cyclic
systems
286
(vii)
Vicinal
coupling
in
flexible
systems
289
(viii)
Uses
and
abuses
of
the
Karplus
equation
292
(ix)
Examples
of
application
of
the
Karplus
rule
294
(x)
Coupling
in
the
system
CH
3
—CH
298
(xi)
Coupling
in
the
system
H—C—X—H
where
X
is
a
heteroatom
298
(xii)
Vicinal
coupling
as
an
aid
in
structure
determination
300
B.
Vicinal
interproton
coupling
across
one
double
and
two
single
bonds
301
(i)
Cis
and
trans
coupling
301
(ii)
Influence
of
electronegativity
of
substituents
302
(iii)
Influence
of
H—C=C
angle
303
(iv)
Influence
of
bond-order
of
the
double
bond
303
Contents
xi
Chapter
4-3.
Interproton
coupling
in
aromatic
and
heterocyclic
systems
305
A.
Influence
of
ring
size
310
B.
Influence
of
bond
order
310
C.
Effects
due
to
heteroatoms
310
D.
Effects
due
to
substituents
310
Chapter
4-4.
Long-range
interproton
coupling
312
A.
Observation
of
long-range
coupling
312
B.
Theory
of
long-range
coupling
315
C.
Allylic
and
homoallylic
coupling
316
D.
Long-range
coupling
in
acetylenes,
allenes
and
cumulenes
328
E.
Benzylic
coupling
330
F.
Coupling
between
protons
separated
by
five
bonds
along
an
extended
zig-zag
path
333
G.
Coupling
across
four
single
bonds
334
H.
Long-range
coupling
in
1,3-butadiene
derivatives
341
I.
Miscellaneous
examples
of
long-range
coupling
342
Chapter
4-5.
Coupling
between
protons
and
other
nuclei
345
A.
Coupling
between
1
H
and
13
C
345
B.
Coupling
between
and
19
F
348
C.
Coupling
between
1
H
and
31
P
353
D.
Coupling
between
protons
and
other
elements
356
PART
5
Applications
of
time-dependent
phenomena
357
Chapter
5-1.
General
applications
358
A.
Experimental
methods
involved
in
the
study
of
time-dependent
phenomena
in
n.m.r.
spectroscopy
358
B.
Hydrogen
exchange
and
hydrogen
bonding
359
C.
Ligand
exchange
360
D.
Partial
double
bond
character
361
E.
Valence-bond
tautomerism
362
F.
Conformational
changes
364
G.
Miscellaneous
processes
366
Chapter
5-2.
Internal
rotation
and
equivalence
of
nuclei
368
Chapter
5-3.
Tautomerism
380
References
385
Index
441
Other
Titles
in
the
Series
457
|
| any_adam_object | 1 |
| author | Jackman, Lloyd Miles Sternhell, Sev 1930- |
| author_GND | (DE-588)141639385 |
| author_facet | Jackman, Lloyd Miles Sternhell, Sev 1930- |
| author_role | aut aut |
| author_sort | Jackman, Lloyd Miles |
| author_variant | l m j lm lmj s s ss |
| building | Verbundindex |
| bvnumber | BV001930927 |
| callnumber-first | Q - Science |
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| dewey-full | 547.35/83 547/.3/087 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.35/83 547/.3/087 |
| dewey-search | 547.35/83 547/.3/087 |
| dewey-sort | 3547.35 283 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV001930927 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T07:43:25Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001258590 |
| oclc_num | 1041 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-83 DE-11 DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-83 DE-11 DE-188 |
| physical | XVI, 456 S. Ill., graph. Darst. |
| psigel | TUB-nveb HUB-ZB011200911 |
| publishDate | 1969 |
| publishDateSearch | 1969 |
| publishDateSort | 1969 |
| publisher | Pergamon Pr. |
| record_format | marc |
| series | International series of monographs on organic chemistry |
| series2 | International series of monographs on organic chemistry |
| spellingShingle | Jackman, Lloyd Miles Sternhell, Sev 1930- Applications of nuclear magnetic resonance spectroscopy in organic chemistry International series of monographs on organic chemistry Chimie organique Spectroscopie de la résonance magnétique nucléaire Chemistry, Organic Magnetic Resonance Spectroscopy Nuclear magnetic resonance spectroscopy Spectrum Analysis Organische Verbindungen (DE-588)4043816-8 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Organische Chemie (DE-588)4043793-0 gnd |
| subject_GND | (DE-588)4043816-8 (DE-588)4075421-2 (DE-588)4043793-0 |
| title | Applications of nuclear magnetic resonance spectroscopy in organic chemistry |
| title_auth | Applications of nuclear magnetic resonance spectroscopy in organic chemistry |
| title_exact_search | Applications of nuclear magnetic resonance spectroscopy in organic chemistry |
| title_full | Applications of nuclear magnetic resonance spectroscopy in organic chemistry by L. M. Jackman ; S. Sternhell |
| title_fullStr | Applications of nuclear magnetic resonance spectroscopy in organic chemistry by L. M. Jackman ; S. Sternhell |
| title_full_unstemmed | Applications of nuclear magnetic resonance spectroscopy in organic chemistry by L. M. Jackman ; S. Sternhell |
| title_short | Applications of nuclear magnetic resonance spectroscopy in organic chemistry |
| title_sort | applications of nuclear magnetic resonance spectroscopy in organic chemistry |
| topic | Chimie organique Spectroscopie de la résonance magnétique nucléaire Chemistry, Organic Magnetic Resonance Spectroscopy Nuclear magnetic resonance spectroscopy Spectrum Analysis Organische Verbindungen (DE-588)4043816-8 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Organische Chemie (DE-588)4043793-0 gnd |
| topic_facet | Chimie organique Spectroscopie de la résonance magnétique nucléaire Chemistry, Organic Magnetic Resonance Spectroscopy Nuclear magnetic resonance spectroscopy Spectrum Analysis Organische Verbindungen NMR-Spektroskopie Organische Chemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001258590&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000893331 |
| work_keys_str_mv | AT jackmanlloydmiles applicationsofnuclearmagneticresonancespectroscopyinorganicchemistry AT sternhellsev applicationsofnuclearmagneticresonancespectroscopyinorganicchemistry |