In situ spectroscopic techniques at high pressure:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Amsterdam
Elsevier
[2015]
|
| Series: | Supercritical fluid science and technology
volume 7 |
| Subjects: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029086234&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Item Description: | Includes bibliographical references and index |
| Physical Description: | xviii, 376 Seiten Illustrationen, Diagramme. - Illustrationen, Diagramme 24 cm |
| ISBN: | 9780444634221 0444634223 |
Staff View
MARC
| LEADER | 00000nam a2200000 cb4500 | ||
|---|---|---|---|
| 001 | BV043673147 | ||
| 003 | DE-604 | ||
| 005 | 00000000000000.0 | ||
| 007 | t| | ||
| 008 | 160715s2015 xx a||| |||| 00||| eng d | ||
| 016 | 7 | |a 017484222 |2 DE-101 | |
| 020 | |a 9780444634221 |c hardback |9 978-0-444-63422-1 | ||
| 020 | |a 0444634223 |c hardback |9 0-444-63422-3 | ||
| 020 | |z 9780444634207 |c ebook |9 9780444634207 | ||
| 035 | |a (OCoLC)944072512 | ||
| 035 | |a (DE-599)BSZ455383367 | ||
| 040 | |a DE-604 |b ger |e rda | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-29T | ||
| 082 | 0 | |a 543.5 | |
| 100 | 1 | |a Bräuer, Andreas |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a In situ spectroscopic techniques at high pressure |c Andreas Braeuer, Erlangen Graduate School in Advanced Optical Technologies (SAOT) and Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universtität Erlangen-Nürnberg, Germany |
| 264 | 1 | |a Amsterdam |b Elsevier |c [2015] | |
| 264 | 4 | |c © 2015 | |
| 300 | |a xviii, 376 Seiten |b Illustrationen, Diagramme. - Illustrationen, Diagramme |c 24 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Supercritical fluid science and technology |v volume 7 | |
| 500 | |a Includes bibliographical references and index | ||
| 650 | 4 | |a Spectrum analysis | |
| 650 | 4 | |a High pressure measurements | |
| 650 | 4 | |a Supercritical fluids | |
| 650 | 0 | 7 | |a Spektroskopie |0 (DE-588)4056138-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Hochdruck |0 (DE-588)4160091-5 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Spektroskopie |0 (DE-588)4056138-0 |D s |
| 689 | 0 | 1 | |a Hochdruck |0 (DE-588)4160091-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 830 | 0 | |a Supercritical fluid science and technology |v volume 7 |w (DE-604)BV041655162 |9 7 | |
| 856 | 4 | 2 | |m HEBIS Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029086234&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-029086234 | |
Record in the Search Index
| _version_ | 1819265296992567296 |
|---|---|
| adam_text | IG 1
terdam, Netherlands’
Oxford 0X5
USA
reserved
ÖfliVörsitäts- und
Uäftd^ihibiiothek
Darmstadt
or transmitted in any form or by any means, elec-
g, recording, or any information storage and retrieval
the publisher Details on how to seek permission, further
ons policies and our arrangements with organizations
the Copyright Licensing Agency, can be found at our
Contents
Foreword
Preface
List of Abbreviations and Parameters
ix
xi
xv
contained in it are protected under copyright by the
)•
constantly changing As new research and experience
h methods, professional practices, or medical treat-
yon their own experience and knowledge in evaluating
ands, or experiments described herein In using such
of their own safety and the safety of others, includ-
responsibility
Usher nor the authors, contributors, or editors, assume
persons or property as a matter of products liability,
operation of any methods, products, instructions, or
Data
m the British Library
tion Data
m the Library of Congress
1 High Pressure: Fellow and Opponent of
Spectroscopic Techniques
1 1 Compressible Fluids in High-Pressure Process Technology
1 2 Spectroscopic Techniques Bring Light into the Darkness of
High-Pressure Processes
1 3 Why High Pressure is an Opponent of Spectroscopic
Techniques?
1 4 Why High Pressure is a Fellow of Spectroscopic Techniques?
1 5 Advantages of Spectroscopic Techniques
151 Non-invasive Measurement Principle of In Situ
Spectroscopic Techniques
152 Temporal Resolution and Sampling Rates of In Situ
Spectroscopic Techniques
153 Spatial Resolution of In Situ Spectroscopic Techniques
154 Dimensionality of In Situ Spectroscopic Techniques
1 6 Exercises Corresponding to Chapter 1
Exercise 1 1: Temporal Resolution and Sampling Rate
Exercise 1 2: Spatial Resolution
Exercise 1 3: Spatial Resolution
1 7 Appendix—Chapter 1
171 Supercritical Fluids
172 Supercritical Anti-solvent (SAS) Process
References
1
5
6
7
8
8
10
14
15
20
20
24
25
26
26
33
36
ether
ies in
ountries
2 Interaction of Matter and Electromagnetic Radiation
2 1 Properties of Electromagnetic Radiation and Photons 41
211 Equation of a Harmonic Wave 42
212 Polarisation of the Electric Field 44
213 Spectrum of Electromagnetic Radiation 47
214 Energy and Momentum of a Photon 49
215 Exercises Corresponding to Section 2 1 50
v
vi Contents
2 2 Properties of Molecules 54
221 Specific Heat Capacity of a Gas 54
222 Translational Energy 56
223 Rotational Energy of a Diatomic Molecule 58
224 Vibrational Energy of a Diatomic Molecule 62
225 Electronic Energy 68
226 Energy of Molecules Relevant for Spectroscopy 71
227 Boltzmann s Distribution 74
2 3 Interaction of Bulk Matter and Electromagnetic Radiation 81
231 Index of Refraction 81
232 Reflection and Refraction of Electromagnetic Radiation 83
233 Diffraction of Electromagnetic Radiation 87
234 Elastic Light Scattering From Drops 90
235 Exercises Corresponding to Section 2 3 93
2 4 Interaction of Molecules and Electromagnetic Radiation 95
241 Absorption and Emission Processes 95
242 Scattering Processes 130
243 Brief Comparison of Absorption Techniques, Laser-Induced Fluorescence and Raman Scattering 169
244 Exercises Corresponding to Section 2 4 170
2 5 Appendix—Chapter 2 176
251 Translational Movement of Gas Molecules, the Mean Velocity of Gases and the Maxwell Velocity Distribution 176
252 Boltzmann s Distribution 179
253 Beer-Lambert Law 182
254 Meaning of a Cross-Section 183
255 Calibration of a Composition (Fuel/Air-Ratio) Indicating LIF Tracer 183
256 Hybrid Deconvolution of Mixture Spectra (Spectral Fit Approach) 186
References 188
Raman Spectroscopy From an Engineering Point of View
3 1 Three Basic Raman Sensor Designs 194
311 Signal Detection From One Point (0-D Raman Spectroscopy) 195
312 Detection of Line Profiles 202
313 Raman Imaging (Ramanography) 205
3 2 Engineering of a Raman Sensor 208
321 What Is the Suitable Excitation Wavelength for Linear Raman Spectroscopy 208
322 Stretching the Laser Pulse in Order to Prevent Window Damage 211
323 What Is the Suitable Detector 213
324 Guiding the Signals to the Detector 214
4
*1:;
4
5
f
#;
Contents
vii
325 Helpful Suggestions One Might Not Consider:
Unexpected and Undesired Interferences
3 3 Purification of Raman Signals from Undesired Interferences
331 Background Elimination via Post-Processing
332 Experimental Background Elimination Using SERDS
3 4 Case Studies
341 Vapour Liquid Equilibria
342 Gas Hydrates
343 Reactions
344 Mass Transfer During Sorption or Extraction Processes
345 Fuel-Air Mixture Generation Analysis in Internal
Combustion Engines Using 1-D Raman Spectroscopy
346 Fuel/Oxygen Mixture Generation Analysis in
Rocket Engines Using Raman Imaging
347 Heat and Mass Transfer Analysis in Hydrogen
Jets Injected Into Compressed Nitrogen Using
Raman Imaging
348 SAS Raman Imaging
3 5 Appendix—Chapter 3
351 Pulsed Excitation Lasers (Q-Switching Using a
Pockels Cell)
352 Detectors: CCD, EMCCD and ICCD
References
220
228
229
232
234
234
238
240
241
245
249
250
253
256
256
259
276
Shadowgraph and Schlieren Techniques
4 1 How Shadowgraph and Schlieren Techniques Work
411 Light Refraction by a Two-Dimensional Schliere
412 Working Principle of Shadowgraph Techniques
413 Working Principle of Schlieren Techniques
414 Distinction Between the Shadowgraph and the
Schlieren Technique
4 2 Ballistic Spray Imaging: A Special Shadowgraph Technique
4 3 Case Studies
431 Characterisation of Sprays, Jets
432 Pendant, Sessile and Levitated Drops at High Pressure
433 Supercritical Drying of Gels
434 Microfluidics for High Pressure
References
284
284
285
286
293
294
297
298
302
305
306
309
Laser-Induced Fluorescence (LIF) and Phosphorescence
(LIP) Techniques
5 1 LIF and LIP-Thermometry
511 Laser-Induced Fluorescence (LIF) for Liquid-Phase
Thermometry
512 Laser-Induced Phosphorescence (LIP) for Liquid-Phase
Thermometry
314
314
315
viii Contents
513 Laser-Induced Fluorescence (LIF) for Vapour-Phase
Thermometry 317
514 Laser-Induced Phosphorescence (LIP) for Vapour Phase
Thermometry 324
5 2 Laser-Induced Excited-Complex Fluorescence (LIEF) 326
5 3 Case Studies 329
531 Drops on Demand at Near Critical Conditions 329
532 Jet Mixing in the Vicinity of the Critical Point 332
533 Comprehensive Multi-Parameter Measurements
in Transparent Internal Combustion Engines 335
534 Brief Comparison Between Elastic Light Scattering
and LIF for Transcritical Jet Mixing Analysis 337
References 339
6 Absorption Spectroscopy
6 1 Working Principles of Absorption Spectrometers 348
611 Absorption in Transmission 348
612 Fourier-Transform Absorption Spectroscopy 350
613 Absorption in the Evanescent Field 355
614 Supercontinuum Time-of-Flight Absorption Spectroscopy 358
6 2 Case Studies 360
621 NIR Absorption Spectroscopy for Inline Monitoring
of Extraction Processes 360
622 Supercontinuum Absorption Spectroscopy for
Temperature Sensing at Elevated Pressure 361
623 In Situ Imaging of Diffusion and Dissolution
Phenomena at High Pressures 363
References 365
Subject Index
367
if-
Foreword
s
It is with great pleasure that I in
Supercritical Fluid Science and T
troscopic techniques at high pres
fied scholar, Dr Andreas Braeuer,
Erlangen-Nürnberg where he is
Laboratory and the High Press
of Administration of SAOT, the
c cal Technologies The book is
* spectroscopy at high pressure as
and warm personal writing style
to teaching The book has been
easy for a beginner to follow
more advanced practitioners in
presented with a detailed account
with superbly prepared diagrams
and practical case studies
Chapter 1 starts with an ove
ue in high-pressure research and
The author questions whether hi
‘opponent’ that hinders the utili
so provides clear presentations o
lining the challenges and limitati
i basic background pertaining to s
Chapter 2 is devoted to pro
tons, and their interaction with
rotational, vibrational and elect*
to spectroscopy are presented R
topics covered on the interaction
Absorption and emission proces
nescence, fluorescence, phosph
- Rayleigh (elastic light scattering)
ing from molecules are discuss
Chapter 3 is focused on R
are sensor design, excitation m
Raman imaging and signal proce
|
| any_adam_object | 1 |
| author | Bräuer, Andreas |
| author_facet | Bräuer, Andreas |
| author_role | aut |
| author_sort | Bräuer, Andreas |
| author_variant | a b ab |
| building | Verbundindex |
| bvnumber | BV043673147 |
| ctrlnum | (OCoLC)944072512 (DE-599)BSZ455383367 |
| dewey-full | 543.5 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543.5 |
| dewey-search | 543.5 |
| dewey-sort | 3543.5 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01984nam a2200457 cb4500</leader><controlfield tag="001">BV043673147</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">00000000000000.0</controlfield><controlfield tag="007">t|</controlfield><controlfield tag="008">160715s2015 xx a||| |||| 00||| eng d</controlfield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">017484222</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9780444634221</subfield><subfield code="c">hardback</subfield><subfield code="9">978-0-444-63422-1</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">0444634223</subfield><subfield code="c">hardback</subfield><subfield code="9">0-444-63422-3</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="z">9780444634207</subfield><subfield code="c">ebook</subfield><subfield code="9">9780444634207</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)944072512</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BSZ455383367</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rda</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-29T</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">543.5</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Bräuer, Andreas</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">In situ spectroscopic techniques at high pressure</subfield><subfield code="c">Andreas Braeuer, Erlangen Graduate School in Advanced Optical Technologies (SAOT) and Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universtität Erlangen-Nürnberg, Germany</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Amsterdam</subfield><subfield code="b">Elsevier</subfield><subfield code="c">[2015]</subfield></datafield><datafield tag="264" ind1=" " ind2="4"><subfield code="c">© 2015</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">xviii, 376 Seiten</subfield><subfield code="b">Illustrationen, Diagramme. - Illustrationen, Diagramme</subfield><subfield code="c">24 cm</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="1" ind2=" "><subfield code="a">Supercritical fluid science and technology</subfield><subfield code="v">volume 7</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">Includes bibliographical references and index</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Spectrum analysis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">High pressure measurements</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Supercritical fluids</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Spektroskopie</subfield><subfield code="0">(DE-588)4056138-0</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Hochdruck</subfield><subfield code="0">(DE-588)4160091-5</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Spektroskopie</subfield><subfield code="0">(DE-588)4056138-0</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Hochdruck</subfield><subfield code="0">(DE-588)4160091-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="830" ind1=" " ind2="0"><subfield code="a">Supercritical fluid science and technology</subfield><subfield code="v">volume 7</subfield><subfield code="w">(DE-604)BV041655162</subfield><subfield code="9">7</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">HEBIS Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029086234&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-029086234</subfield></datafield></record></collection> |
| id | DE-604.BV043673147 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T17:42:14Z |
| institution | BVB |
| isbn | 9780444634221 0444634223 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-029086234 |
| oclc_num | 944072512 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | xviii, 376 Seiten Illustrationen, Diagramme. - Illustrationen, Diagramme 24 cm |
| publishDate | 2015 |
| publishDateSearch | 2015 |
| publishDateSort | 2015 |
| publisher | Elsevier |
| record_format | marc |
| series | Supercritical fluid science and technology |
| series2 | Supercritical fluid science and technology |
| spellingShingle | Bräuer, Andreas In situ spectroscopic techniques at high pressure Supercritical fluid science and technology Spectrum analysis High pressure measurements Supercritical fluids Spektroskopie (DE-588)4056138-0 gnd Hochdruck (DE-588)4160091-5 gnd |
| subject_GND | (DE-588)4056138-0 (DE-588)4160091-5 |
| title | In situ spectroscopic techniques at high pressure |
| title_auth | In situ spectroscopic techniques at high pressure |
| title_exact_search | In situ spectroscopic techniques at high pressure |
| title_full | In situ spectroscopic techniques at high pressure Andreas Braeuer, Erlangen Graduate School in Advanced Optical Technologies (SAOT) and Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universtität Erlangen-Nürnberg, Germany |
| title_fullStr | In situ spectroscopic techniques at high pressure Andreas Braeuer, Erlangen Graduate School in Advanced Optical Technologies (SAOT) and Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universtität Erlangen-Nürnberg, Germany |
| title_full_unstemmed | In situ spectroscopic techniques at high pressure Andreas Braeuer, Erlangen Graduate School in Advanced Optical Technologies (SAOT) and Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universtität Erlangen-Nürnberg, Germany |
| title_short | In situ spectroscopic techniques at high pressure |
| title_sort | in situ spectroscopic techniques at high pressure |
| topic | Spectrum analysis High pressure measurements Supercritical fluids Spektroskopie (DE-588)4056138-0 gnd Hochdruck (DE-588)4160091-5 gnd |
| topic_facet | Spectrum analysis High pressure measurements Supercritical fluids Spektroskopie Hochdruck |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029086234&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV041655162 |
| work_keys_str_mv | AT brauerandreas insituspectroscopictechniquesathighpressure |