Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes: = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren
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| Format: | Thesis/Dissertation Book |
| Language: | English |
| Published: |
2015
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| Subjects: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027821366&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Item Description: | Aus: Angewandte Chemie : Internationale Edition ; 51. 2012 u.d.T.: Statistical raman spectrosopy / Ferdinand Hof ... - Weitere Sonderdr. enthalten |
| Physical Description: | IV, 241 S. Ill., graph. Darst. |
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| 245 | 1 | 0 | |a Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes |b = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |c vorgelegt von Ferdinand Constantin Hof |
| 246 | 1 | 1 | |a Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
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| 300 | |a IV, 241 S. |b Ill., graph. Darst. | ||
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| 500 | |a Aus: Angewandte Chemie : Internationale Edition ; 51. 2012 u.d.T.: Statistical raman spectrosopy / Ferdinand Hof ... - Weitere Sonderdr. enthalten | ||
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| adam_text | EFFICIENT SYNTHETIC SEQUENCES FOR THE COVALENT
FUNCTIONALIZATION OF SINGLE WALL CARBON NANOTUBES
EFFIZIENTE REAKTIONSSEQUENZEN FUER DIE KOVALENTE
FUNKTIONALISIERUNG VON EINWANDIGEN
KOHLENSTOFFNANOROEHREN
DER NATURWISSENSCHAFTLICHEN FAKULTAET DER FRIEDRICH-ALEXANDER-UNIVERSITAET
ERLANGEN-NUERNBERG
ZUR
ERLANGUNG DES DOKTORGRADES DR. RER. NAT.
VORGELEGT VON
FERDINAND CONSTANTIN
HOF
AUS
KOELN
HTTP://D-NB.INFO/1068782161
TABLE OF CONTENT
TABLE OF CONTENT
LIST OF ABBREVIATIONS IV
1. INTRODUCTION 1
1.1.
NANOSTRUCTURES 1
1.2. CARBON ALLOTROPES 3
1.3. BASICS CONCEPTS OF CARBON NANOTUBES 4
1.3.1. STRUCTURAL PROPERTIES OF CARBON NANOTUBES 4
1.3.2. ELECTRONIC PROPERTIES OF CARBON NANOTUBES 7
1.3.3. PRODUCTION OF CNTS 8
1.3.4. SPECIFIC SURFACE AREA OF CNTS 9
1.3.5. BASIC CONCEPTS FORTHE FUNCTIONALIZATION AND THE SEPARATION OF
CNTS. 11
1.4. COVALENT FUNCTIONALIZATION OF THE FRAMEWORK OF CARBON NANOTUBES 14
1.4.1. OXIDATIVE FUNCTIONALIZATION OF SWCNTS 16
1.4.2. FLUORINATION OF SWCNTS 17
1.4.3. ADDITION REACTIONS TO THE CARBON LATTICE OF SWCNTS 17
1.4.4. FUNCTIONALIZATION OF SWCNTS USING DIAZONIUM SALTS 19
1.4.5. REDUCTIVE FUNCTIONALIZATION OF SWCNTS 20
1.5. CHARACTERIZATION OF FUNCTIONALIZED SWCNT SPECIES 21
1.5.1. RAMAN SPECTROSCOPY OF SWCNTS 21
1.5.2. THERMO GRAVIMETRIE ANALYSIS OF FUNCTIONALIZED SWCNTS 24
1.5.3. IR-SPECTROSCOPY OF FUNCTIONALIZED SWCNTS 26
1.5.4. OPTICAL SPECTROSCOPY OF SWCNTS 26
1.6. REACTIVITY OF SWCNTS 28
1.6.1. DESCRIBING THE REACTIVITY OF CNTS BY THE MODEL OF THE
PYRAMIDALIZATION
ANGLE 28
1.6.2. REACTIVITY OF SWCNTS CONSIDERING INDIVIDUAL VS BUNDLED SWCNTS....
30
1.7. SELECTIVITY 32
/
TABLE OF CONTENT
1.7.1. ENDO VS EXO - COVALENT FUNCTIONALIZATION OF SWCNTS 33
1.7.2. REGIOSELECTIVELY ATTACHED FUNCTIONAL GROUPS AT THE FRAMEWORK OF
SWCNTS 35
1.7.3. TYPE SELECTIVE REACTIONS ON SWCNTS 37
2. PROPOSAL 43
3. INDEX OF PUBLICATIONS 44
4. RESULTS AND DISCUSSIONS 46
4.1. DETERMINATION OF INTRODUCED DEFECTS AND ELECTRONIC TYPE SELECTIVE
REACTION
ON CARBON NANOTUBES 53
4.1.1. STATISTICAL RAMAN SPECTROSCOPY: A METHOD FOR THE CHARACTERIZATION
OF
COVALENTLY FUNCTIONALIZED SINGLE-WALLED CARBON NANOTUBES - MANUSCRIPT 63
4.1.2. STATISTICAL RAMAN SPECTROSCOPY: A METHOD FOR THE CHARACTERIZATION
OF
COVALENTLY FUNCTIONALIZED SINGLE-WALLED CARBON NANOTUBES * ELECTRONIC
SUPPORTING INFORMATION 68
4.2. IDENTIFICATION OF ENTITIES ATTACHED TO CARBON NANOTUBES 76
4.2.1. NEW BASIC INSIGHT INTO REDUCTIVE FUNCTIONALIZATION SEQUENCES OF
SINGLE
WALLED CARBON NANOTUBES (SWCNTS)RMANUSCRIPT 85
4.2.2. NEW BASIC INSIGHT INTO REDUCTIVE FUNCTIONALIZATION SEQUENCES OF
SINGLE
WALLED CARBON NANOTUBES (SWCNTS)-ELECTRONIC SUPPORTING INFORMATION 97
4.3. ANALYSIS OF HIGHLY REACTIVE INTERMEDIATES SUCH AS BROMINATED SWCNTS
119
4.3.1. BROMINATED SINGLE WALLED CARBON NANOTUBES AS VERSATILE PRECURSORS
FOR
COVALENT SIDEWALL FUNCTIONALIZATION - MANUSCRIPT 122
4.3.2. BROMINATED SINGLE WALLED CARBON NANOTUBES AS VERSATILE PRECURSORS
FOR
COVALENT SIDEWALL FUNCTIONALIZATION - ELECTRONIC SUPPORTING INFORMATION
126
4.4. BULK ANALYSIS OF FUNCTIONALIZED CARBON NANOTUBES AND GRAPHENE 136
4.4.1. NOVEL X.
3
-LODANE
BASED FUNCTIONALIZATION OF SYNTHETIC CARBON ALLOTROPES
(SCAS) - COMMON CONCEPTS AND QUANTIFICATION OF THE DEGREE OF ADDITION -
MANUSCRIPT 144
//
TABLE OF CONTENT
4.4.2. NOVEL X.
3
-LODANE BASED FUNCTIONALIZATION OF SYNTHETIC CARBON ALLOTROPES
(SCAS) - COMMON CONCEPTS AND QUANTIFICATION OF THE DEGREE OF ADDITION -
ELECTRONIC SUPPORTING INFORMATION 153
4.5. CO-AUTHOR PUBLICATIONS 182
4.5.1. CO-AUTHOR PUBLICATION * 1 * 183
4.5.2. CO-AUTHOR PUBLICATION - 2 - 199
4.5.3. CO-AUTHOR PUBLICATION * 3 * 207
4.5.4. CO-AUTHOR PUBLICATION - 4- 212
5. SUMMARY 220
6. ZUSAMMENFASSUNG 223
7. LITERATURE 226
8. APPENDIX 238-
III
|
| any_adam_object | 1 |
| author | Hof, Ferdinand Constantin |
| author_GND | (DE-588)1067768270 |
| author_facet | Hof, Ferdinand Constantin |
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| bvnumber | BV042385377 |
| ctrlnum | (OCoLC)904344155 (DE-599)BVBBV042385377 |
| dewey-full | 546.681425 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 546 - Inorganic chemistry |
| dewey-raw | 546.681425 |
| dewey-search | 546.681425 |
| dewey-sort | 3546.681425 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| illustrated | Illustrated |
| indexdate | 2024-12-20T17:09:46Z |
| institution | BVB |
| language | English |
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| physical | IV, 241 S. Ill., graph. Darst. |
| publishDate | 2015 |
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| spellingShingle | Hof, Ferdinand Constantin Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren Kohlenstoff-Nanoröhre (DE-588)4581365-6 gnd Funktionalisierung Chemie (DE-588)4279323-3 gnd |
| subject_GND | (DE-588)4581365-6 (DE-588)4279323-3 (DE-588)4113937-9 |
| title | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
| title_alt | Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
| title_auth | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
| title_exact_search | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
| title_full | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren vorgelegt von Ferdinand Constantin Hof |
| title_fullStr | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren vorgelegt von Ferdinand Constantin Hof |
| title_full_unstemmed | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren vorgelegt von Ferdinand Constantin Hof |
| title_short | Efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes |
| title_sort | efficient synthetic sequences for the covalent functionalization of single wall carbon nanotubes effiziente reaktionssequenzen fur die kovalente funktionalisierung von einwandigen kohlenstoffnanorohren |
| title_sub | = Effiziente Reaktionssequenzen für die kovalente Funktionalisierung von einwandigen Kohlenstoffnanoröhren |
| topic | Kohlenstoff-Nanoröhre (DE-588)4581365-6 gnd Funktionalisierung Chemie (DE-588)4279323-3 gnd |
| topic_facet | Kohlenstoff-Nanoröhre Funktionalisierung Chemie Hochschulschrift |
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