Verfügbarkeit: Introduction to nanoscience and nanomaterials

Introduction to nanoscience and nanomaterials:

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Bibliographische Detailangaben
Beteilige Person:	Agrawal, Dinesh Chandra 1943- (VerfasserIn)
Format:	Buch
Sprache:	Englisch
Veröffentlicht:	New Jersey [u.a.] World Scientific 2013
Schlagwörter:	Nanostrukturiertes Material Nanowissenschaften Nanotechnologie
Links:	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027503957&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027503957&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA
Umfang:	XV, 556 S. zahlr. Ill. und graph. Darst.
ISBN:	9789814397971

Internformat

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245	1	0	\|a Introduction to nanoscience and nanomaterials \|c Dinesh C. Agrawal
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Datensatz im Suchindex

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adam_text	Contents Preface ....................................................................................................................... v Acknowledgements ........................................................................................................... vi Chapter 1 : Introduction ....................................................................................................1 Chapter 2 : Surfaces .........................................................................................................9 2.1 Introduction .............................................................................................................9 2.2 The solid—vapor interface ......................................................................................3 1 2.2.1 Surface energy ...........................................................................................11 2.2.2 Equilibrium shape of a crystal ....................................................................14 2.2.3 Structure of nanoclusters ............................................................................17 2.2.3.1 Icosahedron (Ih) ...........................................................................19 2.2.3.2 Decahedron (Dh) ..........................................................................19 2.2.4 Surface reconstruction and surface relaxation ............................................22 2.2.4.1 Surface relaxation .........................................................................23 2.2.4.2 Surface reconstruction ..................................................................23 2.2.4.3 Reconstructed surfaces as templates for nanostructures ...............27 2.2.5 Surface defects and crystal defects .............................................................27 2.2.5.1 Defects on the vicinal surfaces .....................................................27 2.2.5.2 Crystal defects ..............................................................................29 2.2.6 Effect of surface curvature .........................................................................30 2.2.6.1 Chemical potential at the curved surfaces ....................................30 2.2.6.2 Pressure under a curved surface ...................................................31 2.2.6.3 Vapor pressure over a curved surface ...........................................33 2.2.6.4 Vacancy concentration under a curved surface .............................33 2.2.6.5 Solubility of curved surfaces ........................................................34 2.2.7 Examples and applications .........................................................................36 2.2.7Д Melting point of nanoparticles ......................................................36 2.2.7.2 Coarsening of particles — the OstwaJd ripening ..........................36 2.2.7.3 Sintering of solids .........................................................................37 2.2.7.4 Condensation of vapor in a capillary: agglomeration of nanoparticles due to pendular forces ............................................38 vii vili Introduction to Nanoscience and Nano mat e rials 2.3 The solid—liquid interface .....................................................................................40 2.3.1 The surface tension ....................................................................................40 2.3.2 The contact angle .......................................................................................41 2.3.3 The contact angle hysteresis .......................................................................44 2.3.4 Superhydropbobic, superhydrophilic and self cleaning surfaces ................46 2.3.4.1 Increase in contact angle on rough hydrophobic surfaces: the lotus effect ...........................................................................46 2.3.4.2 The Wenzel and the Cassie— Baxter equations ..............................47 2.3.4.3 Superb ydrophilic surfaces: Enhanced hydjophilicity due to surface roughness .........................................................................51 2.3.4.4 Examples of superhydrophobic and superhydrophilic surfaces byn anostructuring ........................................................................55 2.3.4.5 Titania coated superhydrophilic and self cleaning surfaces ..........55 Appendix 2.1 : Melting point of nanoparticles .................................................................58 Problems ..........................................................................................................................61 Chapter 3 : Zero Dimensiona] Nan os tru с tures I Review of Some Topics m Physics .....65 3.1 Introduction ...........................................................................................................65 3.2 Size dependence of properties in the nanometer range .........................................66 3.3 Review of some topics in physics .........................................................................69 3.3.1 Particle and wave: The Schrodinger équation ............................................69 3.3.1.1 lhe hydrogen atom .......................................................................72 3.3.1.2 A free ρ article ...............................................................................73 3.3.1.3 Particle in an infinite potential square well ...................................73 3.3.2 Free electron model of a solid ....................................................................76 3.3.3 Electron in a periodic potential: the occurrence of the band gap ................79 3.3.4 Reciprocal lattice and theBiillourn zone ...................................................83 3.3.4.1 The reciprocal lattice ....................................................................83 3.3.4.2 The Bnlloum zones ......................................................................84 3.3.5 The band structures of semiconductors ......................................................86 3.3.6 Energy levels withm the band gap — shallow traps and the deep traps .....91 3.3.6.1 Shallow traps in doped semiconductors ........................................91 3.3.6.2 Deep level traps ............................................................................93 3.3.7 Characteristic lengths in the nanometer range ............................................93 3.3.7.1 de Braghe Wavelength ...................................,.............................93 3.3.7.2 Mean free path of electrons ..........................................................94 3.3.7.3 Exciton and Bohr excitonradius ...................................................95 3.3.7.4 Other length scales .....................................................................101 3.3.8 The Density of States function for low dimensional systems ...................102 3.3.8.1 The quantum well .......................................................................104 3.3.8.2 The quantum wire .......................................................................109 3.3.8.3 The quantum dot ......................................................................... Ill Contents їх Problems ........................................................................................................................134 Chapter 4 : Semiconductor quantum dots .....................................................................117 4.1 Introduction .........................................................................................................117 4.2 Energy levels and change in band gap with size in quantum dots .......................118 4.3 Coulomb blockade m a quantum dot ...................................................................121 4.4 Formation of self assembled quantum dots by epitaxial deposition. ....................124 4.4.1 Introduction ..............................................................................................124 4.4.2 Quantum dots by epitaxial deposition ......................................................125 4.4.3 Energetics of self assembled quantum dot formation — the Stranski- Kxanstanow growth ..................................................................................127 4.4.4 Stacked layers of quantum dot arrays .......................................................131 4.5 Applications of quantum dots .............................................................................133 Problems ........................................................................................................................137 Chapter 5 : Zero Dimensional Nanostructures Π The Metal Nanoparticles ..................141 5.1 Introdu ction .........................................................................................................141 5.2 Optical properties of bulk metals ........................................................................141 5.3 Interaction of light with metal nanoparticles .......................................................145 5.4 Surface plasmon resonance .................................................................................147 5.4.1 Introduction ..............................................................................................147 5.4.2 Effect of particle shape .............................................................................151 5.4.3 Applications .............................................................................................152 Problems ........................................................................................................................157 Chapter 6 : Zero Dimensional Nanostructures III The Nanoscale Magnetic Structures ...................................................................................................159 6.1 Introduction ........................................................................................................159 6.2 Definitions ..........................................................................................................160 6.2.1 Magnetic lines of force .............................................................................160 6.2.2 Magnetic field ..........................................................................................161 6.2.3 Magnetic moment and magnetization ......................................................161 6.2.4 Magnetic moment of an atom ...................................................................163 6.2.5 Magnetic moment of a solid .....................................................................164 6.3 Classification of magnetic materials ...................................................................165 6.3.1 Diamagnetic materials ..............................................................................165 6.3.2 Paramagnetic materials ............................................................................166 6.3.3 Ferromagnetic materials ...........................................................................167 6.3.4 Antiferro magnetic and femmagnetic materials ........................................168 6.4 Nanoscale ferromagnetic materials .....................................................................168 6.4.1 Magnetization curve of a ferromagnetic crystal .......................................168 χ Introduction to Nanoscience and Nanomaterials 6.4.2 Magnetic anisotropy .................................................................................170 6.4.2.1 Magnetocrystallme anisotropy ....................................................170 6.4.2.2 Shape anisotropy ........................................................................174 6.4.2.3 Surface anisotropy ......................................................................176 6.4.3 Superparamgnetism ..................................................................................178 6.4.4 Superparamagnetic matenals: Ferrofimds ................................................185 6.4.5 Nan о structures exploiting the shape anisotropy .......................................187 6.4.6 Spin dependent scattering: The Giant Magnetoresistance (GMR)...........189 Problems ........................................................................................................................194 Chapter 7 : Zero Dimensional Nanostractures IV Colloids and Colloidal Crystals ......195 7.1 Introduction .........................................................................................................195 7.2 The van der Waal s forces ..................................................................................196 7.2.1 Introduction ..............................................................................................196 7.2.2 The van der Waal s forces between particles ...........................................199 7.2.3 Effect of the parti cle geometry .................................................................202 7.2.3.1 Plane parallel plates ....................................................................202 7.2.3.2 Two equ al spheres ......................................................................203 7.2.3.3 Sphere and a plate .......................................................................203 7.2.4 Charge on the particle surfaces ................................................................204 7.2.5 Zeta potential and die isoelectric point .....................................................207 7.2.6 Electrostatic stabilization: The electrical double layer .............................209 7.2.6.1 Introduction ................................................................................209 Ί .2.6.2 Thickness of the double layer .....................................................210 7.2.6.3 Controlling the stability of the electrostatically stabilized suspensions .................................................................................215 7.3 Steric stabilization of suspensions ......................................................................216 7.3.1 Introduction ..............................................................................................216 7.3.2 Mechanism ................................................................................................217 7.3.3 Requirement on the cham length ..............................................................220 7.4 Colloidal crystals for photonic applications ........................................................226 7.4.1 Introduction ..............................................................................................226 7.4.2 Soft and hard interactions .........................................................................229 7.4.3 Preparation of colloidal crystals ................................................................231 Problems ........................................................................................................................234 Chapter 8 : Carbon Nanostractures ...............................................................................237 8.1 Introduction .........................................................................................................237 8.2 Structure ..............................................................................................................238 8.2.1 Structure of graphite .................................................................................238 8.2.2 Structure of graphene ...............................................................................240 Contents xi 8.2.3 Structure of fullerene................................................................................ 244 8.2.4 Structure of carbon nanotubes ..................................................................246 8.3 Préparation of carbon nanotubes .........................................................................251 8.3.1 The arc—discharge method .......................................................................252 8.3.2 Laser vaporization ....................................................................................253 8.3.3 Chemical vapor deposition .......................................................................254 8.3.4 Patterned growth of carbon nanotubes .....................................................255 8.3.5 Theories of nanotube growth ....................................................................256 8.4 Preparation of graphene ......................................................................................256 8.5 Properties ............................................................................................................258 8.5.1 Mechanical properties ..............................................................................258 8.5.1.1 Theoretical modeling of the modulus, strength and fracture ......259 8.5.1.2 Experimental measurements of modulus and strength ................261 8.5.2 Electrical properties .................................................................................265 8.5.2.1 Electrical properties of graphene ................................................265 8.5.2.2 Electrical properties of carbon nanotubes ...................................268 8.6 Applications of carbon nanotubes .......................................................................270 8.6.1 Composites ...............................................................................................270 8.6.2 Field emission ..........................................................................................270 8.6.3 Conductive composites ............................................................................273 8.6.4 Other applications ....................................................................................276 Problems ........................................................................................................................278 Chapter 9 : Other One Dimensional Nanostructures .....................................................281 9.1 Introduction .........................................................................................................281 9.2 GrowtJh of one dimensional nanostructures .........................................................282 9.2.1 The vapor-liquid-solid (VLS) nano wire growth process ..........................282 9.2.1.1 Dependence of growth rate on the diameter ...............................287 9.2.1.2 Conditions fornanowire growth .................................................289 9.2.2 Template assisted growth of nanowires ...................................................293 9.2.3 Exploitation of inherent or induced surface energy amsotropy ................294 9.3 Selected properties and applications ...................................................................295 Problems ........................................................................................................................300 Chapter 10 : Two Dimensiona] Nanostructures ............................................................301 10.1 Introduction .........................................................................................................301 10.2 Thin film deposition ............................................................................................302 10.2.1 Some considerations in thin film deposition ............................................302 10.2.2 Physical vapor deposition (PVD) .............................................................304 10.2.3 Chemical vapor deposition .......................................................................310 10.2.4 The sol- gel process ................................................................................315 xii Introduction to Nanoscience and Nanomaterials 10.2.4.1 Introduction ................................................................................315 10.2.4.2 Sols from metal salts.................................................................. 317 10.2.4.3 Sols from alkoxides ....................................................................319 10.2.4.4 Thin film deposition from a sol ..................................................322 10.2.4.5 Cracking of gels and films ..........................................................325 10.2.4.6 Preparation of mesoporous matenals ..........................................327 10.2.5 Atomic Layer Deposition (ALD) .............................................................328 10.2.6 Layer—by-layer (LBL) deposition ............................................................332 10.2.6.1 Introduction ................................................................................332 10.2.6.2 The layer—by-layer deposition process .......................................332 10.2.6.3 Controlling the thickness of the individual layers ......................336 10.2.6.4 Incorporating nanoparticles in an LBL film ...............................337 10.2.6.5 Surface functionalization of nanoparticles .................................338 10.3 Multilayers for mechanical engineering applications ..........................................339 10.3.1 Introduction ..............................................................................................339 10.3.2 The hardening mechanisms for superlattices ............................................340 10.3.2.1 Dislocation nucleation and multiplication within a layer ...........341 10.3.2.2 Dislocation movement across an interface .................................344 10.3.2.3 Comparison with experiments ....................................................348 10.3.3 Mechanisms for nanocomposite coatings .................................................349 Problems ........................................................................................................................353 Chapter 11 : Bulk Nanos tinctured Matenals .................................................................355 11.1 Introduction .........................................................................................................355 11.2 Preparation of bulk nanocry stalline metals .........................................................355 11.2.1 Consolidation of fine metal powder by cold compaction .........................356 11.2.2 Electxodeposition ......................................................................................357 11.2.3 Crystallization of metallic glasses .............................................................358 11.2.4 Severe plastic deformation (SPD),.........................................,..................358 11.2.5 Nanocrystalline steel by thermomechanical working ...............................360 11.3 Mechanical properties of nano scale metals ..........................................................360 11.3.1 Hardness and nanoindentation ....................................................................360 11.3.2 Effect of nano-grain size on the concentration of defects .........................362 11.3.3 Effect of grain size on the yield strength: the inverse Hall— Petch effect ...............................................................................................364 11.3.4 Ductility of the nanocrystallme metals .....................................................368 Problems ........................................................................................................................374 Chapter 12 : Polymer Nanocomposites ..........................................................................377 12.1 Introduction .........................................................................................................377 12.2 Introduction to the mechanical properties of composites ....................................378 12.2.1 Modulus and strength of the unidirectional fiber reinforced composites . 380 Contents xiii 12.2.2 Short fiber and particle reinforced composites ......................................... 383 12.2.2.1 Importance of the aspect ratio ....................................................383 12.2.2.2 Modulus and strength of short fiber composites .........................386 12.2.2.3 The HaJpin-Tsai and Mori-TanaJca formulations ......................388 12.3 Polymer-CNT nanocomposites ..........................................................................392 12.3.1 Introduction ...............................................................................................392 12.3.2 Some important considerations m CNT— composites ................................393 12.3.2.1 Aspect ratio of the CNT .............................................................393 12.3.2.2 Shear strength of the matrix-CNT interface ...............................394 12.3.2.3 Dispersion of the nanotubes in the matrix ..................................395 12.3.2.4 Wavmess of the nanotubes .........................................................397 12.3.3 Processing and properties of the polymer-CNT composites ....................398 12.4 Polymer—clay nanocomposites ............................................................................401 12 А Л Filled polymers vs. the polymer nanocomposites .....................................401 12.4.2 Clays used in the nanocomposites ............................................................403 12.4.3 Preparation of the polymer-exfoliated clay nano-composites ..................408 12.4.4 Properties of the polymer-clay nanocomposites ......................................410 12.4.4.1 Introduction ................................................................................410 12.4.4.2 Mechanical properties ................................................................411 12.4.4.3 The barrier properties of the polymer nanocomposites ...............416 12.4.5 The nanoeffects ........................................................................................419 Problems ........................................................................................................................421 Chapter 13: Molecules for Nanotechnology: Polymers, Biopolymers, Dendrimers and Surfactants .......................................................................423 13.1 Polymers .............................................................................................................423 13.1.1 Some common polymers ..........................................................................424 13.1.2 Properties of polymers .............................................................................424 13.1.2.1 Molecular weight ........................................................................424 13.1.2.2 Length of a polymer chain ..........................................................426 13.1.2.3 Bonding within and between polymer chains: thermoplastics, thermosets and elastometers .......................................................429 13.1.2.4 Glass transition temperature .......................................................431 13.1.3 Crystalline polymers ................................................................................433 13.1.4 Polymer solutions: Phase separation ........................................................434 13.2 Polyelectxolytes ...................................................................................................438 13.3 Copolymers .........................................................................................................439 13.3.1 Types of copolymers ................................................................................439 13.3.2 Phase separation in block copolymers ......................................................440 13.4 Biopolymers........................................................................................................442 13.4.1 Proteins ....................................................................................................443 xiv Introduction to Nanoscíence and Nanomaterials 13.4.2 Nucleic acids ............................................................................................446 13.4.2.1 Deoxynbonucleic acid (DNA)....................................................447 13.4.2.2 Ribonucleic acid (RNA) .............................................................449 13.5 Surfactants ..........................................................................................................450 13.5.1 Introduction ..............................................................................................450 13.5.2 Types of surfactants .................................................................................452 13.5.3 Absorption of surfactant molecules in a solution .....................................456 13.5.3.1 Introduction ................................................................................456 13.5.3.2 The Gibbs absorption equation ...................................................460 13.6 Dendrimers .........................................................................................................463 13.6.1 Synthesis ..................................................................................................463 13.6.2 Properties and applications .......................................................................466 Problems ........................................................................................................................468 Chapter 14: Self Assembly and Self Organization .........................................................471 14.1 Introduction .........................................................................................................471 14.2 Interactions important in self assembly ...............................................................472 14.2.1 Ionic and electrostatic interactions ...........................................................472 14.2.2 The π -interactions .................................................................................... 474 14.2.3 The hydrogen bond ..................................................................................476 14.2.4 van der Waals interactions .......................................................................478 14.2.5 Coordinative bond and coordination complex ..........................................478 14.2.6 Dative bond ..............................................................................................480 14.2.7 The hydrophobic effect ............................................................................480 14.3 Examples of self assembled systems ...................................................................481 14.3.1 Self assembled monolayers (SAM) ..........................................................481 14.3.2 Self assembly of amphiphiles into nanostructures ....................................482 14.3.2.1 The critical micelle concentration (CMC) ..................................482 14.3.2.2 Spherical micelle — tihe simplest amphiphile nanostructure ......483 14.3-2.3 Other nanostractures — relation to the packing factor ...............484 14.3.3 Langmuu-Blodge« (L-B) films ..................................................................486 14.3.3.1 Deposition of nanoparticles films using the Ъ-В technique .......491 14.3.4 Liquid crystals ..........................................................................................491 14.3.5 Dendrimer self assembly ..........................................................................493 Problems ........................................................................................................................495 A.I. Appendix 1. Description of crystal structure ......................................................497 A.2. Appendix 2: Review of the mechanical properties of crystalline solids ..............502 A2.1 Stress ......................................................................................................502 A2.2 Strain ......................................................................................................504 Contents xv A2.3 The elastic moduli ..................................................................................506 A2 .4 The elastic strain energy .........................................................................507 A2.5 The tensile test ........................................................................................508 A2.6 The theoretical yield stress .....................................................................513 A2.7 The critical resolved stress .....................................................................514 A2. 8 Dislocation multiplication and strain hardening ....................................516 A2. 8.1 Dislocation multiplication ..........................................................517 A2.8.2 Strain hardening ..........................................................................520 A2 .9 Dispersion hardening ..............................................................................520 A2.10 Creep ......................................................................................................522 A2.11 Bnttle fracture ........................................................................................526 References ......................................................................................................................533 Index ..............................................................................................................................553 This textbook is aimed primarily at the senior undergraduate ano first year graduate students from the various engineering and sciences departments including physics, chemistry, materiais engineering, chemical engineering, electrical engineering, mechanical engineering, bioengineeringr and biology. Researchers in the areas of nanomateriais ana nanoscience wilt aiso find the book useful for building the background necessary to understand the current literature año as a reference book. The text assumes only з basic level of competency in physics, chemistry and mathematics. Some of the background materia! and introductory matter are included in the first few chapters and as appendices. Although this material may be familiar to some of tht students, it is the author s experience after teaching such a course for many years that this can not be taken for granted and moreover, serves as a ready reference to understand the text. As the area of nanoscience, nanotechnofogy nanomateriais is з fast developing one, an approach which equips the students ίο comprehend the developing field rather than providing a large volume of information is essential. With this in view, while providing в broad perspective, the book emphasizes basics of nanoscience anć nanoscale materiais and goes into sufficient ůepth for the reader to be Bb t to handle numerical problems. The treatment is kept Bt a level which is easily comprehensible to an undergraduate student. Solved examples зге provided in each chapter to aid understanding a set of problems rs given at the end of each chapter.
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id	DE-604.BV042063116
illustrated	Illustrated
indexdate	2024-12-20T17:01:17Z
institution	BVB
isbn	9789814397971
language	English
oai_aleph_id	oai:aleph.bib-bvb.de:BVB01-027503957
oclc_num	892429359
open_access_boolean
owner	DE-355 DE-BY-UBR DE-20
owner_facet	DE-355 DE-BY-UBR DE-20
physical	XV, 556 S. zahlr. Ill. und graph. Darst.
publishDate	2013
publishDateSearch	2013
publishDateSort	2013
publisher	World Scientific
record_format	marc
spellingShingle	Agrawal, Dinesh Chandra 1943- Introduction to nanoscience and nanomaterials Nanostrukturiertes Material Nanowissenschaften (DE-588)7734987-8 gnd Nanotechnologie (DE-588)4327470-5 gnd Nanostrukturiertes Material (DE-588)4342626-8 gnd
subject_GND	(DE-588)7734987-8 (DE-588)4327470-5 (DE-588)4342626-8
title	Introduction to nanoscience and nanomaterials
title_alt	Nanoscience and nanomaterials
title_auth	Introduction to nanoscience and nanomaterials
title_exact_search	Introduction to nanoscience and nanomaterials
title_full	Introduction to nanoscience and nanomaterials Dinesh C. Agrawal
title_fullStr	Introduction to nanoscience and nanomaterials Dinesh C. Agrawal
title_full_unstemmed	Introduction to nanoscience and nanomaterials Dinesh C. Agrawal
title_short	Introduction to nanoscience and nanomaterials
title_sort	introduction to nanoscience and nanomaterials
topic	Nanostrukturiertes Material Nanowissenschaften (DE-588)7734987-8 gnd Nanotechnologie (DE-588)4327470-5 gnd Nanostrukturiertes Material (DE-588)4342626-8 gnd
topic_facet	Nanostrukturiertes Material Nanowissenschaften Nanotechnologie
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027503957&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027503957&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT agrawaldineshchandra introductiontonanoscienceandnanomaterials AT agrawaldineshchandra nanoscienceandnanomaterials

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