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Homogeneous catalysts: activity - stability - deactivation

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Bibliographic Details
Main Authors:	Leeuwen, Piet W. N. M. van 1942- (Author), Chadwick, John C. 1950- (Author)
Format:	Book
Language:	English
Published:	Weinheim Wiley-VCH 2011
Subjects:	Katalysator Homogene Katalyse
Links:	http://deposit.dnb.de/cgi-bin/dokserv?id=3655689&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024148811&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Item Description:	Literaturangaben
Physical Description:	XIII, 404 S. graph. Darst.
ISBN:	9783527323296 3527323295

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Record in the Search Index

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adam_text	IMAGE 1 CONTENTS PREFACE XI 1 ELEMENTARY STEPS 1 1.1 INTRODUCTION 1 1.2 METAL DEPOSITION 2 1.2.1 LIGAND LOSS 2 1.2.2 LOSS OF H + , REDUCTIVE ELIMINATION OF HX 2 1.2.3 REDUCTIVE ELIMINATION OF C-, N-, O-DONOR FRAGMENTS 5 1.2.4 METALLIC NANOPARTICLES 6 1.3 LIGAND DECOMPOSITION BY OXIDATION 7 1.3.1 GENERAL 7 1.3.2 OXIDATION 7 1.3.2.1 CATALYSIS USING O 2 7 1.3.2.2 CATALYSIS USING HYDROPEROXIDES 8 1.4 PHOSPHINES 8 1.4.1 INTRODUCTION 8 1.4.2 OXIDATION OF PHOSPHINES 9 1.4.3 OXIDATIVE ADDITION OF A P-C BOND TO A LOW-VALENT METAL 11 1.4.4 NUDEOPHILIC ATTACK AT PHOSPHORUS 16 1.4.5 ARYL EXCHANGE VIA PHOSPHONIUM INTERMEDIATES 19 1.4.6 ARYL EXCHANGE VIA METALLOPHOSPHORANES 21 1.5 PHOSPHITES 23 1.6 IMINES AND PYRIDINES 26 1.7 CARBENES 27 1.7.1 INTRODUCTION TO NHCS AS IIGANDS 27 1.7.2 REDUCTIVE ELIMINATION OF NHCS 28 1.7.3 CARBENE DECOMPOSITION IN METATHESIS CATALYSTS 31 1.8 REACTIONS OF METAL-CARBON AND METAL-HYDRIDE BONDS 36 1.8.1 REACTIONS WITH PROTIC REAGENTS 36 1.8.2 REACTIONS OF ZIRCONIUM AND TITANIUM ALKYL CATALYSTS 37 1.9 REACTIONS BLOCKING THE ACTIVE SITES 38 1.9.1 POLAR IMPURITIES 38 1.9.2 DIMER FORMATION 39 BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1009639854 DIGITALISIERT DURCH IMAGE 2 VI CONTENTS 1.9.3 LIGAND METALLATION 40 REFERENCES 41 2 EARLY TRANSITION METAL CATALYSTS FOR OLEFIN POLYMERIZATION 51 2.1 ZIEGLER-NATTA CATALYSTS 51 2.1.1 INTRODUCTION 52 2.1.2 EFFECT OF CATALYST POISONS 52 2.1.3 TICL 3 CATALYSTS 53 2.1.4 MGCL 2 -SUPPORTED CATALYSTS 54 2.1.4.1 MGCL 2 /TICL 4 /ETHYL BENZOATE CATALYSTS 54 2.1.4.2 MGCL 2 /TICL 4 /DIESTER CATALYSTS 56 2.1.4.3 MGCL 2 /TICL 4 /DIETHER CATALYSTS 57 2.1.5 ETHENE POLYMERIZATION 57 2.2 METALLOCENES 58 2.2.1 INTRODUCTION 58 2.2.2 METALLOCENE/MAO SYSTEMS 62 2.2.3 METALLOCENE/BORATE SYSTEMS 66 2.3 OTHER SINGLE-CENTER CATALYSTS 69 2.3.1 CONSTRAINED GEOMETRY AND HALF-SANDWICH COMPLEXES 69 2.3.2 OCTAHEDRAL COMPLEXES 73 2.3.3 DIAMIDE AND OTHER COMPLEXES 75 2.4 VANADIUM-BASED CATALYSTS 76 2.5 CHROMIUM-BASED CATALYSTS 80 2.6 CONCLUSIONS 82 REFERENCES 83 3 LATE TRANSITION METAL CATALYSTS FOR OLEFIN POLYMERIZATION 91 3.1 NICKEL- AND PALLADIUM-BASED CATALYSTS 91 3.1.1 DIIMINE COMPLEXES 91 3.1.2 NEUTRAL NICKEL(II) COMPLEXES 94 3.1.3 OTHER NICKEL(II) AND PALLADIUM(II) COMPLEXES 98 3.2 IRON- AND COBALT-BASED CATALYSTS 98 3.2.1 BIS(IMINO)PYRIDYL COMPLEXES 98 3.3 CONCLUSIONS 101 REFERENCES 102 4 EFFECTS OF IMMOBILIZATION OF CATALYSTS FOR OLEFIN POLYMERIZATION 105 4.1 INTRODUCTION 205 4.2 METALLOCENES AND RELATED COMPLEXES 206 4.2.1 IMMOBILIZED MAO/METALLOCENE SYSTEMS 206 4.2.2 IMMOBILIZED BORANE AND BORATE ACTIVATORS 209 4.2.3 SUPERACIDIC SUPPORTS 120 4.2.4 MGCL 2 -SUPPORTED SYSTEMS 220 4.3 OTHER TITANIUM AND ZIRCONIUM COMPLEXES 223 IMAGE 3 CONTENTS VIL 4.3.1 CONSTRAINED GEOMETRY COMPLEXES 113 4.3.2 OCTAHEDRAL COMPLEXES 225 4.4 VANADIUM COMPLEXES 117 4.5 CHROMIUM COMPLEXES 122 4.6 NICKEL COMPLEXES 122 4.7 IRON COMPLEXES 124 4.8 CONCLUSIONS 125 REFERENCES 126 5 DORMANT SPECIES IN TRANSITION METAL-CATALYZED OLEFIN POLYMERIZATION 131 5.1 INTRODUCTION 131 5.2 ZIEGLER-NATTA CATALYSTS 132 5.2.1 ETHENE POLYMERIZATION 132 5.2.2 PROPENE POLYMERIZATION 132 5.3 METALLOCENES AND RELATED EARLY TRANSITION METAL CATALYSTS 134 5.3.1 CATION-ANION INTERACTIONS 134 5.3.2 EFFECTS OF AIME 3 136 5.3.3 EFFECTS OF 2,1-INSERTION IN PROPENE POLYMERIZATION 137 5.3.4 EFFECTS OF R\| 3 -ALLYLIC SPECIES IN PROPENE POLYMERIZATION 140 5.3.5 CHAIN EPIMERIZATION IN PROPENE POLYMERIZATION 141 5.3.6 EFFECTS OF DORMANT SITE FORMATION ON POLYMERIZATION KINETICS 142 5.4 LATE TRANSITION METAL CATALYSTS 243 5.4.1 RESTING STATES IN NICKEL DIIMINE-CATALYZED POLYMERIZATION 243 5.4.2 EFFECTS OF HYDROGEN IN BIS(IMINOPYRIDYL) IRON-CATALYZED POLYMERIZATION 243 5.5 REVERSIBLE CHAIN TRANSFER IN OLEFIN POLYMERIZATION 245 5.6 CONCLUSIONS 147 REFERENCES 248 6 TRANSITION METAL CATALYZED OLEFIN OLIGOMERIZATION 252 6.1 INTRODUCTION 252 6.2 ZIRCONIUM CATALYSTS 252 6.3 TITANIUM CATALYSTS 253 6.4 TANTALUM CATALYSTS 256 6.5 CHROMIUM CATALYSTS 257 6.5.1 CHROMIUM-CATALYZED TRIMERIZATION 157 6.5.2 CHROMIUM-CATALYZED TETRAMERIZATION OF ETHENE 260 6.5.3 CHROMIUM-CATALYZED OLIGOMERIZATION 162 6.5.4 SINGLE-COMPONENT CHROMIUM CATALYSTS 264 6.6 NICKEL CATALYSTS 266 6.7 IRON CATALYSTS 268 IMAGE 4 VIII CONTENTS 6.8 TANDEM CATALYSIS INVOLVING OLIGOMERIZATION AND POLYMERIZATION 270 6.9 CONCLUSIONS 272 REFERENCES 272 7 ASYMMETRIC HYDROGENATION 277 7.1 INTRODUCTION 277 7.2 INCUBATION BY DIENES IN RHODIUM DIENE PRECURSORS 279 7.3 INHIBITION BY SUBSTRATES, SOLVENTS, POLAR ADDITIVES, AND IMPURITIES 282 7.3.1 INHIBITION BY SUBSTRATES: INDIUM 282 7.3.2 INHIBITION BY SUBSTRATES, ADDITIVES: RHODIUM 282 7.3.3 INHIBITION BY SUBSTRATES: RUTHENIUM 287 7.4 INHIBITION BY FORMATION OF BRIDGED SPECIES 190 7.4.1 INHIBITION BY FORMATION OF BRIDGED SPECIES: IRIDIUM 192 7.4.2 INHIBITION BY FORMATION OF BRIDGED SPECIES: RHODIUM 295 7.5 INHIBITION BY LIGAND DECOMPOSITION 298 7.6 INHIBITION BY THE PRODUCT 299 7.6.1 INHIBITION BY THE PRODUCT: RHODIUM 199 7.6.2 RUTHENIUM 200 7.7 INHIBITION BY METAL FORMATION; HETEROGENEOUS CATALYSIS BY METALS 202 7.8 SELECTIVE ACTIVATION AND DEACTIVATION OF ENANTIOMERIC CATALYSTS 204 7.9 CONCLUSIONS 206 REFERENCES 207 8 CARBONYLATION REACTIONS 213 8.1 INTRODUCTION 213 8.2 COBALT-CATALYZED HYDROFORMYLATION 214 8.3 RHODIUM-CATALYZED HYDROFORMYLATION 217 8.3.1 INTRODUCTION OF RHODIUM-CATALYZED HYDROFORMYLATION 217 8.3.2 CATALYST FORMATION 221 8.3.3 INCUBATION BY IMPURITIES: DORMANT SITES 223 8.3.4 DECOMPOSITION OF PHOSPHINES 227 8.3.5 DECOMPOSITION OF PHOSPHITES 231 8.3.6 DECOMPOSITION OF NHCS 235 8.3.7 TWO-PHASE HYDROFORMYLATION 238 8.3.8 HYDROFORMYLATION BY NANOPARTICLE PRECURSORS 244 8.4 PALLADIUM-CATALYZED ALKENE-CO REACTIONS 244 8.4.1 INTRODUCTION 244 8.4.2 BRIEF MECHANISTIC OVERVIEW 246 IMAGE 5 CONTENTS IX 8.4.3 EARLY REPORTS ON DECOMPOSITION AND REACTIVATION 248 8.4.4 COPOLYMERIZATION 250 8.4.5 METHOXY- AND HYDROXY-CARBONYLATION 253 8.5 METHANOL CARBONYLATION 259 8.5.1 INTRODUCTION 259 8.5.2 MECHANISM AND SIDE REACTIONS OF THE MONSANTO RHODIUM-BASED PROCESS 260 8.5.3 THE MECHANISM OF THE ACETIC ANHYDRIDE PROCESS USING RHODIUM AS A CATALYST 262 8.5.4 PHOSPHINE-MODIFIED RHODIUM CATALYSTS 263 8.5.5 IRIDIUM CATALYSTS 265 8.6 CONCLUSIONS 268 REFERENCES 269 9 METAL-CATALYZED CROSS-COUPLING REACTIONS 279 9.1 INTRODUCTION; A FEW HISTORIC NOTES 279 9.2 ON THE MECHANISM OF INITIATION AND PRECURSORS 283 9.2.1 INITIATION VIA OXIDATIVE ADDITION TO PD(0) 283 9.2.2 HYDROCARBYL PD HALIDE INITIATORS 290 9.2.3 METALLATED HYDROCARBYL PD HALIDE INITIATORS 293 9.3 TRANSMETALLATION 299 9.4 REDUCTIVE ELIMINATION 303 9.4.1 MONODENTATE VS BIDENTATE PHOSPHINES AND REDUCTIVE ELIMINATION 303 9.4.2 REDUCTIVE ELIMINATION OF C-F BONDS 313 9.5 PHOSPHINE DECOMPOSITION 326 9.5.1 PHOSPHINE OXIDATION 316 9.5.2 P-C CLEAVAGE OF LIGANDS 317 9.6 METAL IMPURITIES 322 9.7 METAL NANOPARTIDES AND SUPPORTED METAL CATALYSTS 327 9.7.1 SUPPORTED METAL CATALYSTS 327 9.7.2 METAL NANOPARTIDES AS CATALYSTS 330 9.7.3 METAL PRECIPITATION 334 9.8 CONCLUSIONS 334 REFERENCES 335 10 ALKENE METATHESIS 347 10.1 INTRODUCTION 347 10.2 MOLYBDENUM AND TUNGSTEN CATALYSTS 349 10.2.1 DECOMPOSITION ROUTES OF ALKENE METATHESIS CATALYSTS 349 10.2.2 REGENERATION OF ACTIVE ALKYLIDENES SPECIES 356 10.2.3 DECOMPOSITION ROUTES OF ALKYNE METATHESIS CATALYSTS 359 10.3 RHENIUM CATALYSTS 363 10.3.1 INTRODUCTION 363 IMAGE 6 X CONTENTS 10.3.2 CATALYST INITIATION AND DECOMPOSITION 365 10.4 RUTHENIUM CATALYSTS 370 10.4.1 INTRODUCTION 370 10.4.2 INITIATION AND INCUBATION PHENOMENA 371 10.4.3 DECOMPOSITION OF THE ALKYLIDENE FRAGMENT 376 10.4.4 REACTIONS INVOLVING THE NHC LIGAND 379 10.4.5 REACTIONS INVOLVING OXYGENATES 381 10.4.6 TANDEM METATHESIS/HYDROGENATION REACTIONS 385 10.5 CONCLUSIONS 388 REFERENCES 390 INDEX 397
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spellingShingle	Leeuwen, Piet W. N. M. van 1942- Chadwick, John C. 1950- Homogeneous catalysts activity - stability - deactivation Katalysator (DE-588)4029919-3 gnd Homogene Katalyse (DE-588)4160579-2 gnd
subject_GND	(DE-588)4029919-3 (DE-588)4160579-2
title	Homogeneous catalysts activity - stability - deactivation
title_auth	Homogeneous catalysts activity - stability - deactivation
title_exact_search	Homogeneous catalysts activity - stability - deactivation
title_full	Homogeneous catalysts activity - stability - deactivation Piet W. N. M. van Leeuwen and John C. Chadwick
title_fullStr	Homogeneous catalysts activity - stability - deactivation Piet W. N. M. van Leeuwen and John C. Chadwick
title_full_unstemmed	Homogeneous catalysts activity - stability - deactivation Piet W. N. M. van Leeuwen and John C. Chadwick
title_short	Homogeneous catalysts
title_sort	homogeneous catalysts activity stability deactivation
title_sub	activity - stability - deactivation
topic	Katalysator (DE-588)4029919-3 gnd Homogene Katalyse (DE-588)4160579-2 gnd
topic_facet	Katalysator Homogene Katalyse
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Call Number:	0302 CHE 167f 2011 A 5984 Floor plan
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