Spectroscopic methods in organic chemistry: 100 tables
Gespeichert in:
| Beteiligte Personen: | , , |
|---|---|
| Format: | Buch |
| Sprache: | Englisch Deutsch |
| Veröffentlicht: |
Stuttgart [u.a.]
Thieme
2008
|
| Ausgabe: | 2. ed. |
| Schriftenreihe: | Thieme foundations of organic chemistry series
|
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016683693&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Abstract: | This book provides the necessary equipment for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.The following methods are explained and examples given: UV/Vis Spectroscopy, derivative Spectroscopy, chirooptical methods CD and ORD.Aggregated molecules, charge transfer complexes, conjugated oligomers. Infrared (IR) and Raman Spectroscopy, Fourier transform IR spectroscopy, and GC/IRcombination methods. Nuclear Magnetic Resonance Spectroscopy (NMR), 1H-, 13C-, 19F-, 15N- und 31P-NMR, spin decoupling, triple resonance, INDOR difference spectroscopy, 2D- and 3D-NMR, COSY, TOCSY, ROESY and NOESY spectra, NOE, INEPT, and DEPT technique, DEPTQ, HETCOR, HRMAS, INADEQUATE and lanthanide shift reagents, simulation and calculation of spectra, and the combination of separation and NMR methods.The new 2D NMR techniques TOCSY, HMQC and HMBC, more examples and a guide to completely assign all 1H and 13C NMR signals of a given substrate. Mass spectrometry (MS), electron impact and chemical ionization (EI and CI), fast atom bombardment (FAB), electrospray und thermospray ionization (ESI and TSI), MS/MS technique (MSn), field ionization and field desorption (FI and FD), atmospheric pressure chemical ionization (APCI), MALDI TOF technique, GC/MS, LC/MS, and HPLC-UV(DAD)-APCI combination MS/MS technique. Fourier transform ion cyclotron resonance MS (FT-ICR-MS).The layout and manytables help to introduce the reader to spectroscopy. The extensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher course in practical spectroscopy. |
| Umfang: | IX, 453 S. zahlr. graph. Darst. |
| ISBN: | 9783131060426 9781588904881 |
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| 240 | 1 | 0 | |a Spektroskopische Methoden in der organischen Chemie |
| 245 | 1 | 0 | |a Spectroscopic methods in organic chemistry |b 100 tables |c Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a Stuttgart [u.a.] |b Thieme |c 2008 | |
| 300 | |a IX, 453 S. |b zahlr. graph. Darst. | ||
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| 490 | 0 | |a Thieme foundations of organic chemistry series | |
| 520 | 3 | |a This book provides the necessary equipment for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.The following methods are explained and examples given: UV/Vis Spectroscopy, derivative Spectroscopy, chirooptical methods CD and ORD.Aggregated molecules, charge transfer complexes, conjugated oligomers. Infrared (IR) and Raman Spectroscopy, Fourier transform IR spectroscopy, and GC/IRcombination methods. Nuclear Magnetic Resonance Spectroscopy (NMR), 1H-, 13C-, 19F-, 15N- und 31P-NMR, spin decoupling, triple resonance, INDOR difference spectroscopy, 2D- and 3D-NMR, COSY, TOCSY, ROESY and NOESY spectra, NOE, INEPT, and DEPT technique, DEPTQ, HETCOR, HRMAS, INADEQUATE and lanthanide shift reagents, simulation and calculation of spectra, and the combination of separation and NMR methods.The new 2D NMR techniques TOCSY, HMQC and HMBC, more examples and a guide to completely assign all 1H and 13C NMR signals of a given substrate. Mass spectrometry (MS), electron impact and chemical ionization (EI and CI), fast atom bombardment (FAB), electrospray und thermospray ionization (ESI and TSI), MS/MS technique (MSn), field ionization and field desorption (FI and FD), atmospheric pressure chemical ionization (APCI), MALDI TOF technique, GC/MS, LC/MS, and HPLC-UV(DAD)-APCI combination MS/MS technique. Fourier transform ion cyclotron resonance MS (FT-ICR-MS).The layout and manytables help to introduce the reader to spectroscopy. The extensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher course in practical spectroscopy. | |
| 650 | 4 | |a Organische Chemie - Spektroskopie - Lehrbuch | |
| 650 | 4 | |a Spectrum analysis | |
| 650 | 4 | |a Organic compounds |x Analysis | |
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Datensatz im Suchindex
| DE-BY-TUM_call_number | 0303 CHE 236f 2009 L 499(2) |
|---|---|
| DE-BY-TUM_katkey | 1667816 |
| DE-BY-TUM_location | 03 |
| DE-BY-TUM_media_number | 040071313583 040071313618 040071313561 040071313594 040071313607 |
| _version_ | 1821933603844521984 |
| adam_text |
Contents
1 UV/Vis Spectroscopy 7
H. Meier
1 Theoretical Introduction. 1
1.1 Electronic Transitions . 1
1.2 Light Absorption and the Spectrum . 4
2 Sample Preparation and Measurement
of Spectra . 7
3 Chromophores . 9
3.1 Individual Chromophoric Croups and their
Interactions . 9
3.2 Olefins, Polyenes . 10
3.3 Benzene and Benzenoid Aromatics . 14
3.4 Carbonyl Compounds . 17
3.5 Conjugated Oligomers and Polymers . 20
3.6 Aggregated Molecules, Charge-Transfer
Complexes . 23
4 Applications of UV/Vis Spectroscopy . 24
5 Derivative Spectroscopy . 26
6 Chirooptical Methods . 27
Supplementary Literature . 32
2 Infrared and Raman Spectroscopy 33
B. Zeeh
1 Introduction. 33
2 Basic Principles and Selection Rules . 34
3 IR Spectrometers . 36
3.1 Classical (scanning) IR spectrometers . 36
3.2 Fourier-Transform IR Spectrometers . 37
3.3 Coupled Techniques . 38
4 Sample Preparation . 38
4.1 Measurements in the Cas Phase . 39
4.2 Measurements on Liquids . 39
4.3 Measurements in Solution. 39
4.4 Measurements in the Solid State . 39
5 ThelRSpectrum . 40
6 Overview of Characteristic Absorptions . 44
7 IR Absorptions of Single Bonds
to Hydrogen . 48
7.1 (C—H) Absorptions. 48
7.2 (O—H) and (N—H) Absorptions . 49
8 IR Absorptions of Triple Bonds
and Cumulated Double Bonds . 51
9 IR Absorptions of Double Bonds . 52
10 Typical IR Absorptions of Aromatic
Compounds . 56
11 IR Absorptions in the Fingerprint
Region . 57
12 Examples of IR-Spectra . 59
13 Information Technology as an Aid
to IR Spectroscopy . 68
14 Quantitative IR Spectroscopy. 68
15 Raman Spectroscopy . 69
15.1 The Raman Effect . 69
15.2 Selection Rules . 70
15.3 Raman Spectrometers . 71
15.4 Applications . 72
Literature. 73
3 Nuclear Magnetic Resonance Spectroscopy 74
H. Meier
1. Physical Principles. 74
1.1 The Resonance Phenomenon . 74
1.2 Chemical Shift . 76
1.3 Spin-Spin Coupling . 77
1.4 Line Widths . 85
1.5 Intensity . 87
2. NMR Spectra and Molecular Structure. 89
2.1 Molecules with "Rigid" Atomic Positions . 89
2.2 Intramolecular Motion . 91
2.3 Chemical Exchange Processes . 99
3. 'H NMRSpectroscopy .104
3.1 Sample Preparation and Measurement
of Spectra (CW and PFT Techniques). 104
3.2 'H Chemical Shifts. 107
3.3. ]H-'HCoupling . 111
3.4 Coupling to Other Nuclei . 118
3.5 Correlation of] H Shifts with Structural
Features. 118
3.6 Increment Systems for Estimating 1H Shifts.120
3.7 1H NMR Data of Representatives of the
Commoner Classes of Compounds. 120
3.8 Specialised Techniques . 120
4. 13C NMR spectroscopy .152
4.1 Sample Preparation and Measurement
of Spectra . 152
4.2 13C Chemical Shifts . 155
4.3 13C,'H Couplings . 159
4.4 Coupling of 13C to Other Nuclei (D,F,N,P) . 160
4.5 13C.13C Couplings . 163
4.6 Correlation of 13C Shifts with Structural
Features . 168
4.7 Increment Systems for the Estimation
of '3C Shifts. 168
4.8 Special Methods . 173
5 Combination of 'Hand' 3C NMR
Spectroscopy .199
5.1 Complete Assignment of'H and nCNMR
Signals . 199
5.2 Use of Databases .201
5.3 ^and nC NMR Data of representatives of the
most important Classes of Compounds'1 .205
6 NMR of other Nuclei .226
6.1 I9F NMR Spectroscopy .226
6.2 31P NMR Spectroscopy .228
6.3 !5N NMR Spectroscopy.232
6.4 Other Nuclei .238
4 Mass Spectra
M. Hesse
1 Introduction .
242
Instrumentation and the Recording
of Spectra .
242
243
2.1 The Principle of the Mass Spectrometer .243
3 Fragmentation of Organic Compounds .245
4 The Main Fragmentation Reactions
of Organic Compounds .250
4.1 a-Cleavage .250
4.2 Benzyl- and Allyl-Cleavage.255
4.3 The Cleavage of "Non-Activated" Bonds .257
4.4 The Retro Diels-Alder Reaction (RDA Reaction) . 260
4.5 The McLafferty Rearrangement .263
4.6 The Onium Reaction.264
4.7 Loss of CO .267
5 Thermal Reactions in the Mass
Spectrometer.270
5.1 The Most Important Types of Thermal
Reactions5.270
5.2 Recognition of Thermal Reactions .274
5.3 Prevention of Thermal Reactions in the Mass
Spectrometer .275
6 Mass Spectra of Contaminated Samples
and Mixtures .275
6.1 Solvents .276
6.2 Foreign Substances in Solvents.276
6.3 Foreign Substances in Reagents .277
6.4 Materials from Laboratory Apparatus .277
6.5 Contaminants from Thin-Layer
Chromatography Plates .277
7. Isotopic Labelling Reactions.278
7.1 H/D Exchange Reactions .278
7.2 Transformations of Functional Croups
under Deuterating Conditions .280
7.3 Determination of the Degree of Labelling .280
8 Additional lonisation Methods . 282
8.1 lonisation Methods . 282
8.2 Atmospheric Pressure Chemical
lonisation (APCI) . 283
8.3 Chemical lonisation (Cl) . 283
8.4 Direct Chemical lonisation (DCI) . 289
8.5 Electrospray lonisation (ESI) . 289
8.6 Fast Atom Bombardment (FAB) . 290
8.7 Field Desorption (FD) . 293
8.8 Field lonisation (Fl) . 293
8.9 Cation Addition Mass Spectroscopy . 294
8.10 Laser Desorption/lonisation Mass
Spectrometry (LDI). 294
8.11 MALDI . 294
8.12 Photoionisation (PI) . 297
8.13 Secondary Ion Mass Spectrometry (SIMS) . 297
8.14 Thermal Desorption Mass
Spectrometry (TD) .298
8.15 The Thermospray lonisation Procedure28
(TSI) .298
9 Other Aspects of Mass Spectrometry
and Terminology.298
9.1 Fourier Transform Ion Cyclotron Resonance Mass
Spectrometry .298
9.2 Field lonisation Kinetics (FIK) .299
9.3 Measurement of High Masses.301
9.4 Ion Trap Spectrometer .303
9.5 The Coupling of other Instruments
to Mass Spectrometers .303
9.6 Multiply Charged Ions .308
9.7 The Memory Effect .309
9.8 Neighbouring Croup Participation
Reactions .309
9.9 Quadrupole Mass Analysers .313
9.10 Spectral Libraries.314
9.11 Stereoisomers .316
9.12 Collision Activation (CA) .316
9.13 Tandem Mass Spectrometry .317
9.14 Metastable Signals .319
10 Tables for Use in Mass Spectrometry .320
10.1 List of Frequently Occurring Ions and
Characteristic Mass Differences Resulting from Mass
Spectrometric and Chemical
Reactions .320
10.2 Mass Differences Between the Reactant and
Product of Frequently used Chemical
Reactions .333
10.3 Isotopic ratios in compounds containing
ClandBr .335
10.4 Mass spectra of solvents .338
10.5 Mass spectra of common impurities .342
10.6 Mass Numbers and Abundances of the Isotopes
of Naturally Occurring Elements .345
Literature .348
5 Combined Examples 355
Introduction .355
Examples 1-14. 355-391
Solutions for the Example 1-14 . 397-419 |
| any_adam_object | 1 |
| author | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd |
| author_GND | (DE-588)101805281X (DE-588)13810817X |
| author_facet | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd |
| author_role | aut aut aut |
| author_sort | Hesse, Manfred 1935-2011 |
| author_variant | m h mh h m hm b z bz |
| building | Verbundindex |
| bvnumber | BV035014501 |
| callnumber-first | Q - Science |
| callnumber-label | QD272 |
| callnumber-raw | QD272.S6 |
| callnumber-search | QD272.S6 |
| callnumber-sort | QD 3272 S6 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 8901 VG 8930 VK 5661 |
| classification_tum | CHE 236f |
| ctrlnum | (OCoLC)255188005 (DE-599)DNB976685183 |
| dewey-full | 543.5 547.30858 540 543.17 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry 547 - Organic chemistry 540 - Chemistry and allied sciences |
| dewey-raw | 543.5 547.30858 540 543.17 |
| dewey-search | 543.5 547.30858 540 543.17 |
| dewey-sort | 3543.5 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 2. ed. |
| format | Book |
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Infrared (IR) and Raman Spectroscopy, Fourier transform IR spectroscopy, and GC/IRcombination methods. Nuclear Magnetic Resonance Spectroscopy (NMR), 1H-, 13C-, 19F-, 15N- und 31P-NMR, spin decoupling, triple resonance, INDOR difference spectroscopy, 2D- and 3D-NMR, COSY, TOCSY, ROESY and NOESY spectra, NOE, INEPT, and DEPT technique, DEPTQ, HETCOR, HRMAS, INADEQUATE and lanthanide shift reagents, simulation and calculation of spectra, and the combination of separation and NMR methods.The new 2D NMR techniques TOCSY, HMQC and HMBC, more examples and a guide to completely assign all 1H and 13C NMR signals of a given substrate. Mass spectrometry (MS), electron impact and chemical ionization (EI and CI), fast atom bombardment (FAB), electrospray und thermospray ionization (ESI and TSI), MS/MS technique (MSn), field ionization and field desorption (FI and FD), atmospheric pressure chemical ionization (APCI), MALDI TOF technique, GC/MS, LC/MS, and HPLC-UV(DAD)-APCI combination MS/MS technique. Fourier transform ion cyclotron resonance MS (FT-ICR-MS).The layout and manytables help to introduce the reader to spectroscopy. The extensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher course in practical spectroscopy.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Organische Chemie - Spektroskopie - Lehrbuch</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Spectrum analysis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Organic compounds</subfield><subfield code="x">Analysis</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Organische Verbindungen</subfield><subfield code="0">(DE-588)4043816-8</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Organische Chemie</subfield><subfield code="0">(DE-588)4043793-0</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Spektroskopie</subfield><subfield code="0">(DE-588)4056138-0</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4123623-3</subfield><subfield code="a">Lehrbuch</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Organische Chemie</subfield><subfield code="0">(DE-588)4043793-0</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Spektroskopie</subfield><subfield code="0">(DE-588)4056138-0</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="8">1\p</subfield><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Organische Verbindungen</subfield><subfield code="0">(DE-588)4043816-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Spektroskopie</subfield><subfield code="0">(DE-588)4056138-0</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="8">2\p</subfield><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Meier, Herbert</subfield><subfield code="d">1939-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)13810817X</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zeeh, Bernd</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">HBZ Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016683693&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="883" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="a">cgwrk</subfield><subfield code="d">20201028</subfield><subfield code="q">DE-101</subfield><subfield code="u">https://d-nb.info/provenance/plan#cgwrk</subfield></datafield><datafield tag="883" ind1="1" ind2=" "><subfield code="8">2\p</subfield><subfield code="a">cgwrk</subfield><subfield code="d">20201028</subfield><subfield code="q">DE-101</subfield><subfield code="u">https://d-nb.info/provenance/plan#cgwrk</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-016683693</subfield></datafield></record></collection> |
| genre | (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV035014501 |
| illustrated | Illustrated |
| indexdate | 2025-01-11T10:41:27Z |
| institution | BVB |
| isbn | 9783131060426 9781588904881 |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016683693 |
| oclc_num | 255188005 |
| open_access_boolean | |
| owner | DE-703 DE-91G DE-BY-TUM DE-1046 DE-11 |
| owner_facet | DE-703 DE-91G DE-BY-TUM DE-1046 DE-11 |
| physical | IX, 453 S. zahlr. graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | Thieme |
| record_format | marc |
| series2 | Thieme foundations of organic chemistry series |
| spellingShingle | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd Spectroscopic methods in organic chemistry 100 tables Organische Chemie - Spektroskopie - Lehrbuch Spectrum analysis Organic compounds Analysis Organische Verbindungen (DE-588)4043816-8 gnd Organische Chemie (DE-588)4043793-0 gnd Spektroskopie (DE-588)4056138-0 gnd |
| subject_GND | (DE-588)4043816-8 (DE-588)4043793-0 (DE-588)4056138-0 (DE-588)4123623-3 |
| title | Spectroscopic methods in organic chemistry 100 tables |
| title_alt | Spektroskopische Methoden in der organischen Chemie |
| title_auth | Spectroscopic methods in organic chemistry 100 tables |
| title_exact_search | Spectroscopic methods in organic chemistry 100 tables |
| title_full | Spectroscopic methods in organic chemistry 100 tables Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_fullStr | Spectroscopic methods in organic chemistry 100 tables Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_full_unstemmed | Spectroscopic methods in organic chemistry 100 tables Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_short | Spectroscopic methods in organic chemistry |
| title_sort | spectroscopic methods in organic chemistry 100 tables |
| title_sub | 100 tables |
| topic | Organische Chemie - Spektroskopie - Lehrbuch Spectrum analysis Organic compounds Analysis Organische Verbindungen (DE-588)4043816-8 gnd Organische Chemie (DE-588)4043793-0 gnd Spektroskopie (DE-588)4056138-0 gnd |
| topic_facet | Organische Chemie - Spektroskopie - Lehrbuch Spectrum analysis Organic compounds Analysis Organische Verbindungen Organische Chemie Spektroskopie Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016683693&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hessemanfred spektroskopischemethodeninderorganischenchemie AT meierherbert spektroskopischemethodeninderorganischenchemie AT zeehbernd spektroskopischemethodeninderorganischenchemie AT hessemanfred spectroscopicmethodsinorganicchemistry100tables AT meierherbert spectroscopicmethodsinorganicchemistry100tables AT zeehbernd spectroscopicmethodsinorganicchemistry100tables |
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Teilbibliothek Chemie, Lehrbuchsammlung
| Signatur: |
0303 CHE 236f 2009 L 499(2) Lageplan |
|---|---|
| Exemplar 1 | Ausleihbar Am Standort |
| Exemplar 2 | Ausleihbar Am Standort |
| Exemplar 3 | Ausleihbar Am Standort |
| Exemplar 4 | Ausleihbar Am Standort |
| Exemplar 5 | Ausleihbar Am Standort |