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Columns for gas chromatography: performance and selection

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Bibliographic Details
Main Authors:	Barry, Eugene F. (Author), Grob, Robert Lee 1927- (Author)
Format:	Book
Language:	English
Published:	Hoboken, N.J. Wiley-Interscience 2007
Subjects:	Gas chromatography Chromatographiesäule Gaschromatographie
Links:	http://www.loc.gov/catdir/toc/ecip0619/2006026963.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015655783&sequence=000004&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Item Description:	Includes index.
Physical Description:	XIII, 298 S. Ill., graph. Darst.
ISBN:	9780471740438

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Record in the Search Index

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adam_text	CONTENTS Preface xi Acknowledgments xiii 1 Introduction 1 1.1 Evolution of Gas Chromatographie Columns 1 1.2 Central Role Played by the Column 6 1.3 Justification for Column Selection and Care 8 1.4 Literature on Gas Chromatographie Columns 11 1.5 Gas Chromatographie Resources on the Internet 12 References 13 2 Packed Column Gas Chromatography 15 2.1 Introduction 15 2.2 Solid Supports and Adsorbents 15 Supports for Gas-Liquid Chromatography 15 Adsorbents for Gas-Solid Chromatography 22 2.3 Stationary Phases 33 Requirements of a Stationary Phase 33 USP Designation of Stationary Phases 36 Kovats Retention Index 36 McReynolds and Rohrschneider Classifications of Stationary Phases 41 Evaluation of Column Operation 45 Optimization of Packed Column Separations 53 2.4 Column Preparation 54 Coating Methods 56 Tubing Materials and Dimensions 56 Glass Wool Plugs and Column Fittings 57 Filling the Column 58 Conditioning the Column and Column Care 59 2.5 United States Pharmacopeia and National Formulary Chromatographie Methods 60 References 91 vii viii CONTENTS 3 Capillary Column Gas Chromatography 94 3.1 Introduction 94 Significance and Impact of Capillary Gas Chromatography 94 Chronology of Achievements in Capillary Gas Chromatography 95 Comparison of Packed and Capillary Columns 98 3.2 Capillary Column Technology 100 Capillary Column Materials 100 Fused Silica and Other Glasses 100 Extrusion of a Fused-Silica Capillary Column 103 Aluminum-Clad Fused-Silica Capillary Columns 106 Fused-Silica-Lined Stainless Steel Capillary Columns 106 3.3 Preparation of Fused-Silica Capillary Columns 110 Silanol Deactivation Procedures 110 Static Coating of Capillary Columns 116 Capillary Cages 116 Test Mixtures for Monitoring Column Performance 117 Diagnostic Role Played by Components of Test Mixtures 119 3.4 Chromatographie Performance of Capillary Columns 122 Golay Equation Versus the van Deemter Expression 122 Choice of Carrier Gas 124 Measurement of Linear Velocity and Flow Rate 126 Effect of Carrier Gas Viscosity on Linear Velocity 127 Phase Ratio 129 Coating Efficiency 132 3.5 Stationary-Phase Selection for Capillary Gas Chromatography 132 Requirements 132 History 132 Comparison of Columns from Manufacturers 134 Polysiloxane Phases 140 Polyethylene Glycol Phases 141 Cross-Linked Versus Chemically Bonded Phase 142 Chemical Bonding 149 MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases 150 Sol-Gel Stationary Phases 150 Phenylpolycarborane-Siloxane Phases 151 3.6 Specialty Columns 153 s EPA Methods 153 CONTENTS ix Chiral Stationary Phases 153 Gas-Solid Adsorption Capillary Columns: PLOT Columns 156 3.7 Capillary Column Selection 159 Practical Considerations of Column Diameter, Film Thickness, and Column Length 159 Capillary Columns of 0.53 mm i.d.: Megabore Columns 165 Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation 167 Column Selection for Gas Chromatography by Specifications 172 3.8 Column Installation and Care 186 Carrier Gas Purifiers 186 Ferrule Materials and Fittings 187 Column Installation 191 Column Conditioning 192 Column Bleed 194 Retention Gap and Guard Columns 196 Column Fatigue and Regeneration 200 3.9 Special Gas Chromatographie Techniques 200 Simulated Distillation 200 Multidimensional Gas Chromatography 201 Computer Modeling of Stationary Phases 203 References 204 4 Column Oven Temperature Control 210 4.1 Thermal Performance Variables and Electronic Considerations 210 4.2 Advantages of Temperature Programming over Isothermal Operation 211 4.3 Oven Temperature Profiles for Programmed-Temperature Gas Chromatography 212 4.4 Role of Computer Assistance in Optimizing Separations in Gas Chromatography 214 DryLab (LC Resources) 214 ProezGC (Restek Corporation) 215 GC-SOS (Chem SW) 216 4.5 Fast or High-Speed Gas Chromatography 217 Selectivity Tuning 219 Resistively Heated Columns and Column Jackets 223 4.6 Subambient Oven Temperature Control 228 References 229 X CONTENTS Selected References 230 Appendix A: Guide to Selection of Packed Columns 232 Appendix B: Column Selection 277 Index 281
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spellingShingle	Barry, Eugene F. Grob, Robert Lee 1927- Columns for gas chromatography performance and selection Gas chromatography Chromatographiesäule (DE-588)4290388-9 gnd Gaschromatographie (DE-588)4019330-5 gnd
subject_GND	(DE-588)4290388-9 (DE-588)4019330-5
title	Columns for gas chromatography performance and selection
title_auth	Columns for gas chromatography performance and selection
title_exact_search	Columns for gas chromatography performance and selection
title_full	Columns for gas chromatography performance and selection Eugene F. Barry ; Robert L. Grob
title_fullStr	Columns for gas chromatography performance and selection Eugene F. Barry ; Robert L. Grob
title_full_unstemmed	Columns for gas chromatography performance and selection Eugene F. Barry ; Robert L. Grob
title_short	Columns for gas chromatography
title_sort	columns for gas chromatography performance and selection
title_sub	performance and selection
topic	Gas chromatography Chromatographiesäule (DE-588)4290388-9 gnd Gaschromatographie (DE-588)4019330-5 gnd
topic_facet	Gas chromatography Chromatographiesäule Gaschromatographie
url	http://www.loc.gov/catdir/toc/ecip0619/2006026963.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015655783&sequence=000004&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT barryeugenef columnsforgaschromatographyperformanceandselection AT grobrobertlee columnsforgaschromatographyperformanceandselection

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Call Number:	0302 CHE 234f 2007 A 6511 Floor plan
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