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Dendritic molecules: concepts, synthesis, perspectives

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Bibliographic Details
Main Authors:	Newkome, George R. 1938- (Author), Moorefield, Charles N. (Author), Vögtle, Fritz 1939- (Author)
Format:	Book
Language:	German
Published:	Weinheim [u.a.] VCH 1996
Subjects:	Dendrimeren Macromoleculen Structuur-activiteit-relatie Synthese (chemie) Macromolecular Substances Macromolecules Molecular Structure Molecular structure Sternpolymere
Links:	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007246411&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Physical Description:	XI, 261 S. Ill., zahlr. Darst.
ISBN:	3527293256

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Record in the Search Index

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adam_text	G.R. NEWKOME, C.N. MOOREFIELD, F. VOEGTLE DENDRITIC MOLECULES CONCEPTS * SYNTHESES * PERSPECTIVES WEINHEIM * NEW YORK * BASEL * CAMBRIDGE * TOKYO CONTENTS PROLOGUE AND ACKNOWLEDGMENTS V CONTENTS VII 1 MASSES, SIZES, AND SHAPES OF MACROMOLECULES FROM MULTIFUNCTIONAL MONOMERS 1.1 INTRODUCTION 1 1.2 MOLECULAR MASS AND CHAIN CONNECTIVITY IN MACROMOLECULES 1 1.2.1 DISTRIBUTION WITH LINEAR CHAINS 1 1.2.2 BRANCHED STRUCTURES AND GELATION WITH MULTIFUNCTIONAL MONOMERS 2 1.2.3 BRANCHING WITHOUT NETWORK FORMATION 3 1.3 OVERALL EXTENSION IN SPACE: MOLECULAR SIZES 4 1.3.1 RADIUS OF GYRATION 4 1.3.1.1 LINEAR CHAINS 5 1.3.1.2 MACROCYCLES 6 1.3.1.3 BRANCHED MACROMOLECULES 6 1.3.2 BREADTH OF THE DISTRIBUTION FOR THE SQUARED RADIUS OF GYRATION 7 1.4 SHAPE ANALYSIS FROM THE RADIUS OF GYRATION TENSOR 7 1.4.1 PRINCIPAL MOMENTS 8 1.4.2 ASPHERICITY, ACYLINDRICITY, AND RELATIVE SHAPE ANISOTROPY 9 1.5 APPROACH TO THE GLOBULAR STATE 9 1.5.1 COLLAPSE OF A LINEAR CHAIN 10 1.5.2 SHAPES FROM THE SIMULATIONS OF DENDRIMERS 10 1.6 REFERENCES 12 2 FROM THEORY TO PRACTICE: HISTORICAL PERSPECTIVES 2.1 INTRODUCTION 15 2.2 BRANCHED ARCHITECTURES 15 2.2.1 EARLY OBSERVATIONS 16 2.2.2 PRELUDE TO PRACTICE 17 2.2.3 INCIPIENT MACROMOLECULAR PROGRESSION 19 2.2.3.1 INITIAL CONCEPT AND PRACTICE 19 2.2.3.2 IMPLIED DENDRITIC CONSTRUCTION 19 2.2.3.3 ALTERNATIVE ARCHITECTURES 21 2.3 THE FRACTAL GEOMETRY OF MACROMOLECULES 24 2.3.1 INTRODUCTION 24 2.3.2 FRACTAL GEOMETRY 24 2.3.2.1 SELF-SIMILARITY OR SCALE-INVARIANCE 24 2.3.2.2 FRACTAL DIMENSION (D) 24 2.3.3 APPLIED FRACTAL GEOMETRY 25 2.3.3.1 FRACTALS IN CHEMISTRY 25 2.3.3.2 FRACTALS IN BIOLOGY 27 2.3.3.3 SOLVENT ACCESSIBLE SURFACE AREA (A S AS) 28 2.3.3.4 DENDRITIC FRACTALITY 30 2.3.4 FRACTAL SUMMATION 34 2.4 REFERENCES 34 3 NOMENCLATURE 3.1 BACKGROUND ONTRIVAL AND TRADITIONAL NAMES 37 3.2 DEFINITION OF A CASCADE POLYMER 37 3.3 PROPOSED CASCADE NOMENCLATURE RULES 38 3.4 GENERAL PATTERNS 39 VIII CONTENTS 3.4.1 SIMILAR REPEAT INTERNAL UNITS 39 3.4.2 SIMILAR ARMS WITH DISSIMILAR INTERNAL UNITS 41 3.4.3 DISSIMILAR ARMS WITH SIMILAR INTERNAL BRANCHES 42 3.4.4 DISSIMILAR ARMS WITH DISSIMILAR INTERNAL BRANCHES OR TERMINAL GROUPS 42 3.4.5 UNSYMMETRICALLY BRANCHED CASCADES 44 3.5 FRACTAL NOTATION 45 3.5.1 GENERAL RULES FOR THE PROPOSED FRACTAL NOTATION 45 3.5.2 EXAMPLES USING THE FRACTAL RULES 46 3.6 REFERENCES 46 4 SYNTHETIC METHODOLOGIES: DIVERGENT PROCEDURES 4.1 GENERAL CONCEPTS 49 4.2 EARLY PROCEDURES 49 4.3 1 - 2 IV-BRANCHED 52 4.3.1 1 -* 2 N-BRANCHED AND CONNECTIVITY 52 4.3.2 1 * 2 YV-BRANCHED, AMIDE CONNECTIVITY 56 4.4 1 * 2YLRY/-BRANCHED, AMIDE CONNECTIVITY 61 4.5 1 * » 2ARY/-BRANCHED, ESTER CONNECTIVITY 62 4.6 1 -» 2 C-BRANCHED 63 4.6.1 1 -* 2 C-BRANCHED, AMIDE CONNECTIVITY 63 4.6.2 1 * 2 C-BRANCHED AND CONNECTIVITY 64 4.7 1 * 2 C & ARY/-BRANCHED AND CONNECTIVITY 69 4.8 1 * 2^4RV/-BRANCHED, N-CONNECTIVITY 70 4.9 1 » 2 ETHANO-BRANCHED, ETHER CONNECTIVITY 70 4.10 1 2 57-BRANCHED AND CONNECTIVITY 71 4.11 1 * 2 F-BRANCHED AND CONNECTIVITY 76 4.12 1 - 3 C-BRANCHED 78 4.12.1 1 * 3 C-BRANCHED, AMIDE CONNECTIVITY 78 4.12.1.1 1 * 3 C-BRANCHED, AMIDE ( TRIS ) CONNECTIVITY 78 4.12.1.2 1 - 3 (1 -» 2) C-BRANCHED, AMJDE ( TRIS ) CONNECTIVITY 82 4.12.1.3 1 * 3 C-BRANCHED, AMIDE ( BIS/ZOMOTRIS ) CONNECTIVITY 83 4.12.1.4 L-»3 C-BRANCHED, AMWE ( BEHERA S AMINE ) CONNECTIVITY 84 4.12.2 1 - 3 C-BRANCHED AND CONNECTIVITY 88 4.12.3 1 - 3 C-BRANCHED, RAEER CONNECTIVITY 90 4.12.4 1 * » 3 C-BRANCHED, SS/JER & AMIDE CONNECTIVITY 91 4.13 1 * 3 IV-BRANCHED AND CONNECTIVITY 94 4.14 1 * 3 P-BRANCHED AND CONNECTIVITY 95 4.15 1 * 3 5/-BRANCHED AND CONNECTIVITY 96 4.16 1 * 3 ADAMANTANE-BRANCHED, ESTER CONNECTIVITY 100 4.17 REFERENCES 101 5 SYNTHETIC METHODOLOGIES: CONVERGENT PROCEDURES 5.1 GENERAL CONCEPTS 107 5.2 1 - 2 C-BRANCHED 108 5.2.1 1 * 2 C-BRANCHED AND CONNECTIVITY 108 5.2.2 1 * 2 C-BRANCHED, ETHER CONNECTIVITY 110 5.3 1 * 2 ETHANO-BRANCHED, PHOSPHATE CONNECTIVITY 112 5.4 1 - 2,4RY/-BRANCRIED 112 5.4.1 1 * » 2 Y4RY/-BRANCHED AND CONNECTIVITY 112 5.4.2 1 * 2ARY/-BRANCHED, ETHER CONNECTIVITY 118 5.4.3 1 * 2 ARY/-BRANCHED, AMIDE CONNECTIVITY 129 5.4.4 1 * » 2 ARY/-BRANCHED, ETHER AND AMIDE CONNECTIVITY 131 5.4.5 1 * 2Y4RY/-BRANCHED, ETHER AND URETHANE CONNECTIVITY 136 5.4.6 1 * » 2ARY/-BRANCHED, &TER CONNECTIVITY 138 5.4.7 1 * 2/4RY/-BRANCHED, II^ER AND ESTER CONNECTIVITY 143 5.4.8 1 * 2 ARY /-BRANCHED, ETHER AND KETONE CONNECTIVITY 145 CONTENTS IX 5.4.9 1 * » 2/LRY/-BRANCHED, ETHYNE CONNECTIVITY 145 5.5 1 - 2 N-BRANCHED 157 5.5.1 1 * 2 A -BRANCHED, AMIDE CONNECTIVITY 157 5.6 1 - 2 C- & N-BRANCHED, FCTER CONNECTIVITY 159 5.7 1 » 2 SZ -BRANCHED, SILYLOXY CONNECTIVITY 159 5.8 REFERENCES 161 6 SYNTHETIC METHODOLOGIES: ONE-STEP (HYPERBRANCHED) PROCEDURES 6.1 GENERAL CONCEPTS 165 6.2 1 - 2 ARY/-BRANCHED 165 6.2.1 1 * 2^4RY/-BRANCHED AND CONNECTIVITY 165 6.2.2 1 * * 2 ARY/-BRANCHED, ESTER CONNECTIVITY 167 6.2.3 1 * 2/LRY/-BRANCHED, ETHER CONNECTIVITY 169 6.2.4 1 » 2/LRY/-BRANCHED, /ZER AND KETONE CONNECTIVITY 169 6.2.5 1 2/LRY/-BRANCHED, AMIDE CONNECTIVITY 169 6.2.6 1 -» 2 ARY/-BRANCHED, CARBAMATE CONNECTIVITY 172 6.2.7 1 * 2 ARY/-BRANCHED, URETHANE CONNECTIVITY 174 6.2.8 1 * 2ARY/-BRANCHED, ETHER AND ESTER CONNECTIVITY 174 6.3 1 - 2 C-BRANCHED 175 6.3.1 1 * 2 C-BRANCHED, ESTER CONNECTIVITY 175 6.3.2 1 * 2 C-BRANCHED, T/W CONNECTIVITY 177 6.3.3 1 * 2 C-BRANCHED, AMIDE CONNECTIVITY 178 6.3.4 1 - 2 ARY/-BRANCHED, C-CONNECTIVITY 179 6.3.5 1 » 2 A -BRANCHED AND CONNECTIVITY 179 6.4 1 » 3 GE-BRANCHED AND CONNECTIVITY 179 6.5 1 -» 3 (2)SI-BRANCHED AND CONNECTIVITY 180 6.6 REFERENCES 181 7 CHIRAL DENDRITIC MACROMOLECULES 7.1 DIVERGENT PROCEDURES TO CHIRAL DENDRIMERSS 182 7.1.1 1 -» 3 C-BRANCHED, ETHER AND AMIDE CONNECTIVITY 183 7.1.2 1 -» 2 C-BRANCHED 183 7.1.3 1 * 2Y4RY/-BRANCHED, ESTER AND AMIDE CONNECTIVITY 187 7.1.4 1 * » 2 ARY/-BRANCHED, ETHER AND ESTER CONNECTIVITY 187 7.1.5 1 -» 2 N-BRANCHED AND CONNECTIVITY 187 7.1.6 1 * 2 N-BRANCHED, AMZUEFE-CONNECTIVITY 188 7.2 CONVERGENT PROCEDURES TO CHIRAL DENDRIMERS 192 7.2.1 1 - 2 ARY/-BRANCHED, ETHER CONNECTIVITY 192 7.2.2 1 *» 2 C-BRANCHED, AMIDE CONNECTIVITY 192 7.2.3 1 - 2ARY/-BRANCHED, EZTZER CONNECTIVITY 196 7.2.4 1 -» 3 P- ANDARY/-BRANCHED, P- AND Z7ZER-CONNECTIVITY 198 7.3 REFERENCES 199 8 DENDRIMERS CONTAINING METAL SITES 8.1 METALS AS BRANCHING CENTERS 201 8.2 METALS AS BUILDING BLOCK CONNECTORS 204 8.3 METAL CENTERS AS TERMINATION GROUPS (SURFACE FUNCTIONALIZATION) 209 8.4 METALS AS TRANSFORMATION AUXILIARIES 219 8.4.1 SITE-SPECIFIC METAL INCLUSION 219 8.4.2 RANDOM METAL INCLUSION 219 8.5 REFERENCES 221 X CONTENTS 9 DENDRITIC NETWORKS 9.1 INTRODUCTION: DENDRITIC ASSEMBLIES 223 9.2 NETWORK FORMATION AND CLASSIFICATION 225 9.2.1 ORDERED VERSUS RANDOM 225 9.2.1.1 METHODS OF FORMATION 225 9.2.1.2 COVALENT AND NON-COVALENT POSITIONING 227 9.3 RANDOM CONNECTIVITY 227 9.3.1 RANDOM, COVALENTLY-LINKED DENDRIMER NETWORKS 227 9.3.2 COUPLING VIA SURFACE-TO-SURFACE INTERACTION 228 9.3.3 COUPLING VIA SURFACE-TO-SURFACE BRIDGING UNITS 229 9.4 ORDERED DENDRITIC NETWORKS 229 9.4.1 MULTILAYER CONSTRUCTION 229 9.4.2 DIRECTED NETWORK CONSTRUCTION 229 9.4.2.1 COVALENT, METAL-BASED ASSEMBLY 229 9.4.2.2 HYPERBRANCHED-TYPE, METAL-BASED ASSEMBLY 230 9.4.2.3 HYDROGEN-BONDING ASSEMBLY 231 9.4.2.4 COVALENT ASSEMBLY 236 9.5 REFERENCES 237 10 UTILITARIAN ASPECTS 10.1 GENERAL APPLICATIONS 241 10.2 CHROMATOGRAPHY 241 10.2.1 ION EXCHANGE PROCESS 241 10.2.2 ELEKTROKINETIC CAPILLARY CHROMATOGRAPHY 241 10.2.3 SIZE EXCLUSION CHROMATOGRAPHY 242 10.2.4 GAS SEPARATION MEMBRANES 242 10.3 ELECTRONIC PROPERTIES 242 10.3.1 SEMICONDUCTION 242 10.3.2 PHOTOCHEMICAL MOLECULAR DEVICES 242 10.4 PHYSICAL PROPERTIES 243 10.4.1 SOLUBILIZATION/DRUG DELIVERY 243 10.4.2 SIZE CALIBRATION/PORE CREATION 244 10.4.3 ANTIOXIDANTS 244 10.4.4 INKS AND TONERS 244 10.4.5 LIQUID CRYSTALS 245 10.4.6 CHEMICAL SENSITIVITY 245 10.5 CATALYSIS 245 10.6 BIOCHEMICAL/PHARMACEUTICAL 245 10.6.1 SUCROSE MIMETIC 245 10.6.2 MAP/ANTIGEN 245 10.6.3 ANTIBODY CONJUGATES/LABELING 246 10.6.4 NUCLEIC ACIDS 246 10.6.5 GENE THERAPY 247 10.6.6 PHARMACEUTICAL COMPLEXES/BORON NEUTRON CAPTURE THERAPY 247 10.6.7 SPECIFIC RECEPTORS 248 10.7 SYNTHETIC ASPECTS 248 10.7.1 BUILDING BLOCK PREPARATION (PATENTS) 248 10.7.2 DENDRIMER PREPARATION (PATENTS) 249 11 APPENDICES 11.1 KEY REVIEWS AND HIGHLIGHTS 251 11.1.1 1996 REVIEWS 251 11.1.2 1995 REVIEWS 251 11.1.3 1994 REVIEWS 251 CONTENTS XI 11.1.4 1993 REVIEWS 253 11.1.5 1992 REVIEWS 253 11.1.6 1991 REVIEWS 254 11.1.7 1990 REVIEWS 255 11.1.8 1989 REVIEWS 255 11.1.9 1988 REVIEWS 255 11.1.10 1987 REVIEWS 256 11.1.11 1986 AND EARLIER REVIEWS 256 11.2 ADVANCES SERIES 256 11.3 GLOSSARY OF TERMS 257 INDEX 259
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spellingShingle	Newkome, George R. 1938- Moorefield, Charles N. Vögtle, Fritz 1939- Dendritic molecules concepts, synthesis, perspectives Dendrimeren gtt Macromoleculen gtt Structuur-activiteit-relatie gtt Synthese (chemie) gtt Macromolecular Substances Macromolecules Molecular Structure Molecular structure Sternpolymere (DE-588)4245705-1 gnd
subject_GND	(DE-588)4245705-1
title	Dendritic molecules concepts, synthesis, perspectives
title_auth	Dendritic molecules concepts, synthesis, perspectives
title_exact_search	Dendritic molecules concepts, synthesis, perspectives
title_full	Dendritic molecules concepts, synthesis, perspectives G. R. Newkome ; C. N. Moorefield ; F. Vögtle
title_fullStr	Dendritic molecules concepts, synthesis, perspectives G. R. Newkome ; C. N. Moorefield ; F. Vögtle
title_full_unstemmed	Dendritic molecules concepts, synthesis, perspectives G. R. Newkome ; C. N. Moorefield ; F. Vögtle
title_short	Dendritic molecules
title_sort	dendritic molecules concepts synthesis perspectives
title_sub	concepts, synthesis, perspectives
topic	Dendrimeren gtt Macromoleculen gtt Structuur-activiteit-relatie gtt Synthese (chemie) gtt Macromolecular Substances Macromolecules Molecular Structure Molecular structure Sternpolymere (DE-588)4245705-1 gnd
topic_facet	Dendrimeren Macromoleculen Structuur-activiteit-relatie Synthese (chemie) Macromolecular Substances Macromolecules Molecular Structure Molecular structure Sternpolymere
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007246411&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT newkomegeorger dendriticmoleculesconceptssynthesisperspectives AT moorefieldcharlesn dendriticmoleculesconceptssynthesisperspectives AT vogtlefritz dendriticmoleculesconceptssynthesisperspectives

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Holdings details from Teilbibliothek Chemie
Call Number:	0302 CHE 755f 1996 B 650 Floor plan
Copy 1	Available for loan On Shelf