Liquid chromatography column theory:
Gespeichert in:
| Beteilige Person: | |
|---|---|
| Format: | Buch |
| Sprache: | Englisch |
| Veröffentlicht: |
Chichester u.a.
Wiley
1992
|
| Schriftenreihe: | Separation science series
|
| Schlagwörter: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003676349&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Umfang: | X, 279 S. Ill., graph. Darst. |
| ISBN: | 0471933058 |
Internformat
MARC
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Datensatz im Suchindex
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|---|---|
| adam_text | LIQUID CHROMATOGRAPHY COLUMN THEORY BY RAYMOND P.W. SCOTT CHEMISTRY
DEPARTMENT, BIRKBECK COLLEGE, UNIVERSITY OF LONDON, UK AND CHEMISTRY
DEPARTMENT, GEORGETOWN UNIVERSITY, WASHINGTON DC, USA JOHN WILEY & SONS
CHICHESTER * NEW YORK * BRISBANE * TORONTO * SINGAPORE CONTENTS PREFACE
IX ACKNOWLEDGEMENTS XI 1 INTRODUCTION TO THE LIQUID CHROMATOGRAPHIC
COLUMN 1 THE FACTORS THAT CONTROL RETENTION AND SELECTIVITY 4 IONIC
INTERACTIONS 4 POLAR INTERACTIONS 5 DISPERSIVE INTERACTIONS 5 THE
PHYSICAL NATURE OF THE COLUMN 6 THE COLUMN ENVIRONMENT 8 CHROMATOGRAPHY
NOMENCLATURE 9 LC COLUMN THEORIES 12 REFERENCES 13 2 THE PLATE THEORY 15
THE SOLUTION OF THE DIFFERENTIAL EQUATION 19 THE RETENTION VOLUME OF A
SOLUTE 22 THE CAPACITY RATIO OF A SOLUTE 25 THE SEPARATION RATIO 26
REFERENCES 26 3 THE LC COLUMN DEAD VOLUME 27 REFERENCES 38 4 EXTENSIONS
OF THE PLATE THEORY 39 THE ELUTION CURVE OF A FINITE CHARGE 39 PEAK
ASYMMETRY 41 VI COLUMN EFFICIENCY 45 THE POSITION OF THE POINTS OF
INFLECTION 48 THE GAUSSIAN FORM OF THE ELUTION EQUATION 50 REFERENCES 52
5 APPLICATIONS OF THE PLATE THEORY 53 THE MAXIMUM SAMPLE VOLUME 53
VACANCY CHROMATOGRAPHY 55 THE RESOLVING POWER OF AN LC COLUMN 60 THE
EFFECTIVE PLATE NUMBER 63 THE PEAK CAPACITY OF A CHROMATOGRAPHIC COLUMN
67 PRECISION AS AN ALTERNATIVE TO RESOLUTION 74 A THEORETICAL TREATMENT
OF THE HEAT OF ADSORPTION DETECTOR 77 REFERENCES 90 6 INTRODUCTION TO
THE RATE THEORY 93 THE SUMMATION OF VARIANCES 94 EXTRA COLUMN DISPERSION
95 THE ALTERNATIVE AXIS OF A CHROMATOGRAM 96 THE RANDOM WALK MODEL 98
DISPERSION PROCESSES THAT TAKE PLACE IN AN LC COLUMN 102 THE MULTIPATH
PROCESS 102 LONGITUDINAL DIFFUSION 103 THE RESISTANCE TO MASS TRANSFER
IN THE MOBILE PHASE 105 THE RESISTANCE TO MASS TRANSFER IN THE
STATIONARY PHASE 106 REFERENCES 106 7 THE VAN DEEMTER EQUATION 109
REFERENCES 121 8 ALTERNATIVE EQUATIONS FOR PEAK DISPERSION 123 THE
GIDDINGS EQUATION 123 THE HUBER EQUATION 124 THE KNOX EQUATION 126 THE
HORVATH AND LIN EQUATION 128 THE GOLAY EQUATION 128 REFERENCES 133 9
EXPERIMENTAL VALIDATION OF THE VAN DEEMTER EQUATION 135 THE EFFECT OF
THE FUNCTION OF K ON PEAK DISPERSION 149 REFERENCES 152 VII 10 EXTRA
COLUMN DISPERSION 153 THE EFFECT OF SAMPLE VOLUME 153 THE SAMPLE VALVE
154 CONNECTING TUBES 154 LOW DISPERSION CONNECTING TUBES 158 SERPENTINE
TUBES 161 COLUMN FRITS 164 DISPERSION IN THE DETECTING CELL 164 EFFECT
OF EXTRA COLUMN DISPERSION ON COLUMN RADIUS 167 MASS SENSITIVITY 172
REFERENCES 173 11 LC COLUMN DESIGN - THE DESIGN PROTOCOL 175 PERFORMANCE
CRITERIA 176 THE REDUCED CHROMATOGRAM 177 INSTRUMENT CONSTRAINTS 179
ELECTIVE VARIABLES 181 COLUMN SPECIFICATIONS AND OPERATING CONDITIONS
182 ANALYTICAL SPECIFICATIONS 183 12 LC COLUMN DESIGN - THE DESIGN
PROCESS FOR PACKED COLUMNS 185 THE OPTIMUM PARTICLE DIAMETER 188 THE
OPTIMUM COLUMN LENGTH 192 THE MINIMUM ANALYSIS TIME 194 THE OPTIMUM
COLUMN RADIUS 196 THE OPTIMUM FLOW RATE 199 THE MINIMUM SOLVENT
CONSUMPTION 201 THE PEAK CAPACITY OF THE OPTIMIZED COLUMN 202 MAXIMUM
SAMPLE VOLUME 204 THE OPTIMUM CAPACITY RATIO 204 PACKED COLUMN DESIGN
EQUATIONS 206 COMPUTER PROGRAM FOR PACKED COLUMN DESIGN 208 GRADIENT
ELUTION 212 REFERENCES 213 13 LC COLUMN DESIGN - THE DESIGN PROCESS FOR
OPEN TUBULAR COLUMNS 215 THE OPTIMUM COLUMN RADIUS 218 THITOPTIMUM
LENGTH OF AN OPEN TUBULAR COLUMN 221 MINIMUM ANALYSIS TIME 222 THE
OPTIMUM FLOW-RATE 224 VIII MAXIMUM SAMPLE VOLUME AND MAXIMUM EXTRA
COLUMN DISPERSION 226 THE MAXIMUM PERMISSIBLE DETECTOR DISPERSION 230
DESIGN EQUATIONS 231 THE OPEN TUBULAR COLUMN IN LC 233 REFERENCES 234 14
PREPARATIVE LIQUID CHROMATOGRAPHY COLUMNS 237 PREPARATIVE COLUMN DESIGN
238 THE EFFICIENCY REQUIRED FROM THE PREPARATIVE COLUMN 238 OPTIMUM
PARTICLE DIAMETER 239 THE COLUMN LENGTH AND ANALYSIS TIME 241 THE COLUMN
RADIUS 244 THE OPTIMUM FLOW-RATE 247 SOLVENT CONSUMPTION 248 COLUMN WALL
THICKNESS 248 PREPARATIVE COLUMN DESIGN EQUATIONS 250 THE USE OF THE
DESIGN EQUATIONS 251 COMPUTER PROGRAM FOR PREPARATIVE COLUMN DESIGN 252
DISCUSSION 253 COLUMN OVERLOAD AS AN ALTERNATIVE TO COLUMN DESIGN 259
SAMPLE VOLUME OVERLOAD 259 SAMPLE MASS OVERLOAD 261 REFERENCES 263 LIST
OF SYMBOLS 265 APPENDIX 1 THE DIFFUSION COEFFICIENTS OF SOME LOW
MOLECULAR WEIGHT SUBSTANCES 268 APPENDIX 2 THE DIFFUSION COEFFICIENTS OF
SOME PEPTIDES 270 APPENDIX 3 THE PHYSICAL PROPERTIES OF SOME SOLVENTS
EMPLOYED AS MOBILE PHASES IN LC 271 INDEX 273
|
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| author | Scott, Raymond P. W. |
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| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543/.0894 |
| dewey-search | 543/.0894 |
| dewey-sort | 3543 3894 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV005872340 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T08:39:27Z |
| institution | BVB |
| isbn | 0471933058 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-003676349 |
| oclc_num | 24501839 |
| open_access_boolean | |
| owner | DE-12 |
| owner_facet | DE-12 |
| physical | X, 279 S. Ill., graph. Darst. |
| publishDate | 1992 |
| publishDateSearch | 1992 |
| publishDateSort | 1992 |
| publisher | Wiley |
| record_format | marc |
| series2 | Separation science series |
| spellingShingle | Scott, Raymond P. W. Liquid chromatography column theory Chromatographie en phase liquide ram Liquid chromatography Theorie (DE-588)4059787-8 gnd Säulenflüssigkeitschromatographie (DE-588)4348602-2 gnd |
| subject_GND | (DE-588)4059787-8 (DE-588)4348602-2 |
| title | Liquid chromatography column theory |
| title_auth | Liquid chromatography column theory |
| title_exact_search | Liquid chromatography column theory |
| title_full | Liquid chromatography column theory by Raymond P. W. Scott |
| title_fullStr | Liquid chromatography column theory by Raymond P. W. Scott |
| title_full_unstemmed | Liquid chromatography column theory by Raymond P. W. Scott |
| title_short | Liquid chromatography column theory |
| title_sort | liquid chromatography column theory |
| topic | Chromatographie en phase liquide ram Liquid chromatography Theorie (DE-588)4059787-8 gnd Säulenflüssigkeitschromatographie (DE-588)4348602-2 gnd |
| topic_facet | Chromatographie en phase liquide Liquid chromatography Theorie Säulenflüssigkeitschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003676349&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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