Chromatographic systems: maintenance and troubleshooting
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York u.a.
Acad. Pr.
1977
|
| Edition: | 2. ed. |
| Subjects: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001333336&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Physical Description: | XIII, 359 S. Ill., graph. Darst. |
| ISBN: | 0127320520 |
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MARC
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| 100 | 1 | |a Walker, John Q. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chromatographic systems |b maintenance and troubleshooting |c John Q. Walker ; Minor T. Jackson ; James B. Maynard* |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a New York u.a. |b Acad. Pr. |c 1977 | |
| 300 | |a XIII, 359 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Chromatographie - Appareils et matériel - Entretien et réparations | |
| 650 | 4 | |a Chromatographic analysis |x Equipment and supplies |x Maintenance and repair | |
| 650 | 4 | |a Chromatography, Gas |x instrumentation | |
| 650 | 4 | |a Chromatography, Liquid |x instrumentation | |
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| 650 | 0 | 7 | |a Chromatography, Gas |x instrumentation |2 mesh |
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| 700 | 1 | |a Jackson, Minor T. |e Verfasser |4 aut | |
| 700 | 1 | |a Maynard, J. Barry |e Verfasser |0 (DE-588)1059846675 |4 aut | |
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Record in the Search Index
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|---|---|
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| adam_text |
Titel: Chromatographic systems
Autor: Walker, John Q
Jahr: 1977
CONTENTS
Preface
to
Second
Edition
Preface
to
First
Edition
Acknowledgments
PART
I
—
LIQUID
CHROMATOGRAPHY
Chapter
1
Chromatographic
Systems:
Maintenance
and
Troubleshooting
Chapter
2
Solvent
Delivery
Systems
Purpose.
General
design—pulsed
vs.
pulseless.
Ideal
design.
Routine
maintenance
and
cleaning-solvents,
changing
solvents,
seals,
gaskets.
Problems
and
solutions.
Chapter
3
LC
Sample
Introduction
Systems
Purpose.
General
design—loop
injectors,
septa,
syringes,
dead-volume.
Ideal
design—loop
injector,
dead-volume.
Routine
maintenance
and
cleaning-solvents.
Problems
and
solutions.
Chapter
4
LC
Columns
(Selection
Preparation),
Column
Ovens
and
Column
Heaters
Selecting
the
type
of
separation—liquid-liquid,
liquid-solid,
gel
permeation,
ion
exchange.
Choice
of
materials—stainless
steel,
glass
fittings,
couplings.
Methods
associated
with
packing
columns.
Column
assembly—pre-columns,
purge,
dead-volume.
Problems
and
solutions.
Chapter
5
LC
Detection
Systems
Purpose.
General
designs—refractive
index,
ultraviolet,
flame,
wire-filament,
fluorimeter.
Ideal
design.
Routine
maintenance
and
cleaning-solvents.
Problems
and
solutions.
Chapter
6
Comprehensive
Troubleshooting
of
LC
Systems
Baseline
problems—noise,
drift,
spikes,
stair-stepping.
Poor
peak
shapes.
Loss
of
resolution.
Pump
and
flow
problems.
Other
problems.
3
19
41
51
63
81
v
VI
CONTENTS
PART
II
—
GAS
CHROMATOGRAPHY
Chapter
7
Introduction
to
Gas
Chromatography
95
Chapter
8
Pneumatic
and
Sample
Introduction
Systems
105
Carrier
gas
filters.
Pressure
regulators.
Rotameters.
Flow
controllers.
Sample
inlet
systems.
Gas
valves
and
splitters.
Flow
programmers.
Routine
maintenance
and
troubleshooting.
Problems
and
solutions.
Chapter
9
Pyrolytic
Inlet
Systems
137
Requirements.
Instrumentation.
Comparison
of
performance
of
various
pyrolyzers.
Troubleshooting.
Problems
and
solutions.
Chapter
10
Gas
Chromatographic
Column
Ovens
and
Temperature
Controllers
161
Column
arrangements.
Oven
designs.
Temperature
controllers
and
programmers.
Routine
maintenance.
Problems
and
solutions.
Chapter
11
Gas
Chromatography
Detectors
191
Function.
Terms
and
formulas.
Types
of
detectors:
thermal
conductivity,
flame
ionization,
electron
capture,
and
other
types
of
detectors.
Maintenance.
Troubleshooting
TCD,
FID,
ECD.
Problems
and
solutions.
Chapter
12
Integral
Electronics
223
Electrometers.
TCD
electrical
circuits.
Recorders.
Integrators.
Computer
linkups.
Problems
and
solutions.
Chapter
13
Auxiliary
Systems
257
GC
interfaces:
I.R.,
U.V.,
M.S.
Problems
and
solutions.
Chapter
14
Gas
Chromatographic
Comprehensive
Troubleshooting
277
Baseline
problems:
drift,noise,
zeroing,
cycling,
spikes.
Distorted
peaks,
ghost
peaks,
others.
Reproducibility
problems:
retention
time,
sensitivity
changes.
Other
problems.
Appendix
A
Cleaning
of
GC
Detectors
305
Appendix
B
Care
and
Handling
of
Microsyringes
309
Appendix
C
Troubleshooting
Clues
from
the
Rotameter
311
Appendix
D
Troubleshooting
of
Silicon
Controlled
Rectifier
(SCR)
Heating
Systems
313
Appendix
E
A
Rapid
Fault
Isolation
Method
317
CONTENTS
vii
Appendix
F
Gas
Chromatographic
Column
Preparation
321
Appendix
G
Glossary
of
Terms
and
Formulas
327
Appendix
H
Packing
and
Installation
Technique
for
G.C.
Columns
331
Appendix
I
Conditioning
of
G.C.
Columns
337
Appendix
J
Routine
Maintenance
of
Your
G.C.
341
Appendix
K
Gas
Chromatography
Operating
Hints
350
Index
355 |
| any_adam_object | 1 |
| author | Walker, John Q. Jackson, Minor T. Maynard, J. Barry |
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| author_facet | Walker, John Q. Jackson, Minor T. Maynard, J. Barry |
| author_role | aut aut aut |
| author_sort | Walker, John Q. |
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| building | Verbundindex |
| bvnumber | BV002039075 |
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| callnumber-subject | QD - Chemistry |
| classification_tum | CHE 230f |
| ctrlnum | (OCoLC)3003109 (DE-599)BVBBV002039075 |
| dewey-full | 681/.754 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 681 - Precision instruments and other devices |
| dewey-raw | 681/.754 |
| dewey-search | 681/.754 |
| dewey-sort | 3681 3754 |
| dewey-tens | 680 - Manufacture of products for specific uses |
| discipline | Chemie / Pharmazie Handwerk und Gewerbe / Verschiedene Technologien |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV002039075 |
| illustrated | Illustrated |
| indexdate | 2025-04-03T16:00:46Z |
| institution | BVB |
| isbn | 0127320520 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001333336 |
| oclc_num | 3003109 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-83 |
| owner_facet | DE-91G DE-BY-TUM DE-83 |
| physical | XIII, 359 S. Ill., graph. Darst. |
| psigel | TUB-nveb |
| publishDate | 1977 |
| publishDateSearch | 1977 |
| publishDateSort | 1977 |
| publisher | Acad. Pr. |
| record_format | marc |
| spellingShingle | Walker, John Q. Jackson, Minor T. Maynard, J. Barry Chromatographic systems maintenance and troubleshooting Chromatographie - Appareils et matériel - Entretien et réparations Chromatographic analysis Equipment and supplies Maintenance and repair Chromatography, Gas instrumentation Chromatography, Liquid instrumentation Chromatographie (DE-588)4010153-8 gnd Fehlerquelle (DE-588)4194427-6 gnd Chromatography, Gas instrumentation mesh Chromatography, Liquid instrumentation mesh |
| subject_GND | (DE-588)4010153-8 (DE-588)4194427-6 |
| title | Chromatographic systems maintenance and troubleshooting |
| title_auth | Chromatographic systems maintenance and troubleshooting |
| title_exact_search | Chromatographic systems maintenance and troubleshooting |
| title_full | Chromatographic systems maintenance and troubleshooting John Q. Walker ; Minor T. Jackson ; James B. Maynard* |
| title_fullStr | Chromatographic systems maintenance and troubleshooting John Q. Walker ; Minor T. Jackson ; James B. Maynard* |
| title_full_unstemmed | Chromatographic systems maintenance and troubleshooting John Q. Walker ; Minor T. Jackson ; James B. Maynard* |
| title_short | Chromatographic systems |
| title_sort | chromatographic systems maintenance and troubleshooting |
| title_sub | maintenance and troubleshooting |
| topic | Chromatographie - Appareils et matériel - Entretien et réparations Chromatographic analysis Equipment and supplies Maintenance and repair Chromatography, Gas instrumentation Chromatography, Liquid instrumentation Chromatographie (DE-588)4010153-8 gnd Fehlerquelle (DE-588)4194427-6 gnd Chromatography, Gas instrumentation mesh Chromatography, Liquid instrumentation mesh |
| topic_facet | Chromatographie - Appareils et matériel - Entretien et réparations Chromatographic analysis Equipment and supplies Maintenance and repair Chromatography, Gas instrumentation Chromatography, Liquid instrumentation Chromatographie Fehlerquelle |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001333336&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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