Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Amsterdam [u.a.]
Elsevier
1980
|
| Series: | Wilson and Wilson's Comprehensive analytical chemistry
10 |
| Subjects: | |
| Links: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000560453&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Physical Description: | XIV, 303 S. Ill., graph. Darst. |
| ISBN: | 0444418598 |
Staff View
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| 245 | 1 | 0 | |a Organic spot test analysis |c [E. Jungreis and L. Ben-Dor] |
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| 490 | 1 | |a Wilson and Wilson's Comprehensive analytical chemistry |v 10 | |
| 650 | 4 | |a Chimie analytique | |
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| 650 | 4 | |a Composés organiques - Analyse | |
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| 700 | 1 | 2 | |a Szabadváry, Ferenc |d 1923-2006 |0 (DE-588)138103828 |4 aut |t The history of analytical chemistry |
| 700 | 1 | 2 | |a Robinson, Alan |4 aut |t The history of analytical chemistry |
| 830 | 0 | |a Wilson and Wilson's Comprehensive analytical chemistry |v 10 |w (DE-604)BV000900805 |9 10 | |
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| 249 | |a The history of analytical chemistry |v [F. Szabadváry and A. Robinson] | ||
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-000560453 | |
Record in the Search Index
| _version_ | 1819371061441986560 |
|---|---|
| adam_text | Wilson and Wilson s
COMPREHENSIVE
ANALYTICAL
CHEMISTRY
Edited by
G SVEHLA, PH D,D SC ,FRIC
ReaderinAnalyticalChemistry
TheQueen sUniversityofBelfast
VOLUME X
Organic Spot Test Analysis
The History of Analytical Chemistry
ELSEVIER SCIENTIFIC PUBLISHING COMPANY
AMSTERDAM OXFORD NEW YORK
Contents
Preface x
Chapter 1 ORGANIC SPOT TEST ANALYSIS, by E Jungreis and L
Ben-Dor 1
1 Introduction 1
2 Preliminary tests 3
(A) Sensory test (color and odor) 3
(B) Behavior on ignition 3
(C)Pyrolysi s 4
(D) Acid—base and redox behavior 4
(E) Elementary analysis 9
3 Detection of functional groups 9
(A) Aromatic compounds 9
(B) Unsaturated compounds 11
(C) Hydroxy compounds 11
(1) Alcohols, 11 — (2) Phenols, 12 — (3) Aliphatic polyhydroxides,
(D) Carbonyl compounds 14
(1) Aldehydes, 16 — (2) Ketones, 17 —(3) Acids and esters, 18
(E) Ethers 19
(F) Amines 7 20
(G) Nitro compounds 22
(H) Nitriles 24
(I) Sulfur compounds 25
4 Detection of technically important individual compounds 26
(I) Acetone 26
(II) Acetic acid 27
(1) Monochloroacetic acid, 27 — (2) Dichloroacetic acid, 27 — (3)
Trichloroacetic acid, 28
(III)Acetylaceton e 28
(IV)Acetylen e 28
(V) Anthracene 28
(VI)Ascorbic acid 28
(VII) Barbituric acid 29
(VIII) Carbon disulfide 29
(IX) Carbon monoxide 29
(X) Carbon tetrachloride 29
xi
(XI) Chloroform and bromoform 30
(XII) Cinnamic acid 30
(XIII) Citric acid 30
(XIV) Cysteine 30
(XV) Diphenylamine 30
(XVI) Ethanol 31
(XVII) Formaldehyde 31
(XVIII) Formic acid 31
(XIX) Furfural 32
(XX) Glycerol 32
(XXI) Glyoxal 32
(XXII) Lactic acid 33
(XXIII) Malonic acid V 33
(XXIV) Methanol 33
(XXV) Naphthalene 34
(XXVI) Oxamide : 34
(XXVII) Oxalic acid 34
(XXVIII) Phosgene 34
(XXIX) Piperidine 34
(XXX) Pyridine 35
(XXXI) Quinones : ! 35
(XXXII) Salicylaldehyde ! 36
(XXXIII) Tartaric acid 36
(XXXIV) Thiophen 36
(XXXV) Tyrosine 36
(XXXVI) Urea 36
5 Differentiation of isomers 37
(A) Aminobenzenesulfonic acids 37
(B) Aminobenzoic acids 38
(C) Nitroanilines • • 38
• (D) Dinitroanilines • 39
(E) *Nitrobenzaldehydes • 39
(F) Dihydroxybenzenes 40
(G) Trihydroxybenzenes 40
(H) Naphthols 40
(I) Naphthylamines 41
(J) Aminophenols ; 41
(K) Nitrophenols 42
(L) Phenylenediamines 42
6 Selected test procedures 43
(1) Alcohols, 43 — (2) Phenols, 43 — (3) Aliphatic polyhydroxides, -
43 —(4) Aldehydes, 44 —(5) Aliphatic aldehydes and ketones, ^
44 — (6) Aromatic aldehydes, 44 — (7) Ketones, 44 — (8) Carbox-
ylic acids, 45 —(9) Alkyl esters of carboxylic acids, 45 (10)
Ethers, 45 —(11) Amines (primary, secondary, tertiary; aliphatic
and aromatic), 46 —(12) Primary and secondary amines (aliphatic
and aromatic), 46 — (13) Primary and secondary aliphatic amines,
46 — (14) Aliphatic secondary amines, 46 —(15) Nitro compounds,
47 —(16) Primary aliphatic nitro compounds, 47 — (17) Primary
xii
and secondary aliphatic nitro compounds, 17—(18) Nitriles,
48 — (19) Thioketones and thiols, 48 — (20) Sulfonic acids,
48 —(21) Acetone, 49 — (22) Acetic acid, 49 — (23) Acetylene,
49 — (24) Barbituric acid, 49 —(25) Carbon disulfide, 50 —(26)
Carbon tetrachloride, 50 — (27) Citric acid, 50 — (28) Cysteine;
50 — (29) Ethanol, 51 — (30) Formaldehyde, 50—(31) Formic
acid, 51 — (32) Glycerol, 52 — (33) Malonic acid, 52 —(34)
Naphthalene, 52 — (35) Oxalic acid, 53 — (36) Piperidine, 53 — (37)
Pyridine and derivatives, 53 — (38) Quinones, 53 —(39) Salicylal
dehyde, 54 — (40) Urea, 54
References 54
Chapter 2 THE HISTORY OF ANALYTICAL CHEMISTRY, by F
Szabadvary and A Robinson 61
1 Analytical chemistry before 1700 61
(A) Ancient science 61
(B) Origin of chemistry : 62
(C) Early analysis 63
(D) Alchemy 65
(E) Knowledge of analysis 68
(F) Clarification of chemical concepts 73
(G) The beginning of analysis in aqueous solutions 1 78
(H) Robert Boyle 81
2 The 18th century : 86
(A) The phlogiston theory 86
(B) The blowpipe 90
•(C) Further light on reactions in solution 92
(D) Gas analysis 97
(E) Torbern Bergman 105
(F) Quantitativefanalysis before Laviosier Ill
(G) Indestructibility of matter 114
(H) Stoichiometry 117
3 The period of Berzelius 126
(A) The composition of minerals 126
(B) Berzelius 132
(C) Atomic weights 138
(D) Apparatus and methods at the time of Berzelius 141
(E) Early analytical textbooks 144
4 Qualitative and gravimetric analysis 146
(A) Introduction of systematic tests for the ions 146
(B) Gravimetric analysis 154
(C) Microanalysis1 161
5 Volumetric analysis 165
(A) Early history of titrimetry 165
(B) From Descroizilles to Gay-Lussac 169
(C) From Gay-Lussac to Mohr 178
(D) Friedrich Mohr 184
xiii
(E) Titrimetry before synthetic indicators 190
(F) Indicators 194
(G) More recent titrimetric analysis 198
6 Organic elemental analysis 200
(A) From Lavoisier to Liebig 200
(B) From Liebig to Pregl 204
7 Instrumental methods 214
(A) Electrogravimetry 214
(B) Optical methods 218
(C) Kirchhoff and Bunsen 221
(D) Further development of spectrum analysis 227
(E) Colorimetry 230
(F) The measurement of pH 235
(G) Potentiometric titration 237
(H) Conductometric titrations 240
(I) Polarography 241
8 Development of the theory of analytical chemistry 243
(A) Development of physical chemistry 243
(B) Wilhelm Ostwald 244
(C) Development of the concept of pH 249
(D) Theory of titration 251
9 Other methods of analysis 255
(A) Radiochemical analysis 255
(B) Chromatography 257
(C) Ion exchange 260
(D) Conclusion 261
References 261
Index 283
t
xiv
|
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| id | DE-604.BV000908902 |
| illustrated | Illustrated |
| indexdate | 2024-12-20T07:28:31Z |
| institution | BVB |
| isbn | 0444418598 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000560453 |
| oclc_num | 421841698 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-188 |
| owner_facet | DE-19 DE-BY-UBM DE-188 |
| physical | XIV, 303 S. Ill., graph. Darst. |
| publishDate | 1980 |
| publishDateSearch | 1980 |
| publishDateSort | 1980 |
| publisher | Elsevier |
| record_format | marc |
| series | Wilson and Wilson's Comprehensive analytical chemistry |
| series2 | Wilson and Wilson's Comprehensive analytical chemistry |
| spellingShingle | Jungreis, Ervin 1926- Ben-Dor, L. Szabadváry, Ferenc 1923-2006 Robinson, Alan Organic spot test analysis Wilson and Wilson's Comprehensive analytical chemistry Chimie analytique Chimie analytique - Histoire Composés organiques - Analyse |
| title | Organic spot test analysis |
| title_alt | The history of analytical chemistry |
| title_auth | Organic spot test analysis |
| title_exact_search | Organic spot test analysis |
| title_full | Organic spot test analysis [E. Jungreis and L. Ben-Dor] |
| title_fullStr | Organic spot test analysis [E. Jungreis and L. Ben-Dor] |
| title_full_unstemmed | Organic spot test analysis [E. Jungreis and L. Ben-Dor] |
| title_short | Organic spot test analysis |
| title_sort | organic spot test analysis |
| topic | Chimie analytique Chimie analytique - Histoire Composés organiques - Analyse |
| topic_facet | Chimie analytique Chimie analytique - Histoire Composés organiques - Analyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000560453&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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